##TITLE=              31P MAS NMR spectrum of calcined AlPO-41
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Caldarelli et al. J. Phys. Chem. B, 103, 5477-5487 (1999) Figure 3a
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/15 16:51:26
##SOURCE REFERENCE=   AFO-31P-Caldarelli-1999-calcined
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              AFO
##NAMES=              AlPO-41
##SAMPLE DESCRIPTION= AlPO-41, calcined

$$Bibliographic information 
##$AUTHORS=           Caldarelli, S., Meden, A., Tuel, A.
##$TITLE=             Solid-state nuclear magnetic resonance study of the microporous aluminophosphate AlPO4-41
##$JOURNAL=           Journal of Physical Chemistry B
##$VOLUME=            103
##$PAGES=             5477-5487
##$YEAR=              1999
##$DOI=               10.1021/jp990667b
##$FIGURE=            Figure 3a

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         5
##$PEAK LABELS=        A          B          C          D          E         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -31.3772   -30.3581   -30.0065   -29.7065   -28.481    
##$PEAK AREAS=         1.         1.         1.         1.         1.        
##$PEAK WIDTHS=        2.0031     2.0031     2.0031     2.0031     2.0031    
##$PEAK SHAPES=        0.23351    0.23351    0.23351    0.23351    0.23351   
##$NUMBERING REF=     Kirchner and Bennett. Zeolites, 14, 523-528 (1994)
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 161.2
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     14000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -4.9                  
##LASTX=              -44.8                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            400
##FIRSTY=             -0.00334              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -4.9                -0.00334              
 -5.                 -0.00350              
 -5.1                -0.00254              
 -5.2                 0.00105              
 -5.3                 0.00404              
 -5.4                 0.00380              
 -5.5                -0.00123              
 -5.6                -0.00388              
 -5.7                -0.00328              
 -5.8                -0.00344              
 -5.9                -0.00267              
 -6.                 -0.00072              
 -6.1                 0.00236              
 -6.2                 0.00389              
 -6.3                 0.00217              
 -6.4                 0.00082              
 -6.5                 0.00096              
 -6.6                 0.00117              
 -6.7                 0.00052              
 -6.8                -0.00089              
 -6.9                -0.00467              
 -7.                 -0.00629              
 -7.1                -0.00492              
 -7.2                -0.00168              
 -7.3                -0.00142              
 -7.4                -0.00432              
 -7.5                -0.00777              
 -7.6                -0.00961              
 -7.7                -0.00559              
 -7.8                -0.00018              
 -7.9                 0.00363              
 -8.                  0.00515              
 -8.1                 0.00529              
 -8.2                 0.00447              
 -8.3                 0.00051              
 -8.4                -0.00331              
 -8.5                -0.00612              
 -8.6                -0.00719              
 -8.7                -0.00196              
 -8.8                 0.00339              
 -8.9                 0.00536              
 -9.                  0.00286              
 -9.1                -0.00207              
 -9.2                -0.00325              
 -9.3                -0.00354              
 -9.4                -0.00261              
 -9.5                -0.00042              
 -9.6                 0.00290              
 -9.7                 0.00416              
 -9.8                 0.00643              
 -9.9                 0.00928              
 -10.                 0.00732              
 -10.1                0.00187              
 -10.2               -0.00100              
 -10.3                0.00040              
 -10.4                0.00222              
 -10.5                0.00428              
 -10.6                0.00541              
 -10.7                0.00523              
 -10.8                0.00407              
 -10.9               -0.00012              
 -11.                -0.00277              
 -11.1                0.00005              
 -11.2                0.00305              
 -11.3                0.00406              
 -11.4                0.00593              
 -11.5                0.00720              
 -11.6                0.00858              
 -11.7                0.01194              
 -11.8                0.01189              
 -11.9                0.00212              
 -12.                 0.00018              
 -12.1                0.00429              
 -12.2                0.01046              
 -12.3                0.01411              
 -12.4                0.01230              
 -12.5                0.00732              
 -12.6                0.00584              
 -12.7                0.00559              
 -12.8                0.00330              
 -12.9               -0.00044              
 -13.                -0.00323              
 -13.1               -0.00313              
 -13.2               -0.00229              
 -13.3                0.00006              
 -13.4                0.00333              
 -13.5                0.00467              
 -13.6                0.00223              
 -13.7               -0.00036              
 -13.8               -0.00197              
 -13.9               -0.00299              
 -14.                -0.00348              
 -14.1               -0.00338              
 -14.2               -0.00336              
 -14.3               -0.00338              
 -14.4               -0.00096              
 -14.5                0.00198              
 -14.6               -0.00019              
 -14.7                0.00117              
 -14.8                0.00306              
 -14.9                0.00072              
 -15.                -0.00500              
 -15.1               -0.00628              
 -15.2               -0.00086              
 -15.3                0.00091              
 -15.4                0.00104              
 -15.5                0.00177              
 -15.6                0.00096              
 -15.7               -0.00167              
 -15.8               -0.00282              
 -15.9               -0.00086              
 -16.                 0.00114              
 -16.1                0.00325              
 -16.2                0.00499              
 -16.3                0.00564              
 -16.4                0.00716              
 -16.5                0.00348              
 -16.6               -0.00040              
 -16.7                0.00037              
 -16.8                0.00473              
 -16.9                0.00954              
 -17.                 0.00741              
 -17.1                0.00398              
 -17.2                0.00085              
 -17.3               -0.00166              
 -17.4               -0.00099              
 -17.5               -0.00151              
 -17.6               -0.00184              
 -17.7               -0.00110              
 -17.8               -0.00182              
 -17.9               -0.00316              
 -18.                -0.00343              
 -18.1               -0.00337              
 -18.2               -0.00354              
 -18.3               -0.00130              
 -18.4                0.00507              
 -18.5                0.00595              
 -18.6                0.00261              
 -18.7                0.00357              
 -18.8                0.00367              
 -18.9               -0.00191              
 -19                 -0.01039              
 -19.1               -0.01255              
 -19.2               -0.00432              
 -19.3                0.00119              
 -19.4                0.00339              
 -19.5                0.00395              
 -19.6                0.00498              
 -19.7                0.00476              
 -19.8                0.00265              
 -19.9                0.00111              
 -20.                 0.00180              
 -20.1                0.00377              
 -20.2                0.00757              
 -20.3                0.01038              
 -20.4                0.00933              
 -20.5                0.00771              
 -20.6                0.00725              
 -20.7                0.00608              
 -20.8                0.00379              
 -20.9                0.00336              
 -21.                 0.00376              
 -21.1                0.00472              
 -21.2                0.00533              
 -21.3                0.00517              
 -21.4                0.00530              
 -21.5                0.00447              
 -21.6                0.00359              
 -21.7                0.00343              
 -21.8                0.00365              
 -21.9                0.00229              
 -22.                 0.00092              
 -22.1                0.00114              
 -22.2                0.00109              
 -22.3                0.00207              
 -22.4                0.00292              
 -22.5                0.00168              
 -22.6                0.00348              
 -22.7                0.00565              
 -22.8                0.00304              
 -22.9               -0.00073              
 -23.                 0.00188              
 -23.1                0.00615              
 -23.2                0.00360              
 -23.3                0.00110              
 -23.4                0.00201              
 -23.5                0.00322              
 -23.6                0.00410              
 -23.7                0.00508              
 -23.8                0.00444              
 -23.9                0.00204              
 -24.                 0.00332              
 -24.1                0.00920              
 -24.2                0.01145              
 -24.3                0.00914              
 -24.4                0.00724              
 -24.5                0.00878              
 -24.6                0.00943              
 -24.7                0.00714              
 -24.8                0.00844              
 -24.9                0.01018              
 -25.                 0.00989              
 -25.1                0.01072              
 -25.2                0.01580              
 -25.3                0.02146              
 -25.4                0.01990              
 -25.5                0.01609              
 -25.6                0.01597              
 -25.7                0.01959              
 -25.8                0.02341              
 -25.9                0.02904              
 -26.                 0.03922              
 -26.1                0.04717              
 -26.2                0.05149              
 -26.3                0.05576              
 -26.4                0.05930              
 -26.5                0.06467              
 -26.6                0.07142              
 -26.7                0.08203              
 -26.8                0.09528              
 -26.9                0.11512              
 -27.                 0.13189              
 -27.1                0.15074              
 -27.2                0.17116              
 -27.3                0.19866              
 -27.4                0.22646              
 -27.5                0.24813              
 -27.6                0.28777              
 -27.7                0.32557              
 -27.8                0.36779              
 -27.9                0.41054              
 -28.                 0.44590              
 -28.1                0.49648              
 -28.2                0.55204              
 -28.3                0.59661              
 -28.4                0.64154              
 -28.5                0.69814              
 -28.6                0.75806              
 -28.7                0.81731              
 -28.8                0.87483              
 -28.9                0.92650              
 -29.                 0.98397              
 -29.1                1.04507              
 -29.2                1.10704              
 -29.3                1.16199              
 -29.4                1.2063               
 -29.5                1.26464              
 -29.6                1.3213               
 -29.7                1.36216              
 -29.8                1.39289              
 -29.9                1.41239              
 -30.                 1.42949              
 -30.1                1.44199              
 -30.2                1.44943              
 -30.3                1.44855              
 -30.4                1.4258               
 -30.5                1.39783              
 -30.6                1.35137              
 -30.7                1.30366              
 -30.8                1.26984              
 -30.9                1.21983              
 -31.                 1.15125              
 -31.1                1.08859              
 -31.2                1.02817              
 -31.3                0.95886              
 -31.4                0.88152              
 -31.5                0.80871              
 -31.6                0.74008              
 -31.7                0.68139              
 -31.8                0.61926              
 -31.9                0.54999              
 -32.                 0.48738              
 -32.1                0.43300              
 -32.2                0.38917              
 -32.3                0.34104              
 -32.4                0.29264              
 -32.5                0.24961              
 -32.6                0.21864              
 -32.7                0.19119              
 -32.8                0.16373              
 -32.9                0.13923              
 -33.                 0.11729              
 -33.1                0.10215              
 -33.2                0.09036              
 -33.3                0.08135              
 -33.4                0.07375              
 -33.5                0.06723              
 -33.6                0.06317              
 -33.7                0.05931              
 -33.8                0.05462              
 -33.9                0.04989              
 -34.                 0.04339              
 -34.1                0.03540              
 -34.2                0.02929              
 -34.3                0.02734              
 -34.4                0.02688              
 -34.5                0.02753              
 -34.6                0.02683              
 -34.7                0.02202              
 -34.8                0.01455              
 -34.9                0.01360              
 -35.                 0.01667              
 -35.1                0.01982              
 -35.2                0.02070              
 -35.3                0.01794              
 -35.4                0.01642              
 -35.5                0.01666              
 -35.6                0.01582              
 -35.7                0.01161              
 -35.8                0.00746              
 -35.9                0.00736              
 -36.                 0.00981              
 -36.1                0.01239              
 -36.2                0.01233              
 -36.3                0.00934              
 -36.4                0.00755              
 -36.5                0.00794              
 -36.6                0.00640              
 -36.7                0.00561              
 -36.8                0.00969              
 -36.9                0.01433              
 -37.                 0.01296              
 -37.1                0.01006              
 -37.2                0.00877              
 -37.3                0.00827              
 -37.4                0.00737              
 -37.5                0.00636              
 -37.6                0.00540              
 -37.7                0.00413              
 -37.8                0.00199              
 -37.9               -0.00036              
 -38.                 0.00021              
 -38.1                0.00429              
 -38.2                0.00838              
 -38.3                0.01051              
 -38.4                0.01149              
 -38.5                0.01152              
 -38.6                0.01020              
 -38.7                0.00873              
 -38.8                0.00866              
 -38.9                0.00856              
 -39.                 0.00938              
 -39.1                0.01189              
 -39.2                0.01319              
 -39.3                0.01159              
 -39.4                0.00855              
 -39.5                0.00607              
 -39.6                0.00530              
 -39.7                0.00559              
 -39.8                0.00693              
 -39.9                0.00623              
 -40.                 0.00570              
 -40.1                0.00569              
 -40.2                0.00431              
 -40.3                0.00336              
 -40.4                0.00356              
 -40.5                0.00283              
 -40.6                0.00104              
 -40.7                0.00039              
 -40.8                0.00249              
 -40.9                0.00353              
 -41.                 0.00410              
 -41.1                0.00513              
 -41.2                0.00505              
 -41.3                0.00299              
 -41.4               -0.00151              
 -41.5               -0.00342              
 -41.6               -0.00275              
 -41.7               -0.00089              
 -41.8                0.00221              
 -41.9                0.00403              
 -42.                 0.00608              
 -42.1                0.00866              
 -42.2                0.00756              
 -42.3                0.00590              
 -42.4                0.00595              
 -42.5                0.00583              
 -42.6                0.00267              
 -42.7               -0.00108              
 -42.8               -0.00277              
 -42.9               -0.00056              
 -43.                 0.00203              
 -43.1                0.00314              
 -43.2                0.00502              
 -43.3                0.00551              
 -43.4                0.00363              
 -43.5                0.00178              
 -43.6                0.00296              
 -43.7                0.00176              
 -43.8               -0.00075              
 -43.9               -0.00032              
 -44.                 0.00196              
 -44.1                0.00246              
 -44.2                0.00110              
 -44.3                0.00137              
 -44.4                0.00428              
 -44.5                0.00481              
 -44.6               -0.00032              
 -44.7               -0.00304              
 -44.8               -0.00241              
##END=
