##TITLE=              29Si MAS NMR spectrum of calcined pure silica CIT-5
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Barrett et al. J. Chem. Soc., Faraday Trans., 94, 2475-2481 (1998) Figure 3b
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 13:52:54
##SOURCE REFERENCE=   CFI-29Si-Barrett-1998
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              CFI
##NAMES=              CIT-5
##SAMPLE DESCRIPTION= CIT-5, calcined

$$Bibliographic information 
##$AUTHORS=           Barrett, P.A., Diaz-Cabanas, M.J., Camblor, M.A., Jones, R.H.
##$TITLE=             Synthesis in fluoride and hydroxide media and structure of the extra-large pore pure silica zeolite CIT-5
##$JOURNAL=           Journal of the Chemical Society, Faraday Transactions
##$VOLUME=            94
##$PAGES=             2475-2481
##$YEAR=              1998
##$DOI=               10.1039/a803263g
##$FIGURE=            Figure 3b

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         5
##$PEAK LABELS=        A          B          C          D          E         
##$PEAK TSITES=       
##$PEAK QTYPES=       
##$PEAK POSITIONS=    -115.393   -113.7     -113.431   -108.651   -108.331   
##$PEAK AREAS=         1.         2.         2.         2.         1.        
##$PEAK WIDTHS=        0.80628    1.02721    1.03908    1.0087     1.0914    
##$PEAK SHAPES=        0.59682    0.59682    0.59682    0.59682    0.59682   
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 79.459
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     5500

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -90.02                
##LASTX=              -130.06               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            2003
##FIRSTY=              0.03540              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -90.02               0.03540              
 -90.04               0.03239              
 -90.06               0.02316              
 -90.08               0.01927              
 -90.1                0.02004              
 -90.12               0.01452              
 -90.14               0.00848              
 -90.16               0.00696              
 -90.18               0.00709              
 -90.2                0.00673              
 -90.22               0.00637              
 -90.24               0.00979              
 -90.26               0.01367              
 -90.28               0.01351              
 -90.3                0.01431              
 -90.32               0.01667              
 -90.34               0.01707              
 -90.36               0.01640              
 -90.38               0.01652              
 -90.4                0.01847              
 -90.42               0.02028              
 -90.44               0.02021              
 -90.46               0.01878              
 -90.48               0.01616              
 -90.5                0.01218              
 -90.52               0.00677              
 -90.54               0.00019              
 -90.56              -0.00654              
 -90.58              -0.01085              
 -90.6               -0.01243              
 -90.62              -0.01317              
 -90.64              -0.01155              
 -90.66              -0.00710              
 -90.68              -0.00219              
 -90.7                0.00597              
 -90.72               0.01882              
 -90.74               0.02972              
 -90.76               0.03663              
 -90.78               0.04003              
 -90.8                0.03669              
 -90.82               0.02990              
 -90.84               0.02736              
 -90.86               0.02523              
 -90.88               0.02074              
 -90.9                0.01652              
 -90.92               0.01223              
 -90.94               0.00783              
 -90.96               0.00623              
 -90.98               0.00711              
 -91.                 0.00770              
 -91.02               0.00468              
 -91.04               0.00045              
 -91.06               0.00094              
 -91.08               0.00694              
 -91.1                0.01565              
 -91.12               0.02249              
 -91.14               0.02823              
 -91.16               0.03450              
 -91.18               0.04127              
 -91.2                0.05137              
 -91.22               0.06475              
 -91.24               0.07141              
 -91.26               0.06831              
 -91.28               0.05972              
 -91.3                0.05314              
 -91.32               0.04952              
 -91.34               0.04297              
 -91.36               0.03156              
 -91.38               0.01665              
 -91.4                0.00236              
 -91.42              -0.00780              
 -91.44              -0.01371              
 -91.46              -0.02083              
 -91.48              -0.02956              
 -91.5               -0.03659              
 -91.52              -0.03926              
 -91.54              -0.03853              
 -91.56              -0.03730              
 -91.58              -0.03287              
 -91.6               -0.02626              
 -91.62              -0.02379              
 -91.64              -0.02099              
 -91.66              -0.01432              
 -91.68              -0.00952              
 -91.7               -0.00523              
 -91.72               0.00141              
 -91.74               0.00539              
 -91.76               0.00697              
 -91.78               0.01064              
 -91.8                0.01588              
 -91.82               0.02229              
 -91.84               0.03055              
 -91.86               0.03845              
 -91.88               0.04453              
 -91.9                0.05017              
 -91.92               0.05713              
 -91.94               0.06425              
 -91.96               0.06403              
 -91.98               0.05493              
 -92.                 0.04068              
 -92.02               0.02574              
 -92.04               0.01406              
 -92.06               0.00748              
 -92.08               0.00093              
 -92.1               -0.00561              
 -92.12              -0.00374              
 -92.14               0.00134              
 -92.16               0.00318              
 -92.18               0.00532              
 -92.2                0.00697              
 -92.22               0.00525              
 -92.24               0.00164              
 -92.26              -0.00267              
 -92.28              -0.00643              
 -92.3               -0.00384              
 -92.32               0.00309              
 -92.34               0.00371              
 -92.36               0.00484              
 -92.38               0.01353              
 -92.4                0.02465              
 -92.42               0.03415              
 -92.44               0.04056              
 -92.46               0.04541              
 -92.48               0.04922              
 -92.5                0.05067              
 -92.52               0.04614              
 -92.54               0.03709              
 -92.56               0.03005              
 -92.58               0.02468              
 -92.6                0.01849              
 -92.62               0.00966              
 -92.64              -0.00207              
 -92.66              -0.01492              
 -92.68              -0.02448              
 -92.7               -0.02890              
 -92.72              -0.03017              
 -92.74              -0.03577              
 -92.76              -0.04458              
 -92.78              -0.04880              
 -92.8               -0.05421              
 -92.82              -0.06307              
 -92.84              -0.06827              
 -92.86              -0.07212              
 -92.88              -0.07683              
 -92.9               -0.07589              
 -92.92              -0.06529              
 -92.94              -0.04662              
 -92.96              -0.03059              
 -92.98              -0.01918              
 -93.                -0.00681              
 -93.02               0.00542              
 -93.04               0.01548              
 -93.06               0.02261              
 -93.08               0.02786              
 -93.1                0.03205              
 -93.12               0.03462              
 -93.14               0.03649              
 -93.16               0.03866              
 -93.18               0.04012              
 -93.2                0.03933              
 -93.22               0.03548              
 -93.24               0.03080              
 -93.26               0.02678              
 -93.28               0.02306              
 -93.3                0.01792              
 -93.32               0.01147              
 -93.34               0.00679              
 -93.36               0.00276              
 -93.38              -0.00173              
 -93.4               -0.00340              
 -93.42              -0.00272              
 -93.44              -0.00248              
 -93.46              -0.00346              
 -93.48              -0.00587              
 -93.5               -0.00966              
 -93.52              -0.01443              
 -93.54              -0.01857              
 -93.56              -0.01960              
 -93.58              -0.01880              
 -93.6               -0.01866              
 -93.62              -0.02055              
 -93.64              -0.02234              
 -93.66              -0.02205              
 -93.68              -0.02348              
 -93.7               -0.02551              
 -93.72              -0.02380              
 -93.74              -0.02150              
 -93.76              -0.02193              
 -93.78              -0.02517              
 -93.8               -0.02429              
 -93.82              -0.01732              
 -93.84              -0.01335              
 -93.86              -0.00762              
 -93.88               0.00682              
 -93.9                0.02319              
 -93.92               0.03666              
 -93.94               0.04590              
 -93.96               0.05127              
 -93.98               0.05252              
 -94.                 0.04916              
 -94.02               0.04429              
 -94.04               0.04024              
 -94.06               0.03635              
 -94.08               0.03185              
 -94.1                0.02735              
 -94.12               0.02599              
 -94.14               0.02642              
 -94.16               0.02602              
 -94.18               0.02780              
 -94.2                0.02970              
 -94.22               0.02617              
 -94.24               0.02178              
 -94.26               0.02007              
 -94.28               0.01909              
 -94.3                0.01510              
 -94.32               0.00660              
 -94.34              -0.00283              
 -94.36              -0.01004              
 -94.38              -0.01414              
 -94.4               -0.01853              
 -94.42              -0.02557              
 -94.44              -0.03470              
 -94.46              -0.03988              
 -94.48              -0.03887              
 -94.5               -0.03512              
 -94.52              -0.03056              
 -94.54              -0.02638              
 -94.56              -0.02354              
 -94.58              -0.02208              
 -94.6               -0.02187              
 -94.62              -0.02347              
 -94.64              -0.02559              
 -94.66              -0.02605              
 -94.68              -0.02456              
 -94.7               -0.02239              
 -94.72              -0.02101              
 -94.74              -0.01701              
 -94.76              -0.01035              
 -94.78              -0.00705              
 -94.8               -0.00559              
 -94.82              -0.00331              
 -94.84              -0.00253              
 -94.86              -0.00278              
 -94.88              -0.00252              
 -94.9               -0.00372              
 -94.92              -0.00598              
 -94.94              -0.00664              
 -94.96              -0.00522              
 -94.98              -0.00302              
 -95.                -0.00241              
 -95.02              -0.00297              
 -95.04              -0.00308              
 -95.06              -0.00132              
 -95.08               0.00062              
 -95.1                0.00067              
 -95.12               0.00025              
 -95.14               0.00046              
 -95.16               0.00102              
 -95.18              -0.00090              
 -95.2               -0.00550              
 -95.22              -0.00983              
 -95.24              -0.01384              
 -95.26              -0.01801              
 -95.28              -0.02212              
 -95.3               -0.02636              
 -95.32              -0.03064              
 -95.34              -0.03360              
 -95.36              -0.03163              
 -95.38              -0.02302              
 -95.4               -0.01670              
 -95.42              -0.01293              
 -95.44              -0.00287              
 -95.46               0.01356              
 -95.48               0.03045              
 -95.5                0.03918              
 -95.52               0.04396              
 -95.54               0.05041              
 -95.56               0.05545              
 -95.58               0.05525              
 -95.6                0.04895              
 -95.62               0.04328              
 -95.64               0.03950              
 -95.66               0.03375              
 -95.68               0.02670              
 -95.7                0.02060              
 -95.72               0.01757              
 -95.74               0.01639              
 -95.76               0.01446              
 -95.78               0.00919              
 -95.8               -0.00171              
 -95.82              -0.01698              
 -95.84              -0.02739              
 -95.86              -0.03212              
 -95.88              -0.03734              
 -95.9               -0.04680              
 -95.92              -0.05987              
 -95.94              -0.07194              
 -95.96              -0.07910              
 -95.98              -0.08072              
 -96.                -0.08009              
 -96.02              -0.07626              
 -96.04              -0.06871              
 -96.06              -0.06224              
 -96.08              -0.05384              
 -96.1               -0.03790              
 -96.12              -0.01946              
 -96.14              -0.00353              
 -96.16               0.00782              
 -96.18               0.01674              
 -96.2                0.02499              
 -96.22               0.03219              
 -96.24               0.03711              
 -96.26               0.03917              
 -96.28               0.03957              
 -96.3                0.03939              
 -96.32               0.03932              
 -96.34               0.03961              
 -96.36               0.03942              
 -96.38               0.03762              
 -96.4                0.03508              
 -96.42               0.03309              
 -96.44               0.03254              
 -96.46               0.03318              
 -96.48               0.03336              
 -96.5                0.03031              
 -96.52               0.02572              
 -96.54               0.02182              
 -96.56               0.01628              
 -96.58               0.00998              
 -96.6                0.00562              
 -96.62               0.00187              
 -96.64              -0.00238              
 -96.66              -0.00682              
 -96.68              -0.01027              
 -96.7               -0.01222              
 -96.72              -0.01323              
 -96.74              -0.01194              
 -96.76              -0.00769              
 -96.78              -0.00324              
 -96.8                0.00081              
 -96.82               0.00510              
 -96.84               0.00856              
 -96.86               0.01017              
 -96.88               0.00922              
 -96.9                0.00474              
 -96.92              -0.00179              
 -96.94              -0.00640              
 -96.96              -0.01050              
 -96.98              -0.01666              
 -97.                -0.02504              
 -97.02              -0.03284              
 -97.04              -0.03726              
 -97.06              -0.03987              
 -97.08              -0.04175              
 -97.1               -0.04339              
 -97.12              -0.04683              
 -97.14              -0.05112              
 -97.16              -0.05220              
 -97.18              -0.05108              
 -97.2               -0.05094              
 -97.22              -0.05456              
 -97.24              -0.05837              
 -97.26              -0.05840              
 -97.28              -0.05752              
 -97.3               -0.05805              
 -97.32              -0.06029              
 -97.34              -0.06152              
 -97.36              -0.06124              
 -97.38              -0.06132              
 -97.4               -0.06091              
 -97.42              -0.05872              
 -97.44              -0.05453              
 -97.46              -0.05090              
 -97.48              -0.04911              
 -97.5               -0.04557              
 -97.52              -0.04145              
 -97.54              -0.03949              
 -97.56              -0.03672              
 -97.58              -0.03217              
 -97.6               -0.02761              
 -97.62              -0.02451              
 -97.64              -0.02261              
 -97.66              -0.01970              
 -97.68              -0.01376              
 -97.7               -0.00517              
 -97.72               0.00200              
 -97.74               0.00778              
 -97.76               0.01398              
 -97.78               0.02037              
 -97.8                0.02650              
 -97.82               0.03239              
 -97.84               0.03974              
 -97.86               0.04823              
 -97.88               0.05519              
 -97.9                0.06040              
 -97.92               0.06449              
 -97.94               0.06772              
 -97.96               0.06847              
 -97.98               0.06621              
 -98.                 0.06458              
 -98.02               0.06183              
 -98.04               0.05405              
 -98.06               0.04447              
 -98.08               0.03660              
 -98.1                0.03189              
 -98.12               0.02832              
 -98.14               0.02410              
 -98.16               0.01948              
 -98.18               0.01612              
 -98.2                0.01588              
 -98.22               0.01955              
 -98.24               0.02340              
 -98.26               0.02350              
 -98.28               0.02320              
 -98.3                0.02320              
 -98.32               0.02137              
 -98.34               0.01905              
 -98.36               0.01703              
 -98.38               0.01462              
 -98.4                0.01331              
 -98.42               0.01353              
 -98.44               0.01237              
 -98.46               0.00977              
 -98.48               0.00744              
 -98.5                0.00688              
 -98.52               0.00693              
 -98.54               0.00609              
 -98.56               0.00917              
 -98.58               0.01603              
 -98.6                0.02007              
 -98.62               0.01896              
 -98.64               0.01246              
 -98.66               0.00165              
 -98.68              -0.00726              
 -98.7               -0.01236              
 -98.72              -0.02552              
 -98.74              -0.04273              
 -98.76              -0.05110              
 -98.78              -0.04965              
 -98.8               -0.04224              
 -98.82              -0.03402              
 -98.84              -0.02545              
 -98.86              -0.01710              
 -98.88              -0.01146              
 -98.9               -0.00890              
 -98.92              -0.00885              
 -98.94              -0.01069              
 -98.96              -0.01269              
 -98.98              -0.01300              
 -99.                -0.01149              
 -99.02              -0.00930              
 -99.04              -0.00762              
 -99.06              -0.00418              
 -99.08               0.00251              
 -99.1                0.01142              
 -99.12               0.01810              
 -99.14               0.02174              
 -99.16               0.02897              
 -99.18               0.03726              
 -99.2                0.04158              
 -99.22               0.04410              
 -99.24               0.04595              
 -99.26               0.04652              
 -99.28               0.04467              
 -99.3                0.03999              
 -99.32               0.03341              
 -99.34               0.02835              
 -99.36               0.02456              
 -99.38               0.01643              
 -99.4                0.00930              
 -99.42               0.00925              
 -99.44               0.01229              
 -99.46               0.01718              
 -99.48               0.02392              
 -99.5                0.02781              
 -99.52               0.02953              
 -99.54               0.03387              
 -99.56               0.03668              
 -99.58               0.03621              
 -99.6                0.03663              
 -99.62               0.03541              
 -99.64               0.03087              
 -99.66               0.02789              
 -99.68               0.02189              
 -99.7                0.00858              
 -99.72               0.00045              
 -99.74              -0.00277              
 -99.76              -0.01086              
 -99.78              -0.01855              
 -99.8               -0.02445              
 -99.82              -0.03461              
 -99.84              -0.04397              
 -99.86              -0.04780              
 -99.88              -0.04882              
 -99.9               -0.04793              
 -99.92              -0.04566              
 -99.94              -0.04463              
 -99.96              -0.04501              
 -99.98              -0.04516              
 -100.               -0.04469              
 -100.02             -0.04486              
 -100.04             -0.04663              
 -100.06             -0.04209              
 -100.08             -0.03071              
 -100.1              -0.02500              
 -100.12             -0.02088              
 -100.14             -0.01063              
 -100.16              0.00346              
 -100.18              0.01792              
 -100.2               0.03050              
 -100.22              0.04242              
 -100.24              0.05213              
 -100.26              0.05669              
 -100.28              0.06085              
 -100.3               0.06291              
 -100.32              0.05276              
 -100.34              0.03993              
 -100.36              0.03237              
 -100.38              0.02096              
 -100.4               0.00892              
 -100.42              0.00405              
 -100.44              0.00418              
 -100.46              0.00698              
 -100.48              0.01118              
 -100.5               0.01498              
 -100.52              0.01920              
 -100.54              0.02690              
 -100.56              0.03539              
 -100.58              0.04153              
 -100.6               0.04500              
 -100.62              0.04588              
 -100.64              0.04413              
 -100.66              0.03931              
 -100.68              0.03254              
 -100.7               0.02595              
 -100.72              0.02104              
 -100.74              0.01703              
 -100.76              0.01209              
 -100.78              0.01017              
 -100.8               0.01277              
 -100.82              0.01598              
 -100.84              0.02171              
 -100.86              0.03058              
 -100.88              0.03539              
 -100.9               0.03622              
 -100.92              0.03662              
 -100.94              0.03485              
 -100.96              0.03291              
 -100.98              0.03499              
 -101.                0.03603              
 -101.02              0.03343              
 -101.04              0.03014              
 -101.06              0.02438              
 -101.08              0.01571              
 -101.1               0.00900              
 -101.12              0.00253              
 -101.14             -0.00754              
 -101.16             -0.01965              
 -101.18             -0.02886              
 -101.2              -0.03120              
 -101.22             -0.03364              
 -101.24             -0.03815              
 -101.26             -0.03926              
 -101.28             -0.03804              
 -101.3              -0.03602              
 -101.32             -0.03204              
 -101.34             -0.02819              
 -101.36             -0.02626              
 -101.38             -0.02379              
 -101.4              -0.02229              
 -101.42             -0.02439              
 -101.44             -0.02588              
 -101.46             -0.02552              
 -101.48             -0.02503              
 -101.5              -0.01894              
 -101.52             -0.00778              
 -101.54             -0.00184              
 -101.56              0.00146              
 -101.58              0.00765              
 -101.6               0.01568              
 -101.62              0.01998              
 -101.64              0.01625              
 -101.66              0.01024              
 -101.68              0.00384              
 -101.7              -0.00472              
 -101.72             -0.01170              
 -101.74             -0.01536              
 -101.76             -0.01792              
 -101.78             -0.01918              
 -101.8              -0.01905              
 -101.82             -0.01918              
 -101.84             -0.01885              
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##END=
