##TITLE=              31P MAS NMR spectrum of as-made AlPO-21 (with N,N,N',N'-tetramethylethylenediamine template)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Tuel et al. J. Solid State Chem., 178, 782-791 (2005) Figure 5b
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/20 06:58:08
##SOURCE REFERENCE=   AWO-31P-Tuel-2005-asmade
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              AWO
##NAMES=              AlPO-21
##SAMPLE DESCRIPTION= AlPO-21, as-made

$$Bibliographic information 
##$AUTHORS=           Tuel, A., Jorda, J.L., Gramlich, V., Baerlocher, C.
##$TITLE=             Synthesis and characterization of two aluminophosphates templated by N-methyl-1,3-diaminopropane
##$JOURNAL=           Journal of Solid State Chemistry
##$VOLUME=            178
##$PAGES=             782-791
##$YEAR=              2005
##$DOI=               10.1016/j.jssc.2004.11.027
##$FIGURE=            Figure 5b

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         3
##$PEAK LABELS=        P1         P2         P3         
##$PEAK TSITES=        T2         T3         T1
##$PEAK POSITIONS=    -28.7577   -23.7427   -16.7744   
##$PEAK AREAS=         1.         1.         1.        
##$PEAK WIDTHS=        2.61818    2.2432     2.82178   
##$PEAK SHAPES=        0.60799    0.60799    0.60799   
##$NUMBERING REF=     Bennett et al. Inorg. Chem., 24, 188-193 (1985)
##$ASSIGN REF=        Tuel et al. J. Solid State Chem., 178, 782-791 (2005) Figure 5b
##$ASSIGN METHOD=     average bond angles
##$COMMENT=           Peak assignments are based on average bond angles determined from a single-crystal XRD structure

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 162.0
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     14000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -4.9                  
##LASTX=              -39.8                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            350
##FIRSTY=              0.00326              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -4.9                 0.00326              
 -5                   0.00372              
 -5.1                 0.00408              
 -5.2                 0.00431              
 -5.3                 0.00453              
 -5.4                 0.00472              
 -5.5                 0.00431              
 -5.6                 0.00361              
 -5.7                 0.00284              
 -5.8                 0.00252              
 -5.9                 0.00329              
 -6.                  0.00479              
 -6.1                 0.00670              
 -6.2                 0.00807              
 -6.3                 0.00839              
 -6.4                 0.00756              
 -6.5                 0.00606              
 -6.6                 0.00461              
 -6.7                 0.00340              
 -6.8                 0.00312              
 -6.9                 0.00353              
 -7.                  0.00412              
 -7.1                 0.00448              
 -7.2                 0.00440              
 -7.3                 0.00404              
 -7.4                 0.00385              
 -7.5                 0.00403              
 -7.6                 0.00445              
 -7.7                 0.00511              
 -7.8                 0.00553              
 -7.9                 0.00565              
 -8.                  0.00534              
 -8.1                 0.00462              
 -8.2                 0.00397              
 -8.3                 0.00331              
 -8.4                 0.00301              
 -8.5                 0.00320              
 -8.6                 0.00384              
 -8.7                 0.00498              
 -8.8                 0.00604              
 -8.9                 0.00706              
 -9.                  0.00769              
 -9.1                 0.00800              
 -9.2                 0.00802              
 -9.3                 0.00808              
 -9.4                 0.00861              
 -9.5                 0.00939              
 -9.6                 0.00993              
 -9.7                 0.01048              
 -9.8                 0.01067              
 -9.9                 0.01049              
 -10.                 0.01010              
 -10.1                0.00980              
 -10.2                0.00984              
 -10.3                0.01026              
 -10.4                0.01110              
 -10.5                0.01212              
 -10.6                0.01295              
 -10.7                0.01367              
 -10.8                0.01370              
 -10.9                0.01297              
 -11.                 0.01178              
 -11.1                0.01029              
 -11.2                0.00932              
 -11.3                0.00903              
 -11.4                0.00950              
 -11.5                0.01046              
 -11.6                0.01127              
 -11.7                0.01180              
 -11.8                0.01187              
 -11.9                0.01169              
 -12.                 0.01198              
 -12.1                0.01277              
 -12.2                0.01350              
 -12.3                0.01415              
 -12.4                0.01403              
 -12.5                0.01319              
 -12.6                0.01214              
 -12.7                0.01120              
 -12.8                0.01135              
 -12.9                0.01231              
 -13.                 0.01325              
 -13.1                0.01408              
 -13.2                0.01431              
 -13.3                0.01406              
 -13.4                0.01411              
 -13.5                0.01485              
 -13.6                0.01654              
 -13.7                0.01912              
 -13.8                0.02209              
 -13.9                0.02542              
 -14.                 0.02852              
 -14.1                0.03198              
 -14.2                0.03535              
 -14.3                0.03929              
 -14.4                0.04364              
 -14.5                0.04894              
 -14.6                0.05474              
 -14.7                0.06208              
 -14.8                0.07062              
 -14.9                0.08079              
 -15.                 0.09156              
 -15.1                0.10379              
 -15.2                0.11581              
 -15.3                0.12910              
 -15.4                0.14230              
 -15.5                0.15708              
 -15.6                0.17133              
 -15.7                0.18661              
 -15.8                0.20028              
 -15.9                0.21454              
 -16.                 0.22693              
 -16.1                0.23966              
 -16.2                0.25020              
 -16.3                0.26042              
 -16.4                0.26784              
 -16.5                0.27409              
 -16.6                0.27708              
 -16.7                0.27834              
 -16.8                0.27573              
 -16.9                0.27156              
 -17.                 0.26511              
 -17.1                0.25659              
 -17.2                0.24659              
 -17.3                0.23505              
 -17.4                0.22363              
 -17.5                0.21119              
 -17.6                0.19994              
 -17.7                0.18782              
 -17.8                0.17698              
 -17.9                0.16538              
 -18.                 0.15546              
 -18.1                0.14512              
 -18.2                0.13649              
 -18.3                0.12738              
 -18.4                0.12005              
 -18.5                0.11258              
 -18.6                0.10685              
 -18.7                0.10090              
 -18.8                0.09666              
 -18.9                0.09246              
 -19.                 0.08912              
 -19.1                0.08563              
 -19.2                0.08276              
 -19.3                0.07962              
 -19.4                0.07712              
 -19.5                0.07447              
 -19.6                0.07222              
 -19.7                0.06975              
 -19.8                0.06761              
 -19.9                0.06524              
 -20.                 0.06366              
 -20.1                0.06229              
 -20.2                0.06171              
 -20.3                0.06124              
 -20.4                0.06035              
 -20.5                0.05900              
 -20.6                0.05719              
 -20.7                0.05501              
 -20.8                0.05347              
 -20.9                0.05196              
 -21.                 0.05193              
 -21.1                0.05292              
 -21.2                0.05521              
 -21.3                0.05836              
 -21.4                0.06232              
 -21.5                0.06596              
 -21.6                0.07019              
 -21.7                0.07450              
 -21.8                0.08060              
 -21.9                0.08742              
 -22.                 0.09736              
 -22.1                0.10823              
 -22.2                0.12291              
 -22.3                0.13757              
 -22.4                0.15493              
 -22.5                0.17083              
 -22.6                0.18891              
 -22.7                0.20597              
 -22.8                0.22591              
 -22.9                0.24394              
 -23.                 0.26335              
 -23.1                0.27984              
 -23.2                0.29672              
 -23.3                0.31029              
 -23.4                0.32296              
 -23.5                0.33184              
 -23.6                0.33883              
 -23.7                0.34276              
 -23.8                0.34366              
 -23.9                0.34171              
 -24.                 0.33670              
 -24.1                0.32991              
 -24.2                0.31935              
 -24.3                0.30690              
 -24.4                0.29027              
 -24.5                0.27318              
 -24.6                0.25262              
 -24.7                0.23387              
 -24.8                0.21335              
 -24.9                0.19569              
 -25.                 0.17643              
 -25.1                0.15993              
 -25.2                0.14274              
 -25.3                0.12861              
 -25.4                0.11436              
 -25.5                0.10313              
 -25.6                0.09203              
 -25.7                0.08357              
 -25.8                0.07591              
 -25.9                0.07046              
 -26.                 0.06587              
 -26.1                0.06320              
 -26.2                0.06132              
 -26.3                0.06088              
 -26.4                0.06173              
 -26.5                0.06382              
 -26.6                0.06775              
 -26.7                0.07326              
 -26.8                0.08091              
 -26.9                0.08940              
 -27.                 0.10043              
 -27.1                0.11156              
 -27.2                0.12474              
 -27.3                0.13725              
 -27.4                0.15151              
 -27.5                0.16516              
 -27.6                0.18092              
 -27.7                0.19562              
 -27.8                0.21229              
 -27.9                0.22728              
 -28.                 0.24332              
 -28.1                0.25616              
 -28.2                0.26841              
 -28.3                0.27698              
 -28.4                0.28418              
 -28.5                0.28841              
 -28.6                0.29161              
 -28.7                0.29192              
 -28.8                0.28975              
 -28.9                0.28519              
 -29.                 0.27842              
 -29.1                0.27055              
 -29.2                0.26116              
 -29.3                0.25142              
 -29.4                0.23955              
 -29.5                0.22731              
 -29.6                0.21275              
 -29.7                0.19851              
 -29.8                0.18267              
 -29.9                0.16892              
 -30.                 0.15495              
 -30.1                0.14344              
 -30.2                0.13167              
 -30.3                0.12142              
 -30.4                0.11043              
 -30.5                0.10122              
 -30.6                0.09205              
 -30.7                0.08450              
 -30.8                0.07681              
 -30.9                0.07030              
 -31.                 0.06344              
 -31.1                0.05740              
 -31.2                0.05128              
 -31.3                0.04649              
 -31.4                0.04179              
 -31.5                0.03786              
 -31.6                0.03369              
 -31.7                0.03007              
 -31.8                0.02651              
 -31.9                0.02400              
 -32.                 0.02206              
 -32.1                0.02131              
 -32.2                0.02083              
 -32.3                0.02016              
 -32.4                0.01908              
 -32.5                0.01754              
 -32.6                0.01565              
 -32.7                0.01418              
 -32.8                0.01320              
 -32.9                0.01305              
 -33.                 0.01298              
 -33.1                0.01269              
 -33.2                0.01221              
 -33.3                0.01163              
 -33.4                0.01098              
 -33.5                0.01060              
 -33.6                0.01030              
 -33.7                0.00996              
 -33.8                0.00953              
 -33.9                0.00914              
 -34.                 0.00885              
 -34.1                0.00893              
 -34.2                0.00918              
 -34.3                0.00972              
 -34.4                0.01018              
 -34.5                0.00999              
 -34.6                0.00944              
 -34.7                0.00867              
 -34.8                0.00790              
 -34.9                0.00791              
 -35.                 0.00828              
 -35.1                0.00884              
 -35.2                0.00944              
 -35.3                0.00958              
 -35.4                0.00938              
 -35.5                0.00874              
 -35.6                0.00796              
 -35.7                0.00711              
 -35.8                0.00628              
 -35.9                0.00586              
 -36.                 0.00556              
 -36.1                0.00599              
 -36.2                0.00672              
 -36.3                0.00745              
 -36.4                0.00817              
 -36.5                0.00783              
 -36.6                0.00702              
 -36.7                0.00622              
 -36.8                0.00552              
 -36.9                0.00580              
 -37.                 0.00643              
 -37.1                0.00693              
 -37.2                0.00711              
 -37.3                0.00621              
 -37.4                0.00500              
 -37.5                0.00403              
 -37.6                0.00364              
 -37.7                0.00447              
 -37.8                0.00561              
 -37.9                0.00675              
 -38.                 0.00734              
 -38.1                0.00729              
 -38.2                0.00692              
 -38.3                0.00662              
 -38.4                0.00660              
 -38.5                0.00689              
 -38.6                0.00729              
 -38.7                0.00753              
 -38.8                0.00755              
 -38.9                0.00737              
 -39.                 0.00686              
 -39.1                0.00584              
 -39.2                0.00467              
 -39.3                0.00323              
 -39.4                0.00205              
 -39.5                0.00109              
 -39.6                0.00085              
 -39.7                0.00150              
 -39.8                0.00252              
##END=
