##TITLE=              31P MAS NMR spectrum of as-made AlPO-52
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             McGuire et al. Zeolites, 15, 460-469 (1995) Figure 7d
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/16 11:47:47
##SOURCE REFERENCE=   AFT-31P-McGuire-1995-asmade
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              AFT
##NAMES=              AlPO-52
##SAMPLE DESCRIPTION= AlPO-52, as-made

$$Bibliographic information 
##$AUTHORS=           McGuire, N.K., Bateman, C.A., Scott Blackwell, C., Wilson, S.T., Kirchner, R.M.
##$TITLE=             Structure refinement, electron microscopy, and solid-state magic angle spinning nuclear magnetic resonance characterization of AlPO4-52: An aluminophosphate with a large cage
##$JOURNAL=           Zeolites
##$VOLUME=            15
##$PAGES=             460-469
##$YEAR=              1995
##$DOI=               10.1016/0144-2449(94)00040-Y
##$FIGURE=            Figure 7d

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         3
##$PEAK LABELS=        A          B          C         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -29.2828   -26.5442   -25.0868   
##$PEAK AREAS=         1.         1.         1.        
##$PEAK WIDTHS=        1.94044    2.06241    1.73126   
##$PEAK SHAPES=        0.62479    0.62479    0.62479   
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 161.9
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     15000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              10.3                 
##LASTX=              -46.5                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            569
##FIRSTY=             -0.01276              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  10.3               -0.01276              
  10.2               -0.01237              
  10.1               -0.01241              
  10.                -0.01249              
  9.9                -0.01318              
  9.8                -0.01321              
  9.7                -0.01322              
  9.6                -0.01305              
  9.5                -0.01379              
  9.4                -0.01494              
  9.3                -0.01459              
  9.2                -0.01396              
  9.1                -0.01462              
  9.                 -0.01478              
  8.9                -0.01470              
  8.8                -0.01473              
  8.7                -0.01472              
  8.6                -0.01472              
  8.5                -0.01472              
  8.4                -0.01471              
  8.3                -0.01482              
  8.2                -0.01416              
  8.1                -0.01424              
  8.                 -0.01483              
  7.9                -0.01469              
  7.8                -0.01473              
  7.7                -0.01477              
  7.6                -0.01403              
  7.5                -0.01438              
  7.4                -0.01490              
  7.3                -0.01443              
  7.2                -0.01389              
  7.1                -0.01397              
  7.                 -0.01396              
  6.9                -0.01396              
  6.8                -0.01396              
  6.7                -0.01396              
  6.6                -0.01395              
  6.5                -0.01397              
  6.4                -0.01394              
  6.3                -0.01395              
  6.2                -0.01461              
  6.1                -0.01485              
  6.                 -0.01427              
  5.9                -0.01388              
  5.8                -0.01398              
  5.7                -0.01395              
  5.6                -0.01396              
  5.5                -0.01396              
  5.4                -0.01396              
  5.3                -0.01396              
  5.2                -0.01394              
  5.1                -0.01401              
  5.                 -0.01385              
  4.9                -0.01319              
  4.8                -0.01322              
  4.7                -0.01261              
  4.6                -0.01236              
  4.5                -0.01245              
  4.4                -0.01242              
  4.3                -0.01243              
  4.2                -0.01243              
  4.1                -0.01243              
  4.                 -0.01244              
  3.9                -0.01239              
  3.8                -0.01258              
  3.7                -0.01191              
  3.6                -0.01076              
  3.5                -0.01092              
  3.4                -0.01091              
  3.3                -0.01090              
  3.2                -0.01091              
  3.1                -0.01088              
  3.                 -0.01097              
  2.9                -0.01074              
  2.8                -0.01010              
  2.7                -0.01014              
  2.6                -0.01015              
  2.5                -0.01014              
  2.4                -0.01015              
  2.3                -0.01012              
  2.2                -0.01019              
  2.1                -0.01006              
  2.                 -0.00938              
  1.9                -0.00936              
  1.8                -0.00935              
  1.7                -0.00954              
  1.6                -0.00871              
  1.5                -0.00770              
  1.4                -0.00787              
  1.3                -0.00786              
  1.2                -0.00793              
  1.1                -0.00665              
  1.                 -0.00620              
  0.9                -0.00634              
  0.8                -0.00637              
  0.7                -0.00619              
  0.6                -0.00554              
  0.5                -0.00558              
  0.4                -0.00496              
  0.3                -0.00469              
  0.2                -0.00498              
  0.1                -0.00425              
 -0.00000            -0.00317              
 -0.1                -0.00324              
 -0.2                -0.00253              
 -0.3                -0.00253              
 -0.4                -0.00200              
 -0.5                -0.00162              
 -0.6                -0.00190              
 -0.7                -0.00139              
 -0.8                -0.00014              
 -0.9                -0.00022              
 -1.                  0.00043              
 -1.1                 0.00060              
 -1.2                 0.00050              
 -1.3                 0.00061              
 -1.4                 0.00035              
 -1.5                -0.00027              
 -1.6                -0.00021              
 -1.7                -0.00021              
 -1.8                -0.00022              
 -1.9                -0.00021              
 -2.                 -0.00021              
 -2.1                -0.00022              
 -2.2                -0.00021              
 -2.3                -0.00022              
 -2.4                -0.00025              
 -2.5                 0.00030              
 -2.6                 0.00109              
 -2.7                 0.00136              
 -2.8                 0.00128              
 -2.9                 0.00132              
 -3.                  0.00129              
 -3.1                 0.00127              
 -3.2                 0.00192              
 -3.3                 0.00215              
 -3.4                 0.00197              
 -3.5                 0.00232              
 -3.6                 0.00292              
 -3.7                 0.00280              
 -3.8                 0.00278              
 -3.9                 0.00412              
 -4.                  0.00445              
 -4.1                 0.00436              
 -4.2                 0.00424              
 -4.3                 0.00470              
 -4.4                 0.00596              
 -4.5                 0.00588              
 -4.6                 0.00653              
 -4.7                 0.00673              
 -4.8                 0.00653              
 -4.9                 0.00700              
 -5.                  0.00739              
 -5.1                 0.00757              
 -5.2                 0.00894              
 -5.3                 0.00897              
 -5.4                 0.00896              
 -5.5                 0.00878              
 -5.6                 0.00962              
 -5.7                 0.01057              
 -5.8                 0.01054              
 -5.9                 0.01124              
 -6.                  0.01121              
 -6.1                 0.01181              
 -6.2                 0.01208              
 -6.3                 0.01192              
 -6.4                 0.01218              
 -6.5                 0.01294              
 -6.6                 0.01354              
 -6.7                 0.01354              
 -6.8                 0.01345              
 -6.9                 0.01403              
 -7.                  0.01438              
 -7.1                 0.01420              
 -7.2                 0.01443              
 -7.3                 0.01509              
 -7.4                 0.01507              
 -7.5                 0.01491              
 -7.6                 0.01612              
 -7.7                 0.01671              
 -7.8                 0.01657              
 -7.9                 0.01650              
 -8.                  0.01670              
 -8.1                 0.01808              
 -8.2                 0.01815              
 -8.3                 0.01810              
 -8.4                 0.01803              
 -8.5                 0.01843              
 -8.6                 0.01890              
 -8.7                 0.01893              
 -8.8                 0.01963              
 -8.9                 0.01966              
 -9.                  0.01956              
 -9.1                 0.02001              
 -9.2                 0.02081              
 -9.3                 0.02121              
 -9.4                 0.02115              
 -9.5                 0.02115              
 -9.6                 0.02113              
 -9.7                 0.02168              
 -9.8                 0.02246              
 -9.9                 0.02276              
 -10.                 0.02261              
 -10.1                0.02281              
 -10.2                0.02347              
 -10.3                0.02347              
 -10.4                0.02337              
 -10.5                0.02396              
 -10.6                0.02430              
 -10.7                0.02415              
 -10.8                0.02432              
 -10.9                0.02506              
 -11.                 0.02572              
 -11.1                0.02575              
 -11.2                0.02577              
 -11.3                0.02558              
 -11.4                0.02631              
 -11.5                0.02742              
 -11.6                0.02724              
 -11.7                0.02726              
 -11.8                0.02728              
 -11.9                0.02718              
 -12.                 0.02770              
 -12.1                0.02811              
 -12.2                0.02801              
 -12.3                0.02803              
 -12.4                0.02803              
 -12.5                0.02802              
 -12.6                0.02805              
 -12.7                0.02795              
 -12.8                0.02836              
 -12.9                0.02887              
 -13.                 0.02878              
 -13.1                0.02879              
 -13.2                0.02879              
 -13.3                0.02879              
 -13.4                0.02880              
 -13.5                0.02875              
 -13.6                0.02890              
 -13.7                0.02854              
 -13.8                0.02721              
 -13.9                0.02724              
 -14.                 0.02730              
 -14.1                0.02717              
 -14.2                0.02766              
 -14.3                0.02809              
 -14.4                0.02805              
 -14.5                0.02798              
 -14.6                0.02729              
 -14.7                0.02723              
 -14.8                0.02728              
 -14.9                0.02726              
 -15.                 0.02726              
 -15.1                0.02728              
 -15.2                0.02725              
 -15.3                0.02725              
 -15.4                0.02793              
 -15.5                0.02807              
 -15.6                0.02803              
 -15.7                0.02797              
 -15.8                0.02822              
 -15.9                0.02885              
 -16.                 0.02879              
 -16.1                0.02879              
 -16.2                0.02880              
 -16.3                0.02879              
 -16.4                0.02881              
 -16.5                0.02874              
 -16.6                0.02890              
 -16.7                0.02957              
 -16.8                0.02957              
 -16.9                0.02954              
 -17.                 0.02956              
 -17.1                0.02955              
 -17.2                0.02957              
 -17.3                0.02952              
 -17.4                0.02959              
 -17.5                0.03028              
 -17.6                0.03035              
 -17.7                0.03032              
 -17.8                0.03027              
 -17.9                0.03052              
 -18                  0.03129              
 -18.1                0.03188              
 -18.2                0.03186              
 -18.3                0.03171              
 -18.4                0.03294              
 -18.5                0.03345              
 -18.6                0.03359              
 -18.7                0.03431              
 -18.8                0.03506              
 -18.9                0.03641              
 -19.                 0.03694              
 -19.1                0.03930              
 -19.2                0.04146              
 -19.3                0.04413              
 -19.4                0.04706              
 -19.5                0.04914              
 -19.6                0.05325              
 -19.7                0.05724              
 -19.8                0.06096              
 -19.9                0.06620              
 -20.                 0.07264              
 -20.1                0.07751              
 -20.2                0.08064              
 -20.3                0.08469              
 -20.4                0.08808              
 -20.5                0.08918              
 -20.6                0.08858              
 -20.7                0.08836              
 -20.8                0.08608              
 -20.9                0.08131              
 -21.                 0.07820              
 -21.1                0.07425              
 -21.2                0.06929              
 -21.3                0.06259              
 -21.4                0.05779              
 -21.5                0.05513              
 -21.6                0.05122              
 -21.7                0.04680              
 -21.8                0.04494              
 -21.9                0.04238              
 -22.                 0.04006              
 -22.1                0.03892              
 -22.2                0.03870              
 -22.3                0.03869              
 -22.4                0.03877              
 -22.5                0.03946              
 -22.6                0.04008              
 -22.7                0.04129              
 -22.8                0.04271              
 -22.9                0.04617              
 -23.                 0.04902              
 -23.1                0.05098              
 -23.2                0.05784              
 -23.3                0.06207              
 -23.4                0.07247              
 -23.5                0.08216              
 -23.6                0.09135              
 -23.7                0.10564              
 -23.8                0.12805              
 -23.9                0.15652              
 -24.                 0.17939              
 -24.1                0.20775              
 -24.2                0.25233              
 -24.3                0.28635              
 -24.4                0.31893              
 -24.5                0.37372              
 -24.6                0.42479              
 -24.7                0.45684              
 -24.8                0.49933              
 -24.9                0.51731              
 -25.                 0.52740              
 -25.1                0.54178              
 -25.2                0.54841              
 -25.3                0.55041              
 -25.4                0.54973              
 -25.5                0.54519              
 -25.6                0.54174              
 -25.7                0.53709              
 -25.8                0.53047              
 -25.9                0.52400              
 -26.                 0.51726              
 -26.1                0.51073              
 -26.2                0.50722              
 -26.3                0.49730              
 -26.4                0.48647              
 -26.5                0.47877              
 -26.6                0.46798              
 -26.7                0.44890              
 -26.8                0.42831              
 -26.9                0.41556              
 -27.                 0.39206              
 -27.1                0.37047              
 -27.2                0.34813              
 -27.3                0.32611              
 -27.4                0.31248              
 -27.5                0.29773              
 -27.6                0.28182              
 -27.7                0.26876              
 -27.8                0.25807              
 -27.9                0.25293              
 -28.                 0.25248              
 -28.1                0.25261              
 -28.2                0.25885              
 -28.3                0.27594              
 -28.4                0.28056              
 -28.5                0.29730              
 -28.6                0.33852              
 -28.7                0.36564              
 -28.8                0.37577              
 -28.9                0.40129              
 -29.                 0.41256              
 -29.1                0.41583              
 -29.2                0.41429              
 -29.3                0.40691              
 -29.4                0.40127              
 -29.5                0.39248              
 -29.6                0.37302              
 -29.7                0.35517              
 -29.8                0.32885              
 -29.9                0.30968              
 -30.                 0.29317              
 -30.1                0.26741              
 -30.2                0.23852              
 -30.3                0.21607              
 -30.4                0.19435              
 -30.5                0.17113              
 -30.6                0.14425              
 -30.7                0.13118              
 -30.8                0.11691              
 -30.9                0.09815              
 -31.                 0.08537              
 -31.1                0.06868              
 -31.2                0.05729              
 -31.3                0.05003              
 -31.4                0.04138              
 -31.5                0.03260              
 -31.6                0.02709              
 -31.7                0.02312              
 -31.8                0.01774              
 -31.9                0.01377              
 -32.                 0.01173              
 -32.1                0.00929              
 -32.2                0.00687              
 -32.3                0.00528              
 -32.4                0.00403              
 -32.5                0.00268              
 -32.6                0.00136              
 -32.7                0.00066              
 -32.8                0.00004              
 -32.9               -0.00065              
 -33.                -0.00122              
 -33.1               -0.00209              
 -33.2               -0.00342              
 -33.3               -0.00403              
 -33.4               -0.00400              
 -33.5               -0.00450              
 -33.6               -0.00533              
 -33.7               -0.00554              
 -33.8               -0.00575              
 -33.9               -0.00636              
 -34.                -0.00632              
 -34.1               -0.00700              
 -34.2               -0.00716              
 -34.3               -0.00698              
 -34.4               -0.00745              
 -34.5               -0.00788              
 -34.6               -0.00794              
 -34.7               -0.00863              
 -34.8               -0.00864              
 -34.9               -0.00853              
 -35.                -0.00910              
 -35.1               -0.00947              
 -35.2               -0.00930              
 -35.3               -0.00951              
 -35.4               -0.01017              
 -35.5               -0.01015              
 -35.6               -0.01015              
 -35.7               -0.01006              
 -35.8               -0.01052              
 -35.9               -0.01101              
 -36.                -0.01084              
 -36.1               -0.01097              
 -36.2               -0.01167              
 -36.3               -0.01099              
 -36.4               -0.01137              
 -36.5               -0.01177              
 -36.6               -0.01163              
 -36.7               -0.01170              
 -36.8               -0.01163              
 -36.9               -0.01165              
 -37.                -0.01300              
 -37.1               -0.01329              
 -37.2               -0.01316              
 -37.3               -0.01321              
 -37.4               -0.01319              
 -37.5               -0.01319              
 -37.6               -0.01319              
 -37.7               -0.01319              
 -37.8               -0.01320              
 -37.9               -0.01319              
 -38.                -0.01321              
 -38.1               -0.01314              
 -38.2               -0.01330              
 -38.3               -0.01397              
 -38.4               -0.01396              
 -38.5               -0.01402              
 -38.6               -0.01347              
 -38.7               -0.01313              
 -38.8               -0.01316              
 -38.9               -0.01332              
 -39.                -0.01399              
 -39.1               -0.01397              
 -39.2               -0.01395              
 -39.3               -0.01394              
 -39.4               -0.01403              
 -39.5               -0.01371              
 -39.6               -0.01309              
 -39.7               -0.01325              
 -39.8               -0.01393              
 -39.9               -0.01399              
 -40.                -0.01395              
 -40.1               -0.01396              
 -40.2               -0.01397              
 -40.3               -0.01392              
 -40.4               -0.01403              
 -40.5               -0.01471              
 -40.6               -0.01475              
 -40.7               -0.01470              
 -40.8               -0.01477              
 -40.9               -0.01458              
 -41.                -0.01511              
 -41.1               -0.01636              
 -41.2               -0.01625              
 -41.3               -0.01624              
 -41.4               -0.01626              
 -41.5               -0.01625              
 -41.6               -0.01625              
 -41.7               -0.01625              
 -41.8               -0.01625              
 -41.9               -0.01625              
 -42.                -0.01625              
 -42.1               -0.01625              
 -42.2               -0.01625              
 -42.3               -0.01625              
 -42.4               -0.01625              
 -42.5               -0.01625              
 -42.6               -0.01625              
 -42.7               -0.01625              
 -42.8               -0.01625              
 -42.9               -0.01625              
 -43.                -0.01625              
 -43.1               -0.01625              
 -43.2               -0.01625              
 -43.3               -0.01625              
 -43.4               -0.01625              
 -43.5               -0.01625              
 -43.6               -0.01625              
 -43.7               -0.01625              
 -43.8               -0.01625              
 -43.9               -0.01625              
 -44.                -0.01625              
 -44.1               -0.01625              
 -44.2               -0.01624              
 -44.3               -0.01628              
 -44.4               -0.01615              
 -44.5               -0.01663              
 -44.6               -0.01690              
 -44.7               -0.01618              
 -44.8               -0.01625              
 -44.9               -0.01626              
 -45.                -0.01624              
 -45.1               -0.01625              
 -45.2               -0.01625              
 -45.3               -0.01625              
 -45.4               -0.01625              
 -45.5               -0.01625              
 -45.6               -0.01625              
 -45.7               -0.01627              
 -45.8               -0.01617              
 -45.9               -0.01662              
 -46.                -0.01708              
 -46.1               -0.01703              
 -46.2               -0.01698              
 -46.3               -0.01629              
 -46.4               -0.01621              
 -46.5               -0.01627              
##END=
