##TITLE=              31P MAS NMR spectrum of calcined AlPO-52
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             McGuire et al. Zeolites, 15, 460-469 (1995) Figure 7e
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/16 11:53:00
##SOURCE REFERENCE=   AFT-31P-McGuire-1995-calcined
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              AFT
##NAMES=              AlPO-52
##SAMPLE DESCRIPTION= AlPO-52, calcined

$$Bibliographic information 
##$AUTHORS=           McGuire, N.K., Bateman, C.A., Scott Blackwell, C., Wilson, S.T., Kirchner, R.M.
##$TITLE=             Structure refinement, electron microscopy, and solid-state magic angle spinning nuclear magnetic resonance characterization of AlPO4-52: An aluminophosphate with a large cage
##$JOURNAL=           Zeolites
##$VOLUME=            15
##$PAGES=             460-469
##$YEAR=              1995
##$DOI=               10.1016/0144-2449(94)00040-Y
##$FIGURE=            Figure 7e

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         3
##$PEAK LABELS=        A          B          C         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -30.2167   -29.2933   -28.9918   
##$PEAK AREAS=         1.         1.         1.        
##$PEAK WIDTHS=        1.54873    1.54873    1.54873   
##$PEAK SHAPES=        0.32211    0.32211    0.32211   
##$NUMBERING REF=     McGuire et al. Zeolites, 15, 460-469 (1995)
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 161.9
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     15000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              10.8                 
##LASTX=              -48.8                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            597
##FIRSTY=              0.00269              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  10.8                0.00269              
  10.7                0.00269              
  10.6                0.00269              
  10.5                0.00269              
  10.4                0.00269              
  10.3                0.00269              
  10.2                0.00269              
  10.1                0.00269              
  10.                 0.00269              
  9.9                 0.00269              
  9.8                 0.00269              
  9.7                 0.00269              
  9.6                 0.00269              
  9.5                 0.00269              
  9.4                 0.00269              
  9.3                 0.00269              
  9.2                 0.00269              
  9.1                 0.00269              
  9.                  0.00269              
  8.9                 0.00269              
  8.8                 0.00269              
  8.7                 0.00269              
  8.6                 0.00269              
  8.5                 0.00269              
  8.4                 0.00269              
  8.3                 0.00269              
  8.2                 0.00269              
  8.1                 0.00269              
  8.                  0.00269              
  7.9                 0.00269              
  7.8                 0.00269              
  7.7                 0.00269              
  7.6                 0.00269              
  7.5                 0.00269              
  7.4                 0.00269              
  7.3                 0.00269              
  7.2                 0.00269              
  7.1                 0.00269              
  7.                  0.00269              
  6.9                 0.00269              
  6.8                 0.00269              
  6.7                 0.00269              
  6.6                 0.00269              
  6.5                 0.00269              
  6.4                 0.00269              
  6.3                 0.00269              
  6.2                 0.00269              
  6.1                 0.00269              
  6.                  0.00269              
  5.9                 0.00269              
  5.8                 0.00269              
  5.7                 0.00269              
  5.6                 0.00269              
  5.5                 0.00269              
  5.4                 0.00269              
  5.3                 0.00269              
  5.2                 0.00269              
  5.1                 0.00269              
  5.                  0.00269              
  4.9                 0.00269              
  4.8                 0.00269              
  4.7                 0.00269              
  4.6                 0.00269              
  4.5                 0.00269              
  4.4                 0.00269              
  4.3                 0.00269              
  4.2                 0.00269              
  4.1                 0.00269              
  4.                  0.00269              
  3.9                 0.00269              
  3.8                 0.00269              
  3.7                 0.00269              
  3.6                 0.00269              
  3.5                 0.00269              
  3.4                 0.00269              
  3.3                 0.00269              
  3.2                 0.00269              
  3.1                 0.00269              
  3.                  0.00269              
  2.9                 0.00269              
  2.8                 0.00269              
  2.7                 0.00269              
  2.6                 0.00269              
  2.5                 0.00269              
  2.4                 0.00269              
  2.3                 0.00269              
  2.2                 0.00269              
  2.1                 0.00269              
  2.                  0.00269              
  1.9                 0.00269              
  1.8                 0.00269              
  1.7                 0.00269              
  1.6                 0.00269              
  1.5                 0.00269              
  1.4                 0.00269              
  1.3                 0.00269              
  1.2                 0.00269              
  1.1                 0.00269              
  1.                  0.00269              
  0.9                 0.00269              
  0.8                 0.00269              
  0.7                 0.00269              
  0.6                 0.00269              
  0.5                 0.00269              
  0.4                 0.00269              
  0.3                 0.00269              
  0.2                 0.00269              
  0.1                 0.00269              
 -0.00000             0.00269              
 -0.1                 0.00269              
 -0.2                 0.00269              
 -0.3                 0.00269              
 -0.4                 0.00269              
 -0.5                 0.00269              
 -0.6                 0.00269              
 -0.7                 0.00269              
 -0.8                 0.00269              
 -0.9                 0.00269              
 -1.                  0.00269              
 -1.1                 0.00269              
 -1.2                 0.00269              
 -1.3                 0.00269              
 -1.4                 0.00269              
 -1.5                 0.00269              
 -1.6                 0.00269              
 -1.7                 0.00269              
 -1.8                 0.00269              
 -1.9                 0.00269              
 -2.                  0.00269              
 -2.1                 0.00269              
 -2.2                 0.00269              
 -2.3                 0.00269              
 -2.4                 0.00269              
 -2.5                 0.00269              
 -2.6                 0.00269              
 -2.7                 0.00269              
 -2.8                 0.00269              
 -2.9                 0.00269              
 -3.                  0.00269              
 -3.1                 0.00269              
 -3.2                 0.00269              
 -3.3                 0.00269              
 -3.4                 0.00269              
 -3.5                 0.00269              
 -3.6                 0.00269              
 -3.7                 0.00269              
 -3.8                 0.00269              
 -3.9                 0.00269              
 -4.                  0.00269              
 -4.1                 0.00269              
 -4.2                 0.00269              
 -4.3                 0.00269              
 -4.4                 0.00269              
 -4.5                 0.00269              
 -4.6                 0.00268              
 -4.7                 0.00274              
 -4.8                 0.00252              
 -4.9                 0.00323              
 -5.                  0.00454              
 -5.1                 0.00438              
 -5.2                 0.00438              
 -5.3                 0.00440              
 -5.4                 0.00439              
 -5.5                 0.00439              
 -5.6                 0.00439              
 -5.7                 0.00439              
 -5.8                 0.00439              
 -5.9                 0.00439              
 -6.                  0.00439              
 -6.1                 0.00439              
 -6.2                 0.00439              
 -6.3                 0.00439              
 -6.4                 0.00439              
 -6.5                 0.00439              
 -6.6                 0.00439              
 -6.7                 0.00438              
 -6.8                 0.00445              
 -6.9                 0.00418              
 -7.                  0.00503              
 -7.1                 0.00599              
 -7.2                 0.00431              
 -7.3                 0.00425              
 -7.4                 0.00593              
 -7.5                 0.00517              
 -7.6                 0.00401              
 -7.7                 0.00498              
 -7.8                 0.00622              
 -7.9                 0.00608              
 -8.                  0.00609              
 -8.1                 0.00610              
 -8.2                 0.00609              
 -8.3                 0.00609              
 -8.4                 0.00609              
 -8.5                 0.00609              
 -8.6                 0.00609              
 -8.7                 0.00609              
 -8.8                 0.00609              
 -8.9                 0.00609              
 -9.                  0.00609              
 -9.1                 0.00609              
 -9.2                 0.00609              
 -9.3                 0.00609              
 -9.4                 0.00609              
 -9.5                 0.00609              
 -9.6                 0.00609              
 -9.7                 0.00609              
 -9.8                 0.00609              
 -9.9                 0.00609              
 -10.                 0.00609              
 -10.1                0.00609              
 -10.2                0.00614              
 -10.3                0.00591              
 -10.4                0.00688              
 -10.5                0.00798              
 -10.6                0.00776              
 -10.7                0.00780              
 -10.8                0.00780              
 -10.9                0.00779              
 -11.                 0.00780              
 -11.1                0.00778              
 -11.2                0.00783              
 -11.3                0.00773              
 -11.4                0.00784              
 -11.5                0.00936              
 -11.6                0.00959              
 -11.7                0.00946              
 -11.8                0.00951              
 -11.9                0.00949              
 -12.                 0.00950              
 -12.1                0.00950              
 -12.2                0.00950              
 -12.3                0.00950              
 -12.4                0.00950              
 -12.5                0.00950              
 -12.6                0.00950              
 -12.7                0.00950              
 -12.8                0.00950              
 -12.9                0.00950              
 -13.                 0.00950              
 -13.1                0.00950              
 -13.2                0.00950              
 -13.3                0.00950              
 -13.4                0.00950              
 -13.5                0.00950              
 -13.6                0.00949              
 -13.7                0.00954              
 -13.8                0.00931              
 -13.9                0.01026              
 -14.                 0.01138              
 -14.1                0.01116              
 -14.2                0.01120              
 -14.3                0.01121              
 -14.4                0.01115              
 -14.5                0.01138              
 -14.6                0.01044              
 -14.7                0.00932              
 -14.8                0.00953              
 -14.9                0.00949              
 -15.                 0.00950              
 -15.1                0.00949              
 -15.2                0.00954              
 -15.3                0.00934              
 -15.4                0.00997              
 -15.5                0.01133              
 -15.6                0.01119              
 -15.7                0.01118              
 -15.8                0.01125              
 -15.9                0.01101              
 -16.                 0.01195              
 -16.1                0.01308              
 -16.2                0.01286              
 -16.3                0.01290              
 -16.4                0.01290              
 -16.5                0.01290              
 -16.6                0.01289              
 -16.7                0.01294              
 -16.8                0.01278              
 -16.9                0.01313              
 -17.                 0.01461              
 -17.1                0.01454              
 -17.2                0.01587              
 -17.3                0.01647              
 -17.4                0.01623              
 -17.5                0.01638              
 -17.6                0.01619              
 -17.7                0.01634              
 -17.8                0.01937              
 -17.9                0.01991              
 -18                  0.01961              
 -18.1                0.01977              
 -18.2                0.01959              
 -18.3                0.01991              
 -18.4                0.02141              
 -18.5                0.02161              
 -18.6                0.02161              
 -18.7                0.02149              
 -18.8                0.02120              
 -18.9                0.02188              
 -19.                 0.02322              
 -19.1                0.02311              
 -19.2                0.02316              
 -19.3                0.02277              
 -19.4                0.02514              
 -19.5                0.02686              
 -19.6                0.02645              
 -19.7                0.02648              
 -19.8                0.02652              
 -19.9                0.02802              
 -20.                 0.02838              
 -20.1                0.02793              
 -20.2                0.02914              
 -20.3                0.02954              
 -20.4                0.02825              
 -20.5                0.02992              
 -20.6                0.03001              
 -20.7                0.02969              
 -20.8                0.03099              
 -20.9                0.03162              
 -21.                 0.03207              
 -21.1                0.03335              
 -21.2                0.03333              
 -21.3                0.03634              
 -21.4                0.03694              
 -21.5                0.03664              
 -21.6                0.03674              
 -21.7                0.03674              
 -21.8                0.03667              
 -21.9                0.03672              
 -22.                 0.03823              
 -22.1                0.03857              
 -22.2                0.03820              
 -22.3                0.03914              
 -22.4                0.04032              
 -22.5                0.04006              
 -22.6                0.04012              
 -22.7                0.04151              
 -22.8                0.04323              
 -22.9                0.04351              
 -23.                 0.04403              
 -23.1                0.04587              
 -23.2                0.04697              
 -23.3                0.04693              
 -23.4                0.04842              
 -23.5                0.04879              
 -23.6                0.04841              
 -23.7                0.04932              
 -23.8                0.05056              
 -23.9                0.05021              
 -24.                 0.05032              
 -24.1                0.05334              
 -24.2                0.05398              
 -24.3                0.05352              
 -24.4                0.05431              
 -24.5                0.05602              
 -24.6                0.05724              
 -24.7                0.05714              
 -24.8                0.05701              
 -24.9                0.05839              
 -25.                 0.05904              
 -25.1                0.05865              
 -25.2                0.05925              
 -25.3                0.06068              
 -25.4                0.06055              
 -25.5                0.06028              
 -25.6                0.06304              
 -25.7                0.06429              
 -25.8                0.06374              
 -25.9                0.06427              
 -26.                 0.06594              
 -26.1                0.06734              
 -26.2                0.06720              
 -26.3                0.06948              
 -26.4                0.07295              
 -26.5                0.07472              
 -26.6                0.07702              
 -26.7                0.08154              
 -26.8                0.08432              
 -26.9                0.08711              
 -27.                 0.09162              
 -27.1                0.09971              
 -27.2                0.10941              
 -27.3                0.12067              
 -27.4                0.13625              
 -27.5                0.15703              
 -27.6                0.1867               
 -27.7                0.22405              
 -27.8                0.26132              
 -27.9                0.30867              
 -28.                 0.37216              
 -28.1                0.42947              
 -28.2                0.46468              
 -28.3                0.52464              
 -28.4                0.66010              
 -28.5                0.71651              
 -28.6                0.81444              
 -28.7                0.98742              
 -28.8                1.07605              
 -28.9                1.15785              
 -29.                 1.21051              
 -29.1                1.24146              
 -29.2                1.26267              
 -29.3                1.27448              
 -29.4                1.2739               
 -29.5                1.26111              
 -29.6                1.23244              
 -29.7                1.18396              
 -29.8                1.15951              
 -29.9                1.10915              
 -30.                 1.04774              
 -30.1                0.98089              
 -30.2                0.89838              
 -30.3                0.85775              
 -30.4                0.77931              
 -30.5                0.71194              
 -30.6                0.64644              
 -30.7                0.57260              
 -30.8                0.51043              
 -30.9                0.44606              
 -31.                 0.35890              
 -31.1                0.31713              
 -31.2                0.27695              
 -31.3                0.23169              
 -31.4                0.19344              
 -31.5                0.16287              
 -31.6                0.13952              
 -31.7                0.12230              
 -31.8                0.11006              
 -31.9                0.09540              
 -32.                 0.08805              
 -32.1                0.08242              
 -32.2                0.07392              
 -32.3                0.07040              
 -32.4                0.06747              
 -32.5                0.06440              
 -32.6                0.06286              
 -32.7                0.06050              
 -32.8                0.05781              
 -32.9                0.05719              
 -33.                 0.05696              
 -33.1                0.05390              
 -33.2                0.05066              
 -33.3                0.05034              
 -33.4                0.04949              
 -33.5                0.04840              
 -33.6                0.04875              
 -33.7                0.04852              
 -33.8                0.04700              
 -33.9                0.04555              
 -34.                 0.04395              
 -34.1                0.04336              
 -34.2                0.04367              
 -34.3                0.04325              
 -34.4                0.04161              
 -34.5                0.04016              
 -34.6                0.04004              
 -34.7                0.04033              
 -34.8                0.03922              
 -34.9                0.03820              
 -35.                 0.03856              
 -35.1                0.03829              
 -35.2                0.03677              
 -35.3                0.03668              
 -35.4                0.03666              
 -35.5                0.03706              
 -35.6                0.03549              
 -35.7                0.03299              
 -35.8                0.03337              
 -35.9                0.03333              
 -36.                 0.03331              
 -36.1                0.03333              
 -36.2                0.03328              
 -36.3                0.03342              
 -36.4                0.03306              
 -36.5                0.03141              
 -36.6                0.02996              
 -36.7                0.02988              
 -36.8                0.02989              
 -36.9                0.03008              
 -37.                 0.02931              
 -37.1                0.02805              
 -37.2                0.02824              
 -37.3                0.02822              
 -37.4                0.02822              
 -37.5                0.02817              
 -37.6                0.02839              
 -37.7                0.02761              
 -37.8                0.02635              
 -37.9                0.02653              
 -38.                 0.02652              
 -38.1                0.02651              
 -38.2                0.02648              
 -38.3                0.02664              
 -38.4                0.02605              
 -38.5                0.02432              
 -38.6                0.02305              
 -38.7                0.02310              
 -38.8                0.02312              
 -38.9                0.02312              
 -39.                 0.02306              
 -39.1                0.02324              
 -39.2                0.02278              
 -39.3                0.02133              
 -39.4                0.02139              
 -39.5                0.02143              
 -39.6                0.02140              
 -39.7                0.02141              
 -39.8                0.02140              
 -39.9                0.02141              
 -40.                 0.02140              
 -40.1                0.02139              
 -40.2                0.02156              
 -40.3                0.02025              
 -40.4                0.01954              
 -40.5                0.01976              
 -40.6                0.01969              
 -40.7                0.01971              
 -40.8                0.01971              
 -40.9                0.01968              
 -41.                 0.01980              
 -41.1                0.01914              
 -41.2                0.01679              
 -41.3                0.01401              
 -41.4                0.01286              
 -41.5                0.01289              
 -41.6                0.01291              
 -41.7                0.01289              
 -41.8                0.01290              
 -41.9                0.01290              
 -42.                 0.01290              
 -42.1                0.01290              
 -42.2                0.01290              
 -42.3                0.01290              
 -42.4                0.01291              
 -42.5                0.01285              
 -42.6                0.01303              
 -42.7                0.01259              
 -42.8                0.01113              
 -42.9                0.01118              
 -43.                 0.01122              
 -43.1                0.01119              
 -43.2                0.01120              
 -43.3                0.01120              
 -43.4                0.01120              
 -43.5                0.01120              
 -43.6                0.01120              
 -43.7                0.01120              
 -43.8                0.01120              
 -43.9                0.01120              
 -44.                 0.01120              
 -44.1                0.01120              
 -44.2                0.01120              
 -44.3                0.01120              
 -44.4                0.01115              
 -44.5                0.01143              
 -44.6                0.01018              
 -44.7                0.00988              
 -44.8                0.01137              
 -44.9                0.01120              
 -45.                 0.01126              
 -45.1                0.00982              
 -45.2                0.00936              
 -45.3                0.00954              
 -45.4                0.00948              
 -45.5                0.00950              
 -45.6                0.00950              
 -45.7                0.00950              
 -45.8                0.00950              
 -45.9                0.00950              
 -46.                 0.00950              
 -46.1                0.00950              
 -46.2                0.00950              
 -46.3                0.00950              
 -46.4                0.00949              
 -46.5                0.00951              
 -46.6                0.00945              
 -46.7                0.00965              
 -46.8                0.00899              
 -46.9                0.00756              
 -47.                 0.00790              
 -47.1                0.00947              
 -47.2                0.00825              
 -47.3                0.00739              
 -47.4                0.00885              
 -47.5                0.00912              
 -47.6                0.00761              
 -47.7                0.00781              
 -47.8                0.00780              
 -47.9                0.00779              
 -48.                 0.00780              
 -48.1                0.00779              
 -48.2                0.00780              
 -48.3                0.00779              
 -48.4                0.00779              
 -48.5                0.00779              
 -48.6                0.00779              
 -48.7                0.00779              
 -48.8                0.00779              
##END=
