##TITLE=              31P MAS NMR spectrum of as-made AlPO-5 (with fluoride and tetrapropylammonium template)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Gougeon et al. J. Phys. Chem. B, 105, 12249-12256 (2001) Figure 5b
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/15 15:05:11
##SOURCE REFERENCE=   AFI-31P-Gougeon-2001-asmade-TPAF
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              AFI
##NAMES=              AlPO-5
##SAMPLE DESCRIPTION= AlPO-5, as-made

$$Bibliographic information 
##$AUTHORS=           Gougeon, R.D., Brouwer, E.B., Bodart, P.R., Delmotte, L., Marichal, C., ChA~(c)zeau, J.M., Harris, R.K.
##$TITLE=             Solid-state NMR studies of the as-synthesized AlPO4-5/TPAF microporous aluminophosphate
##$JOURNAL=           Journal of Physical Chemistry B
##$VOLUME=            105
##$PAGES=             12249-12256
##$YEAR=              2001
##$DOI=               10.1021/jp0111214
##$FIGURE=            Figure 5b

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         6
##$PEAK LABELS=        A          B          C          D          E          F         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -32.1437   -31.8637   -30.6313   -29.3459   -29.0559   -23.4248   
##$PEAK AREAS=         1.         1.         1.         1.         1.         1.        
##$PEAK WIDTHS=        4.79309    4.79309    4.79309    4.79309    4.79309    4.79309   
##$PEAK SHAPES=        0          0          0          0          0          0         
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           One of the the six P sites is distinguished by its proximity to the fluoride ion

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 162.0
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              2.                   
##LASTX=              -57.8                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            300
##FIRSTY=             -0.01061              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  2.                 -0.01061              
  1.8                -0.01030              
  1.6                -0.00924              
  1.4                -0.00860              
  1.2                -0.00859              
  1.                 -0.00769              
  0.8                -0.00656              
  0.6                -0.00763              
  0.4                -0.00910              
  0.2                -0.01004              
  0.00000            -0.01120              
 -0.2                -0.01228              
 -0.4                -0.01408              
 -0.6                -0.01617              
 -0.8                -0.01818              
 -1.                 -0.01969              
 -1.2                -0.01943              
 -1.4                -0.01781              
 -1.6                -0.0162               
 -1.8                -0.01435              
 -2.                 -0.01211              
 -2.2                -0.01063              
 -2.4                -0.00921              
 -2.6                -0.00860              
 -2.8                -0.00859              
 -3.                 -0.00889              
 -3.2                -0.00994              
 -3.4                -0.01175              
 -3.6                -0.01375              
 -3.8                -0.01592              
 -4.                 -0.01848              
 -4.2                -0.01839              
 -4.4                -0.01677              
 -4.6                -0.01502              
 -4.8                -0.01165              
 -5.                 -0.00840              
 -5.2                -0.00516              
 -5.4                -0.00064              
 -5.6                 0.00338              
 -5.8                 0.00438              
 -6.                  0.00169              
 -6.2                -0.00137              
 -6.4                -0.00425              
 -6.6                -0.00683              
 -6.8                -0.00804              
 -7.                 -0.00827              
 -7.2                -0.00649              
 -7.4                -0.00331              
 -7.6                 0.00110              
 -7.8                 0.00661              
 -8.                  0.01221              
 -8.2                 0.01722              
 -8.4                 0.01945              
 -8.6                 0.02040              
 -8.8                 0.02051              
 -9                   0.01985              
 -9.2                 0.01766              
 -9.4                 0.01378              
 -9.6                 0.01007              
 -9.8                 0.00688              
 -10.                 0.00363              
 -10.2                0.00151              
 -10.4                0.00154              
 -10.6                0.00155              
 -10.8                0.00155              
 -11.                 0.00155              
 -11.2                0.00081              
 -11.4               -0.00070              
 -11.6               -0.00194              
 -11.8               -0.00248              
 -12.                -0.00250              
 -12.2               -0.00104              
 -12.4                0.00104              
 -12.6                0.00473              
 -12.8                0.00941              
 -13.                 0.01306              
 -13.2                0.01553              
 -13.4                0.01688              
 -13.6                0.01839              
 -13.8                0.01757              
 -14.                 0.01438              
 -14.2                0.01224              
 -14.4                0.01014              
 -14.6                0.00831              
 -14.8                0.00736              
 -15.                 0.00576              
 -15.2                0.00604              
 -15.4                0.00748              
 -15.6                0.00889              
 -15.8                0.01096              
 -16.                 0.01171              
 -16.2                0.01223              
 -16.4                0.01314              
 -16.6                0.01370              
 -16.8                0.01373              
 -17.                 0.01374              
 -17.2                0.01454              
 -17.4                0.01547              
 -17.6                0.01631              
 -17.8                0.01841              
 -18.                 0.02021              
 -18.2                0.02202              
 -18.4                0.02492              
 -18.6                0.02818              
 -18.8                0.03127              
 -19.                 0.03342              
 -19.2                0.03484              
 -19.4                0.03668              
 -19.6                0.03986              
 -19.8                0.04329              
 -20.                 0.04696              
 -20.2                0.05292              
 -20.4                0.05939              
 -20.6                0.06560              
 -20.8                0.07188              
 -21.                 0.08107              
 -21.2                0.08961              
 -21.4                0.09643              
 -21.6                0.10454              
 -21.8                0.11422              
 -22.                 0.12505              
 -22.2                0.13597              
 -22.4                0.14709              
 -22.6                0.15894              
 -22.8                0.16839              
 -23.                 0.17457              
 -23.2                0.18221              
 -23.4                0.18721              
 -23.6                0.18718              
 -23.8                0.18434              
 -24.                 0.17961              
 -24.2                0.17443              
 -24.4                0.16890              
 -24.6                0.16410              
 -24.8                0.16032              
 -25.                 0.15884              
 -25.2                0.16158              
 -25.4                0.16707              
 -25.6                0.17474              
 -25.8                0.18892              
 -26.                 0.20494              
 -26.2                0.22064              
 -26.4                0.24224              
 -26.6                0.26993              
 -26.8                0.29787              
 -27.                 0.32676              
 -27.2                0.36067              
 -27.4                0.39944              
 -27.6                0.43677              
 -27.8                0.47253              
 -28.                 0.51226              
 -28.2                0.55039              
 -28.4                0.58634              
 -28.6                0.62090              
 -28.8                0.65004              
 -29.                 0.67712              
 -29.2                0.70438              
 -29.4                0.72839              
 -29.6                0.74939              
 -29.8                0.76958              
 -30.                 0.78351              
 -30.2                0.79278              
 -30.4                0.79924              
 -30.6                0.80399              
 -30.8                0.80599              
 -31.                 0.80329              
 -31.2                0.79540              
 -31.4                0.78216              
 -31.6                0.76478              
 -31.8                0.74465              
 -32.                 0.71677              
 -32.2                0.68299              
 -32.4                0.64687              
 -32.6                0.60959              
 -32.8                0.56625              
 -33.                 0.52402              
 -33.2                0.48212              
 -33.4                0.43727              
 -33.6                0.3954               
 -33.8                0.35188              
 -34.                 0.30577              
 -34.2                0.26442              
 -34.4                0.23475              
 -34.6                0.20317              
 -34.8                0.17473              
 -35.                 0.15219              
 -35.2                0.13172              
 -35.4                0.11282              
 -35.6                0.09680              
 -35.8                0.08381              
 -36.                 0.07297              
 -36.2                0.06424              
 -36.4                0.05879              
 -36.6                0.05550              
 -36.8                0.05049              
 -37.                 0.04689              
 -37.2                0.04422              
 -37.4                0.04085              
 -37.6                0.03653              
 -37.8                0.03272              
 -38                  0.02901              
 -38.2                0.02389              
 -38.4                0.01951              
 -38.6                0.01591              
 -38.8                0.01267              
 -39.                 0.01050              
 -39.2                0.00966              
 -39.4                0.01068              
 -39.6                0.01176              
 -39.8                0.01310              
 -40.                 0.01494              
 -40.2                0.01604              
 -40.4                0.01712              
 -40.6                0.01781              
 -40.8                0.01780              
 -41.                 0.01687              
 -41.2                0.01548              
 -41.4                0.01439              
 -41.6                0.01258              
 -41.8                0.01099              
 -42.                 0.01008              
 -42.2                0.00969              
 -42.4                0.00863              
 -42.6                0.00761              
 -42.8                0.00764              
 -43.                 0.00684              
 -43.2                0.00532              
 -43.4                0.00459              
 -43.6                0.00459              
 -43.8                0.00459              
 -44.                 0.00470              
 -44.2                0.00623              
 -44.4                0.00766              
 -44.6                0.00765              
 -44.8                0.00676              
 -45.                 0.00384              
 -45.2                0.00125              
 -45.4               -0.00073              
 -45.6               -0.00340              
 -45.8               -0.00542              
 -46.                -0.00744              
 -46.2               -0.00858              
 -46.4               -0.00858              
 -46.6               -0.00832              
 -46.8               -0.00740              
 -47.                -0.00537              
 -47.2               -0.00303              
 -47.4               -0.00123              
 -47.6                0.00008              
 -47.8               -0.00050              
 -48.                -0.00206              
 -48.2               -0.00385              
 -48.4               -0.00672              
 -48.6               -0.00883              
 -48.8               -0.01006              
 -49.                -0.01060              
 -49.2               -0.01062              
 -49.4               -0.00988              
 -49.6               -0.00890              
 -49.8               -0.00735              
 -50.                -0.00527              
 -50.2               -0.00556              
 -50.4               -0.00699              
 -50.6               -0.00800              
 -50.8               -0.00860              
 -51.                -0.00859              
 -51.2               -0.00859              
 -51.4               -0.00859              
 -51.6               -0.00859              
 -51.8               -0.00796              
 -52.                -0.00663              
 -52.2               -0.00413              
 -52.4               -0.00175              
 -52.6               -0.00018              
 -52.8                0.00112              
 -53.                 0.00155              
 -53.2                0.00155              
 -53.4                0.00155              
 -53.6                0.00155              
 -53.8                0.00155              
 -54.                 0.00155              
 -54.2                0.00155              
 -54.4                0.00155              
 -54.6                0.00155              
 -54.8                0.00214              
 -55.                 0.00372              
 -55.2                0.00405              
 -55.4                0.00249              
 -55.6                0.00125              
 -55.8                0.00029              
 -56.                -0.00147              
 -56.2               -0.00252              
 -56.4               -0.00250              
 -56.6               -0.00250              
 -56.8               -0.00250              
 -57.                -0.00216              
 -57.2               -0.00109              
 -57.4               -0.00047              
 -57.6               -0.00138              
 -57.8               -0.00245              
##END=
