##TITLE=              31P MAS NMR spectrum of calcined and rehydrated AlPO-52
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             McGuire et al. Zeolites, 15, 460-469 (1995) Figure 7f
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/16 11:58:04
##SOURCE REFERENCE=   AFT-31P-McGuire-1995-rehydrated
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              AFT
##NAMES=              AlPO-52
##SAMPLE DESCRIPTION= AlPO-52, calcined, hydrated

$$Bibliographic information 
##$AUTHORS=           McGuire, N.K., Bateman, C.A., Scott Blackwell, C., Wilson, S.T., Kirchner, R.M.
##$TITLE=             Structure refinement, electron microscopy, and solid-state magic angle spinning nuclear magnetic resonance characterization of AlPO4-52: An aluminophosphate with a large cage
##$JOURNAL=           Zeolites
##$VOLUME=            15
##$PAGES=             460-469
##$YEAR=              1995
##$DOI=               10.1016/0144-2449(94)00040-Y
##$FIGURE=            Figure 7f

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         6
##$PEAK LABELS=        A          B          C          D          E          F         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -25.997    -25.797    -25.597    -25.397    -20.6447   -14.1497   
##$PEAK AREAS=         1.         1.         1.         1.         1.         1.        
##$PEAK WIDTHS=        8.53715    8.53715    8.53715    8.53715    8.53715    8.53715   
##$PEAK SHAPES=        0.3731     0.3731     0.3731     0.3731     0.3731     0.3731    
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 161.9
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     15000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              10.2                 
##LASTX=              -49.6                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            300
##FIRSTY=              0.00358              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  10.2                0.00358              
  10.                 0.00340              
  9.8                 0.00352              
  9.6                 0.00366              
  9.4                 0.00343              
  9.2                 0.00328              
  9.                  0.00331              
  8.8                 0.00328              
  8.6                 0.00338              
  8.4                 0.00366              
  8.2                 0.00358              
  8.                  0.00327              
  7.8                 0.00331              
  7.6                 0.00330              
  7.4                 0.00330              
  7.2                 0.00328              
  7.                  0.00338              
  6.8                 0.00351              
  6.6                 0.00338              
  6.4                 0.00329              
  6.2                 0.00330              
  6.                  0.00330              
  5.8                 0.00331              
  5.6                 0.00325              
  5.4                 0.00302              
  5.2                 0.00288              
  5.                  0.00307              
  4.8                 0.00301              
  4.6                 0.00271              
  4.4                 0.00292              
  4.2                 0.00286              
  4.                  0.00270              
  3.8                 0.00277              
  3.6                 0.00309              
  3.4                 0.00333              
  3.2                 0.00329              
  3.                  0.00330              
  2.8                 0.00330              
  2.6                 0.00330              
  2.4                 0.00330              
  2.2                 0.00329              
  2.                  0.00333              
  1.8                 0.00347              
  1.6                 0.00340              
  1.4                 0.00332              
  1.2                 0.00354              
  1.                  0.00379              
  0.8                 0.00387              
  0.6                 0.00389              
  0.4                 0.00407              
  0.2                 0.00448              
  0.00000             0.00492              
 -0.2                 0.00508              
 -0.4                 0.00542              
 -0.6                 0.00592              
 -0.8                 0.00620              
 -1.                  0.00637              
 -1.2                 0.00661              
 -1.4                 0.00680              
 -1.6                 0.00712              
 -1.8                 0.00732              
 -2.                  0.00768              
 -2.2                 0.00833              
 -2.4                 0.00850              
 -2.6                 0.00906              
 -2.8                 0.00975              
 -3.                  0.01035              
 -3.2                 0.01101              
 -3.4                 0.01174              
 -3.6                 0.01260              
 -3.8                 0.01333              
 -4.                  0.01398              
 -4.2                 0.01470              
 -4.4                 0.01553              
 -4.6                 0.01643              
 -4.8                 0.01753              
 -5.                  0.01868              
 -5.2                 0.01987              
 -5.4                 0.02092              
 -5.6                 0.02157              
 -5.8                 0.02243              
 -6.                  0.02386              
 -6.2                 0.02526              
 -6.4                 0.02595              
 -6.6                 0.02751              
 -6.8                 0.02924              
 -7.                  0.03057              
 -7.2                 0.03229              
 -7.4                 0.03381              
 -7.6                 0.03521              
 -7.8                 0.03692              
 -8.                  0.03903              
 -8.2                 0.04144              
 -8.4                 0.04363              
 -8.6                 0.04618              
 -8.8                 0.04860              
 -9.                  0.05109              
 -9.2                 0.05388              
 -9.4                 0.05669              
 -9.6                 0.05978              
 -9.8                 0.06255              
 -10.                 0.06542              
 -10.2                0.06835              
 -10.4                0.07161              
 -10.6                0.07465              
 -10.8                0.07721              
 -11.                 0.08001              
 -11.2                0.08315              
 -11.4                0.08630              
 -11.6                0.08911              
 -11.8                0.09176              
 -12.                 0.09461              
 -12.2                0.09720              
 -12.4                0.10006              
 -12.6                0.10319              
 -12.8                0.10634              
 -13.                 0.1099               
 -13.2                0.11289              
 -13.4                0.11673              
 -13.6                0.12071              
 -13.8                0.12480              
 -14.                 0.12923              
 -14.2                0.13356              
 -14.4                0.13781              
 -14.6                0.14072              
 -14.8                0.14375              
 -15.                 0.14628              
 -15.2                0.14816              
 -15.4                0.15023              
 -15.6                0.15180              
 -15.8                0.15288              
 -16.                 0.15432              
 -16.2                0.15615              
 -16.4                0.15863              
 -16.6                0.16111              
 -16.8                0.16419              
 -17.                 0.16757              
 -17.2                0.17040              
 -17.4                0.17390              
 -17.6                0.17764              
 -17.8                0.18171              
 -18.                 0.18602              
 -18.2                0.19036              
 -18.4                0.19499              
 -18.6                0.19937              
 -18.8                0.20506              
 -19.                 0.20952              
 -19.2                0.21505              
 -19.4                0.22172              
 -19.6                0.22789              
 -19.8                0.23474              
 -20.                 0.24078              
 -20.2                0.24708              
 -20.4                0.25427              
 -20.6                0.26255              
 -20.8                0.27222              
 -21.                 0.28059              
 -21.2                0.28969              
 -21.4                0.29976              
 -21.6                0.30859              
 -21.8                0.31934              
 -22.                 0.32904              
 -22.2                0.34128              
 -22.4                0.35322              
 -22.6                0.36196              
 -22.8                0.37127              
 -23.                 0.37904              
 -23.2                0.38640              
 -23.4                0.39296              
 -23.6                0.39983              
 -23.8                0.40627              
 -24.                 0.41169              
 -24.2                0.41717              
 -24.4                0.42180              
 -24.6                0.42514              
 -24.8                0.42816              
 -25.                 0.42983              
 -25.2                0.43040              
 -25.4                0.42999              
 -25.6                0.42821              
 -25.8                0.42502              
 -26.                 0.42012              
 -26.2                0.41428              
 -26.4                0.40851              
 -26.6                0.40164              
 -26.8                0.39421              
 -27.                 0.38604              
 -27.2                0.37671              
 -27.4                0.36641              
 -27.6                0.35449              
 -27.8                0.34358              
 -28.                 0.33185              
 -28.2                0.31837              
 -28.4                0.30571              
 -28.6                0.29211              
 -28.8                0.27951              
 -29.                 0.26713              
 -29.2                0.25414              
 -29.4                0.24157              
 -29.6                0.22851              
 -29.8                0.21651              
 -30.                 0.20507              
 -30.2                0.19332              
 -30.4                0.18214              
 -30.6                0.16959              
 -30.8                0.15827              
 -31.                 0.14531              
 -31.2                0.13285              
 -31.4                0.12256              
 -31.6                0.11307              
 -31.8                0.10491              
 -32.                 0.09655              
 -32.2                0.08970              
 -32.4                0.08189              
 -32.6                0.07459              
 -32.8                0.06904              
 -33.                 0.06289              
 -33.2                0.05753              
 -33.4                0.05371              
 -33.6                0.05007              
 -33.8                0.0468               
 -34.                 0.04333              
 -34.2                0.04102              
 -34.4                0.03869              
 -34.6                0.03664              
 -34.8                0.03490              
 -35.                 0.03322              
 -35.2                0.03208              
 -35.4                0.03084              
 -35.6                0.02948              
 -35.8                0.02809              
 -36.                 0.02678              
 -36.2                0.02586              
 -36.4                0.02500              
 -36.6                0.02416              
 -36.8                0.02314              
 -37.                 0.02198              
 -37.2                0.02119              
 -37.4                0.02070              
 -37.6                0.02008              
 -37.8                0.01945              
 -38.                 0.01896              
 -38.2                0.01835              
 -38.4                0.01772              
 -38.6                0.01692              
 -38.8                0.01615              
 -39.                 0.01594              
 -39.2                0.01549              
 -39.4                0.01495              
 -39.6                0.01443              
 -39.8                0.01387              
 -40.                 0.01318              
 -40.2                0.01275              
 -40.4                0.01251              
 -40.6                0.01208              
 -40.8                0.01159              
 -41                  0.01109              
 -41.2                0.01015              
 -41.4                0.00945              
 -41.6                0.00921              
 -41.8                0.00896              
 -42.                 0.00874              
 -42.2                0.00835              
 -42.4                0.00767              
 -42.6                0.00721              
 -42.8                0.00706              
 -43.                 0.00679              
 -43.2                0.00672              
 -43.4                0.00670              
 -43.6                0.00650              
 -43.8                0.00620              
 -44.                 0.00594              
 -44.2                0.00597              
 -44.4                0.00576              
 -44.6                0.00511              
 -44.8                0.00452              
 -45.                 0.00445              
 -45.2                0.00438              
 -45.4                0.00417              
 -45.6                0.00391              
 -45.8                0.00365              
 -46.                 0.00341              
 -46.2                0.00329              
 -46.4                0.00330              
 -46.6                0.00330              
 -46.8                0.00330              
 -47.                 0.00331              
 -47.2                0.00327              
 -47.4                0.00303              
 -47.6                0.00294              
 -47.8                0.00320              
 -48.                 0.00298              
 -48.2                0.00268              
 -48.4                0.00282              
 -48.6                0.00291              
 -48.8                0.00258              
 -49.                 0.00213              
 -49.2                0.00215              
 -49.4                0.00216              
 -49.6                0.00214              
##END=
