##TITLE=              31P MAS NMR spectrum of calcined and rehydrated AlPO-41
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Caldarelli et al. J. Phys. Chem. B, 103, 5477-5487 (1999) Figure 3c
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/15 17:00:32
##SOURCE REFERENCE=   AFO-31P-Caldarelli-1999-hydrated
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              AFO
##NAMES=              AlPO-41
##SAMPLE DESCRIPTION= AlPO-41, calcined, hydrated

$$Bibliographic information 
##$AUTHORS=           Caldarelli, S., Meden, A., Tuel, A.
##$TITLE=             Solid-state nuclear magnetic resonance study of the microporous aluminophosphate AlPO4-41
##$JOURNAL=           Journal of Physical Chemistry B
##$VOLUME=            103
##$PAGES=             5477-5487
##$YEAR=              1999
##$DOI=               10.1021/jp990667b
##$FIGURE=            Figure 3c

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         5
##$PEAK LABELS=        A          C          B          D          E         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -33.8346   -29.753    -28.2773   -25.8997   -23.5134   
##$PEAK AREAS=         1.         1.         1.         1.         1.        
##$PEAK WIDTHS=        3.16257    2.43033    1.95302    1.90135    2.55833   
##$PEAK SHAPES=        0          0          0          0          0         
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 161.2
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     14000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -4.9                  
##LASTX=              -44.9                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            401
##FIRSTY=              0.00309              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -4.9                 0.00309              
 -5.                  0.00093              
 -5.1                 0.00033              
 -5.2                 0.00334              
 -5.3                 0.00639              
 -5.4                 0.00800              
 -5.5                 0.00788              
 -5.6                 0.00673              
 -5.7                 0.00322              
 -5.8                 0.00045              
 -5.9                 0.00002              
 -6.                 -0.00002              
 -6.1                -0.00151              
 -6.2                -0.00298              
 -6.3                -0.00134              
 -6.4                 0.00127              
 -6.5                 0.00068              
 -6.6                -0.00055              
 -6.7                -0.00092              
 -6.8                -0.00102              
 -6.9                -0.00102              
 -7.                 -0.00090              
 -7.1                -0.00047              
 -7.2                 0.00163              
 -7.3                 0.00404              
 -7.4                 0.00463              
 -7.5                 0.00437              
 -7.6                 0.00360              
 -7.7                 0.00315              
 -7.8                 0.00426              
 -7.9                 0.00506              
 -8.                  0.00382              
 -8.1                 0.00344              
 -8.2                 0.00509              
 -8.3                 0.00660              
 -8.4                 0.00761              
 -8.5                 0.00840              
 -8.6                 0.00884              
 -8.7                 0.00888              
 -8.8                 0.00794              
 -8.9                 0.00514              
 -9.                  0.00295              
 -9.1                 0.00300              
 -9.2                 0.00312              
 -9.3                 0.00418              
 -9.4                 0.00547              
 -9.5                 0.00721              
 -9.6                 0.00827              
 -9.7                 0.00723              
 -9.8                 0.00674              
 -9.9                 0.00579              
 -10.                 0.00544              
 -10.1                0.00777              
 -10.2                0.01025              
 -10.3                0.01173              
 -10.4                0.01248              
 -10.5                0.01239              
 -10.6                0.01084              
 -10.7                0.00956              
 -10.8                0.00984              
 -10.9                0.00935              
 -11.                 0.00798              
 -11.1                0.00666              
 -11.2                0.00641              
 -11.3                0.00673              
 -11.4                0.00700              
 -11.5                0.00678              
 -11.6                0.00572              
 -11.7                0.00432              
 -11.8                0.00205              
 -11.9                0.00103              
 -12.                 0.00385              
 -12.1                0.00623              
 -12.2                0.00705              
 -12.3                0.00470              
 -12.4                0.00184              
 -12.5                0.00053              
 -12.6                0.00020              
 -12.7                0.00175              
 -12.8                0.00334              
 -12.9                0.00430              
 -13.                 0.00532              
 -13.1                0.00604              
 -13.2                0.00599              
 -13.3                0.00505              
 -13.4                0.00423              
 -13.5                0.00474              
 -13.6                0.00587              
 -13.7                0.00731              
 -13.8                0.00815              
 -13.9                0.00819              
 -14.                 0.00644              
 -14.1                0.00366              
 -14.2                0.00071              
 -14.3               -0.00067              
 -14.4                0.00173              
 -14.5                0.00462              
 -14.6                0.00445              
 -14.7                0.00347              
 -14.8                0.00369              
 -14.9                0.00500              
 -15.                 0.00606              
 -15.1                0.00670              
 -15.2                0.00751              
 -15.3                0.00854              
 -15.4                0.00930              
 -15.5                0.00884              
 -15.6                0.00782              
 -15.7                0.00738              
 -15.8                0.00772              
 -15.9                0.00747              
 -16.                 0.00659              
 -16.1                0.00677              
 -16.2                0.00697              
 -16.3                0.00622              
 -16.4                0.00473              
 -16.5                0.00230              
 -16.6                0.00023              
 -16.7               -0.00095              
 -16.8               -0.00124              
 -16.9                0.00023              
 -17.                 0.00200              
 -17.1                0.00282              
 -17.2                0.00110              
 -17.3               -0.00017              
 -17.4                0.00037              
 -17.5                0.00226              
 -17.6                0.00295              
 -17.7                0.00261              
 -17.8                0.00386              
 -17.9                0.00483              
 -18.                 0.00400              
 -18.1                0.00229              
 -18.2                0.00024              
 -18.3               -0.00051              
 -18.4               -0.00086              
 -18.5               -0.00101              
 -18.6               -0.00019              
 -18.7                0.00112              
 -18.8                0.00208              
 -18.9                0.00221              
 -19                  0.00199              
 -19.1                0.00214              
 -19.2                0.00501              
 -19.3                0.00784              
 -19.4                0.00667              
 -19.5                0.00458              
 -19.6                0.00331              
 -19.7                0.00267              
 -19.8                0.00284              
 -19.9                0.00435              
 -20.                 0.00620              
 -20.1                0.00835              
 -20.2                0.00922              
 -20.3                0.00828              
 -20.4                0.00762              
 -20.5                0.00813              
 -20.6                0.00972              
 -20.7                0.01333              
 -20.8                0.01721              
 -20.9                0.02092              
 -21.                 0.02391              
 -21.1                0.02695              
 -21.2                0.03203              
 -21.3                0.03637              
 -21.4                0.04219              
 -21.5                0.04950              
 -21.6                0.05809              
 -21.7                0.06904              
 -21.8                0.08022              
 -21.9                0.09082              
 -22.                 0.11026              
 -22.1                0.13409              
 -22.2                0.15946              
 -22.3                0.18218              
 -22.4                0.20753              
 -22.5                0.23425              
 -22.6                0.26374              
 -22.7                0.29189              
 -22.8                0.30834              
 -22.9                0.33177              
 -23.                 0.35369              
 -23.1                0.36697              
 -23.2                0.37620              
 -23.3                0.37628              
 -23.4                0.37663              
 -23.5                0.37368              
 -23.6                0.36937              
 -23.7                0.36328              
 -23.8                0.35489              
 -23.9                0.34332              
 -24.                 0.33284              
 -24.1                0.32570              
 -24.2                0.32013              
 -24.3                0.3184               
 -24.4                0.32080              
 -24.5                0.33149              
 -24.6                0.34128              
 -24.7                0.35828              
 -24.8                0.3792               
 -24.9                0.40734              
 -25.                 0.43739              
 -25.1                0.45584              
 -25.2                0.47435              
 -25.3                0.49291              
 -25.4                0.51017              
 -25.5                0.52494              
 -25.6                0.53174              
 -25.7                0.53728              
 -25.8                0.53446              
 -25.9                0.52800              
 -26.                 0.51685              
 -26.1                0.50305              
 -26.2                0.48544              
 -26.3                0.46584              
 -26.4                0.44455              
 -26.5                0.42642              
 -26.6                0.40968              
 -26.7                0.39195              
 -26.8                0.37896              
 -26.9                0.37051              
 -27.                 0.36658              
 -27.1                0.37039              
 -27.2                0.37846              
 -27.3                0.39472              
 -27.4                0.41103              
 -27.5                0.43276              
 -27.6                0.45714              
 -27.7                0.48687              
 -27.8                0.51976              
 -27.9                0.54396              
 -28.                 0.56074              
 -28.1                0.58580              
 -28.2                0.60946              
 -28.3                0.62784              
 -28.4                0.64414              
 -28.5                0.65324              
 -28.6                0.65832              
 -28.7                0.66065              
 -28.8                0.66014              
 -28.9                0.65555              
 -29.                 0.64282              
 -29.1                0.62672              
 -29.2                0.60704              
 -29.3                0.59010              
 -29.4                0.57312              
 -29.5                0.55209              
 -29.6                0.52908              
 -29.7                0.50452              
 -29.8                0.48206              
 -29.9                0.46300              
 -30.                 0.43804              
 -30.1                0.40912              
 -30.2                0.38894              
 -30.3                0.36878              
 -30.4                0.34898              
 -30.5                0.32785              
 -30.6                0.30568              
 -30.7                0.28806              
 -30.8                0.27408              
 -30.9                0.25555              
 -31.                 0.23721              
 -31.1                0.22267              
 -31.2                0.20950              
 -31.3                0.19676              
 -31.4                0.18439              
 -31.5                0.17684              
 -31.6                0.17093              
 -31.7                0.16581              
 -31.8                0.16059              
 -31.9                0.15660              
 -32.                 0.15421              
 -32.1                0.15336              
 -32.2                0.15468              
 -32.3                0.15787              
 -32.4                0.16410              
 -32.5                0.17044              
 -32.6                0.17857              
 -32.7                0.18693              
 -32.8                0.19835              
 -32.9                0.21199              
 -33.                 0.22441              
 -33.1                0.23486              
 -33.2                0.24861              
 -33.3                0.26145              
 -33.4                0.27259              
 -33.5                0.28314              
 -33.6                0.29078              
 -33.7                0.29915              
 -33.8                0.30420              
 -33.9                0.30670              
 -34.                 0.30541              
 -34.1                0.30188              
 -34.2                0.29561              
 -34.3                0.28126              
 -34.4                0.26648              
 -34.5                0.25352              
 -34.6                0.23806              
 -34.7                0.21990              
 -34.8                0.20122              
 -34.9                0.18488              
 -35.                 0.17084              
 -35.1                0.15124              
 -35.2                0.12982              
 -35.3                0.11300              
 -35.4                0.10059              
 -35.5                0.08879              
 -35.6                0.07706              
 -35.7                0.06561              
 -35.8                0.05553              
 -35.9                0.05095              
 -36.                 0.04428              
 -36.1                0.03802              
 -36.2                0.03442              
 -36.3                0.03098              
 -36.4                0.02679              
 -36.5                0.02143              
 -36.6                0.01804              
 -36.7                0.01685              
 -36.8                0.01811              
 -36.9                0.01816              
 -37.                 0.01583              
 -37.1                0.01311              
 -37.2                0.01167              
 -37.3                0.01170              
 -37.4                0.01239              
 -37.5                0.01245              
 -37.6                0.01164              
 -37.7                0.00929              
 -37.8                0.00668              
 -37.9                0.00451              
 -38.                 0.00225              
 -38.1               -0.00002              
 -38.2               -0.00202              
 -38.3               -0.00195              
 -38.4               -0.00115              
 -38.5               -0.00109              
 -38.6               -0.00173              
 -38.7               -0.00234              
 -38.8               -0.00163              
 -38.9               -0.00099              
 -39.                -0.00022              
 -39.1                0.00222              
 -39.2                0.00447              
 -39.3                0.00403              
 -39.4                0.00214              
 -39.5                0.00054              
 -39.6                0.00032              
 -39.7                0.00085              
 -39.8                0.00143              
 -39.9                0.00155              
 -40.                 0.00232              
 -40.1                0.00287              
 -40.2                0.00136              
 -40.3               -0.00115              
 -40.4               -0.00253              
 -40.5               -0.00269              
 -40.6               -0.00203              
 -40.7               -0.00095              
 -40.8                0.00024              
 -40.9                0.00148              
 -41.                 0.00306              
 -41.1                0.00307              
 -41.2                0.00187              
 -41.3                0.00035              
 -41.4               -0.00091              
 -41.5               -0.00073              
 -41.6                0.00062              
 -41.7                0.00128              
 -41.8                0.00146              
 -41.9                0.00193              
 -42.                 0.00213              
 -42.1                0.00139              
 -42.2                0.00013              
 -42.3               -0.00082              
 -42.4               -0.00089              
 -42.5               -0.00078              
 -42.6               -0.00126              
 -42.7               -0.00094              
 -42.8                0.00105              
 -42.9                0.00274              
 -43.                 0.00216              
 -43.1                0.00035              
 -43.2               -0.00172              
 -43.3               -0.00205              
 -43.4                0.00041              
 -43.5                0.00276              
 -43.6                0.00203              
 -43.7                0.00052              
 -43.8                0.00168              
 -43.9                0.00449              
 -44.                 0.00565              
 -44.1                0.00586              
 -44.2                0.00432              
 -44.3                0.00322              
 -44.4                0.00476              
 -44.5                0.00765              
 -44.6                0.00636              
 -44.7                0.00380              
 -44.8                0.00368              
 -44.9                0.00471              
##END=
