##TITLE=              31P MAS NMR spectrum of calcined and dehydrated AlPO-5
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Meinhold and Tapp. J. Chem. Soc., Chem. Commun., 219-220 (1990) Figure 1
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/15 15:18:43
##SOURCE REFERENCE=   AFI-31P-Meinhold-1990-calcined
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              AFI
##NAMES=              AlPO-5
##SAMPLE DESCRIPTION= AlPO-5, calcined

$$Bibliographic information 
##$AUTHORS=           Meinhold, R.H., Tapp, N.J.
##$TITLE=             An NMR study of the reaction of water with AlPO4-5
##$JOURNAL=           Journal of the Chemical Society, Chemical Communications
##$VOLUME=            
##$PAGES=             219-220
##$YEAR=              1990
##$DOI=               10.1039/C39900000219
##$FIGURE=            Figure 1

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         3
##$PEAK LABELS=        A          B          C         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -30.2595   -27.0855   -26.1091   
##$PEAK AREAS=         1.         1.         1.        
##$PEAK WIDTHS=        4.04629    4.04629    4.04629   
##$PEAK SHAPES=        0          0          0         
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Calcined AlPO-5 has interesting dynamic disorder - see Liu et al, Solid State Sci., 5, 427-434 (2003)

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 80.96
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     5000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              2.6                  
##LASTX=              -47.                  
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            249
##FIRSTY=             -0.00164              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  2.6                -0.00164              
  2.4                -0.00212              
  2.2                -0.00243              
  2.                 -0.00261              
  1.8                -0.00238              
  1.6                -0.00207              
  1.4                -0.00187              
  1.2                -0.00189              
  1.                 -0.00189              
  0.8                -0.00188              
  0.6                -0.00189              
  0.4                -0.00225              
  0.2                -0.00265              
 -0.00000            -0.00261              
 -0.2                -0.00262              
 -0.4                -0.00262              
 -0.6                -0.00262              
 -0.8                -0.00262              
 -1.                 -0.00262              
 -1.2                -0.00262              
 -1.4                -0.00214              
 -1.6                -0.00143              
 -1.8                -0.00142              
 -2.                 -0.00173              
 -2.2                -0.00190              
 -2.4                -0.00188              
 -2.6                -0.00189              
 -2.8                -0.00189              
 -3.                 -0.00189              
 -3.2                -0.00189              
 -3.4                -0.00189              
 -3.6                -0.00189              
 -3.8                -0.00188              
 -4.                 -0.00189              
 -4.2                -0.00187              
 -4.4                -0.00146              
 -4.6                -0.00111              
 -4.8                -0.00117              
 -5.                 -0.00113              
 -5.2                -0.00121              
 -5.4                -0.00141              
 -5.6                -0.00144              
 -5.8                -0.00151              
 -6.                 -0.00136              
 -6.2                -0.00159              
 -6.4                -0.00193              
 -6.6                -0.00187              
 -6.8                -0.00189              
 -7.                 -0.00189              
 -7.2                -0.00186              
 -7.4                -0.00145              
 -7.6                -0.00068              
 -7.8                -0.00042              
 -8.                 -0.00042              
 -8.2                -0.00042              
 -8.4                -0.00042              
 -8.6                -0.00042              
 -8.8                -0.00042              
 -9.                 -0.00041              
 -9.2                -0.00045              
 -9.4                -0.00067              
 -9.6                -0.00061              
 -9.8                -0.00041              
 -10.                -0.00043              
 -10.2               -0.00042              
 -10.4               -0.00042              
 -10.6               -0.00042              
 -10.8               -0.00042              
 -11.                -0.00042              
 -11.2               -0.00042              
 -11.4               -0.00042              
 -11.6               -0.00042              
 -11.8               -0.00042              
 -12.                -0.00042              
 -12.2               -0.00042              
 -12.4               -0.00042              
 -12.6               -0.00042              
 -12.8               -0.00043              
 -13.                -0.00042              
 -13.2               -0.00045              
 -13.4               -0.00034              
 -13.6                0.00012              
 -13.8                0.00034              
 -14.                 0.00020              
 -14.2               -0.00024              
 -14.4               -0.00000              
 -14.6                0.00034              
 -14.8                0.00030              
 -15.                 0.00017              
 -15.2               -0.00007              
 -15.4                0.00010              
 -15.6               -0.00012              
 -15.8               -0.00047              
 -16.                -0.00041              
 -16.2               -0.00044              
 -16.4               -0.00037              
 -16.6               -0.00011              
 -16.8                0.00014              
 -17.                 0.00029              
 -17.2                0.00029              
 -17.4                0.00030              
 -17.6                0.00030              
 -17.8                0.00030              
 -18.                 0.00030              
 -18.2                0.00030              
 -18.4                0.00030              
 -18.6                0.00030              
 -18.8                0.00030              
 -19.                 0.00030              
 -19.2                0.00030              
 -19.4                0.00030              
 -19.6                0.00030              
 -19.8                0.00030              
 -20.                 0.00030              
 -20.2                0.00026              
 -20.4                0.00038              
 -20.6                0.00109              
 -20.8                0.00212              
 -21.                 0.00348              
 -21.2                0.00454              
 -21.4                0.00581              
 -21.6                0.00714              
 -21.8                0.00822              
 -22.                 0.01054              
 -22.2                0.01504              
 -22.4                0.02049              
 -22.6                0.02665              
 -22.8                0.03715              
 -23.                 0.05177              
 -23.2                0.06400              
 -23.4                0.07672              
 -23.6                0.09410              
 -23.8                0.11795              
 -24.                 0.14559              
 -24.2                0.17074              
 -24.4                0.20816              
 -24.6                0.24372              
 -24.8                0.26625              
 -25.                 0.31029              
 -25.2                0.35740              
 -25.4                0.38446              
 -25.6                0.40333              
 -25.8                0.42555              
 -26.                 0.44515              
 -26.2                0.45348              
 -26.4                0.45784              
 -26.6                0.45932              
 -26.8                0.45967              
 -27.                 0.45727              
 -27.2                0.45239              
 -27.4                0.44469              
 -27.6                0.43920              
 -27.8                0.43227              
 -28.                 0.42145              
 -28.2                0.41254              
 -28.4                0.40527              
 -28.6                0.39458              
 -28.8                0.38082              
 -29.                 0.37174              
 -29.2                0.36058              
 -29.4                0.34457              
 -29.6                0.33220              
 -29.8                0.32173              
 -30.                 0.30546              
 -30.2                0.28847              
 -30.4                0.27295              
 -30.6                0.25891              
 -30.8                0.24196              
 -31.                 0.22274              
 -31.2                0.20849              
 -31.4                0.19305              
 -31.6                0.17310              
 -31.8                0.15629              
 -32.                 0.14370              
 -32.2                0.12740              
 -32.4                0.11130              
 -32.6                0.09960              
 -32.8                0.08796              
 -33.                 0.07424              
 -33.2                0.06280              
 -33.4                0.05292              
 -33.6                0.04449              
 -33.8                0.03692              
 -34.                 0.02978              
 -34.2                0.02388              
 -34.4                0.01906              
 -34.6                0.01488              
 -34.8                0.01197              
 -35.                 0.00895              
 -35.2                0.00634              
 -35.4                0.00583              
 -35.6                0.00431              
 -35.8                0.00235              
 -36.                 0.00171              
 -36.2                0.00177              
 -36.4                0.00176              
 -36.6                0.00172              
 -36.8                0.00135              
 -37.                 0.00103              
 -37.2                0.00140              
 -37.4                0.00175              
 -37.6                0.00127              
 -37.8                0.00115              
 -38.                 0.00183              
 -38.2                0.00200              
 -38.4                0.00174              
 -38.6                0.00176              
 -38.8                0.00176              
 -39.                 0.00176              
 -39.2                0.00176              
 -39.4                0.00176              
 -39.6                0.00176              
 -39.8                0.00176              
 -40.                 0.00176              
 -40.2                0.00179              
 -40.4                0.00170              
 -40.6                0.00123              
 -40.8                0.00149              
 -41.                 0.00225              
 -41.2                0.00249              
 -41.4                0.00208              
 -41.6                0.00172              
 -41.8                0.00177              
 -42.                 0.00176              
 -42.2                0.00176              
 -42.4                0.00176              
 -42.6                0.00176              
 -42.8                0.00176              
 -43.                 0.00176              
 -43.2                0.00176              
 -43.4                0.00175              
 -43.6                0.00180              
 -43.8                0.00207              
 -44.                 0.00214              
 -44.2                0.00230              
 -44.4                0.00251              
 -44.6                0.00249              
 -44.8                0.00249              
 -45.                 0.00251              
 -45.2                0.00243              
 -45.4                0.00222              
 -45.6                0.00225              
 -45.8                0.00225              
 -46.                 0.00223              
 -46.2                0.00212              
 -46.4                0.00224              
 -46.6                0.00251              
 -46.8                0.00249              
 -47.                 0.00249              
##END=
