##TITLE=              31P MAS NMR spectrum of calcined and rehydrated EMM-3
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Afeworki et al. Chem. Mater., 18, 1705-1710 (2006) Figure 4c
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/21 15:12:40
##SOURCE REFERENCE=   EZT-31P-Afeworki-2006-rehydrated
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              EZT
##NAMES=              EMM-3
##SAMPLE DESCRIPTION= EMM-3, calcined, hydrated

$$Bibliographic information 
##$AUTHORS=           Afeworki, M., Kennedy, G.J., Dorset, D.L., Strohmaier, K.G.
##$TITLE=             Synthesis and characterization of a new microporous material. 2. AlPO and SAPO forms of EMM-3
##$JOURNAL=           Chemistry of Materials
##$VOLUME=            18
##$PAGES=             1705-1710
##$YEAR=              2006
##$DOI=               10.1021/cm052175j
##$FIGURE=            Figure 4c

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         5
##$PEAK LABELS=        A          B          C          D          E         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -29.6473   -28.4716   -27.0968   -23.1491   -20.9986   
##$PEAK AREAS=         1.         1.         1.         2.         1.        
##$PEAK WIDTHS=        1.53939    1.48049    1.83265    1.31738    1.94272   
##$PEAK SHAPES=        0.92211    0.92211    0.92211    0.92211    0.92211   
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 202.1
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     13000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              16.2                 
##LASTX=              -49.6                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            659
##FIRSTY=             -0.00617              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  16.2               -0.00617              
  16.1               -0.00597              
  16.                -0.00576              
  15.9               -0.00556              
  15.8               -0.00536              
  15.7               -0.00515              
  15.6               -0.00495              
  15.5               -0.00475              
  15.4               -0.00456              
  15.3               -0.00430              
  15.2               -0.00434              
  15.1               -0.00604              
  15.                -0.00857              
  14.9               -0.00892              
  14.8               -0.00708              
  14.7               -0.00557              
  14.6               -0.00386              
  14.5               -0.00265              
  14.4               -0.00260              
  14.3               -0.00235              
  14.2               -0.00221              
  14.1               -0.00184              
  14.                -0.00242              
  13.9               -0.00550              
  13.8               -0.00727              
  13.7               -0.00636              
  13.6               -0.00469              
  13.5               -0.00314              
  13.4               -0.00144              
  13.3               -0.00032              
  13.2               -0.00028              
  13.1               -0.00005              
  13.                 0.00011              
  12.9                0.00031              
  12.8                0.00049              
  12.7                0.00068              
  12.6                0.00087              
  12.5                0.00103              
  12.4                0.00131              
  12.3                0.00106              
  12.2               -0.00084              
  12.1               -0.00363              
  12.                -0.00586              
  11.9               -0.00588              
  11.8               -0.00346              
  11.7               -0.00032              
  11.6                0.00218              
  11.5                0.00288              
  11.4                0.00353              
  11.3                0.00549              
  11.2                0.00597              
  11.1                0.00324              
  11.                -0.00126              
  10.9               -0.00386              
  10.8               -0.00488              
  10.7               -0.00576              
  10.6               -0.00404              
  10.5               -0.00076              
  10.4                0.00169              
  10.3                0.00176              
  10.2                0.00005              
  10.1                0.00021              
  10.                 0.00286              
  9.9                 0.00539              
  9.8                 0.00543              
  9.7                 0.00320              
  9.6                 0.00053              
  9.5                -0.00219              
  9.4                -0.00411              
  9.3                -0.00464              
  9.2                -0.00297              
  9.1                 0.00134              
  9.                  0.00408              
  8.9                 0.00549              
  8.8                 0.00644              
  8.7                 0.00555              
  8.6                 0.00445              
  8.5                 0.00214              
  8.4                 0.00086              
  8.3                 0.00304              
  8.2                 0.00627              
  8.1                 0.00843              
  8.                  0.00898              
  7.9                 0.00906              
  7.8                 0.00922              
  7.7                 0.00948              
  7.6                 0.00886              
  7.5                 0.00649              
  7.4                 0.00446              
  7.3                 0.00523              
  7.2                 0.00719              
  7.1                 0.00693              
  7.                  0.00431              
  6.9                 0.00328              
  6.8                 0.00588              
  6.7                 0.00720              
  6.6                 0.00511              
  6.5                 0.00225              
  6.4                 0.00054              
  6.3                 0.00042              
  6.2                 0.00064              
  6.1                 0.00078              
  6.                  0.00094              
  5.9                 0.00109              
  5.8                 0.00124              
  5.7                 0.00139              
  5.6                 0.00154              
  5.5                 0.00169              
  5.4                 0.00184              
  5.3                 0.00199              
  5.2                 0.00214              
  5.1                 0.00229              
  5.                  0.00244              
  4.9                 0.00259              
  4.8                 0.00273              
  4.7                 0.00288              
  4.6                 0.00303              
  4.5                 0.00317              
  4.4                 0.00332              
  4.3                 0.00346              
  4.2                 0.00361              
  4.1                 0.00375              
  4.                  0.00389              
  3.9                 0.00404              
  3.8                 0.00418              
  3.7                 0.00432              
  3.6                 0.00446              
  3.5                 0.00460              
  3.4                 0.00474              
  3.3                 0.00488              
  3.2                 0.00502              
  3.1                 0.00516              
  3.                  0.00530              
  2.9                 0.00543              
  2.8                 0.00557              
  2.7                 0.00571              
  2.6                 0.00584              
  2.5                 0.00598              
  2.4                 0.00611              
  2.3                 0.00625              
  2.2                 0.00638              
  2.1                 0.00652              
  2.                  0.00665              
  1.9                 0.00678              
  1.8                 0.00691              
  1.7                 0.00704              
  1.6                 0.00717              
  1.5                 0.00731              
  1.4                 0.00744              
  1.3                 0.00756              
  1.2                 0.00769              
  1.1                 0.00782              
  1.                  0.00795              
  0.9                 0.00808              
  0.8                 0.00820              
  0.7                 0.00833              
  0.6                 0.00846              
  0.5                 0.00858              
  0.4                 0.00871              
  0.3                 0.00883              
  0.2                 0.00895              
  0.1                 0.00911              
 -0.00000             0.00906              
 -0.1                 0.00340              
 -0.2                -0.00029              
 -0.3                 0.00281              
 -0.4                 0.00408              
 -0.5                 0.00271              
 -0.6                 0.00153              
 -0.7                 0.00170              
 -0.8                 0.00180              
 -0.9                 0.00193              
 -1.                  0.00203              
 -1.1                 0.00222              
 -1.2                 0.00394              
 -1.3                 0.00688              
 -1.4                 0.00796              
 -1.5                 0.00487              
 -1.6                 0.00092              
 -1.7                -0.00175              
 -1.8                -0.00407              
 -1.9                -0.00200              
 -2.                  0.00051              
 -2.1                 0.00072              
 -2.2                 0.00402              
 -2.3                 0.00636              
 -2.4                 0.00454              
 -2.5                 0.00197              
 -2.6                 0.00101              
 -2.7                 0.00120              
 -2.8                 0.00128              
 -2.9                 0.00140              
 -3.                  0.00151              
 -3.1                 0.00161              
 -3.2                 0.00172              
 -3.3                 0.00182              
 -3.4                 0.00193              
 -3.5                 0.00203              
 -3.6                 0.00214              
 -3.7                 0.00224              
 -3.8                 0.00235              
 -3.9                 0.00245              
 -4.                  0.00255              
 -4.1                 0.00265              
 -4.2                 0.00275              
 -4.3                 0.00285              
 -4.4                 0.00296              
 -4.5                 0.00305              
 -4.6                 0.00315              
 -4.7                 0.00325              
 -4.8                 0.00335              
 -4.9                 0.00345              
 -5.                  0.00355              
 -5.1                 0.00364              
 -5.2                 0.00374              
 -5.3                 0.00383              
 -5.4                 0.00393              
 -5.5                 0.00402              
 -5.6                 0.00412              
 -5.7                 0.00421              
 -5.8                 0.00431              
 -5.9                 0.00440              
 -6.                  0.00449              
 -6.1                 0.00458              
 -6.2                 0.00467              
 -6.3                 0.00476              
 -6.4                 0.00485              
 -6.5                 0.00494              
 -6.6                 0.00503              
 -6.7                 0.00512              
 -6.8                 0.00521              
 -6.9                 0.00530              
 -7.                  0.00538              
 -7.1                 0.00547              
 -7.2                 0.00556              
 -7.3                 0.00564              
 -7.4                 0.00573              
 -7.5                 0.00581              
 -7.6                 0.00590              
 -7.7                 0.00598              
 -7.8                 0.00608              
 -7.9                 0.00609              
 -8.                  0.00642              
 -8.1                 0.00529              
 -8.2                 0.00201              
 -8.3                 0.00071              
 -8.4                 0.00096              
 -8.5                 0.00148              
 -8.6                 0.00391              
 -8.7                 0.00633              
 -8.8                 0.00694              
 -8.9                 0.00692              
 -9.                  0.00702              
 -9.1                 0.00709              
 -9.2                 0.00717              
 -9.3                 0.00725              
 -9.4                 0.00732              
 -9.5                 0.00740              
 -9.6                 0.00747              
 -9.7                 0.00754              
 -9.8                 0.00761              
 -9.9                 0.00769              
 -10.                 0.00774              
 -10.1                0.00792              
 -10.2                0.00758              
 -10.3                0.01000              
 -10.4                0.01513              
 -10.5                0.01662              
 -10.6                0.01717              
 -10.7                0.01899              
 -10.8                0.01954              
 -10.9                0.01947              
 -11.                 0.01971              
 -11.1                0.01890              
 -11.2                0.01734              
 -11.3                0.01681              
 -11.4                0.01786              
 -11.5                0.01955              
 -11.6                0.02006              
 -11.7                0.02002              
 -11.8                0.02011              
 -11.9                0.02017              
 -12.                 0.02020              
 -12.1                0.02039              
 -12.2                0.01954              
 -12.3                0.01782              
 -12.4                0.01847              
 -12.5                0.02025              
 -12.6                0.02065              
 -12.7                0.02063              
 -12.8                0.02071              
 -12.9                0.02076              
 -13.                 0.02082              
 -13.1                0.02087              
 -13.2                0.02092              
 -13.3                0.02099              
 -13.4                0.02100              
 -13.5                0.02122              
 -13.6                0.02009              
 -13.7                0.01960              
 -13.8                0.02098              
 -13.9                0.02137              
 -14.                 0.02134              
 -14.1                0.02141              
 -14.2                0.02145              
 -14.3                0.02150              
 -14.4                0.02155              
 -14.5                0.02160              
 -14.6                0.02165              
 -14.7                0.02170              
 -14.8                0.02175              
 -14.9                0.02179              
 -15.                 0.02184              
 -15.1                0.02188              
 -15.2                0.02193              
 -15.3                0.02198              
 -15.4                0.02201              
 -15.5                0.02208              
 -15.6                0.02203              
 -15.7                0.02331              
 -15.8                0.02482              
 -15.9                0.02613              
 -16.                 0.02896              
 -16.1                0.02949              
 -16.2                0.02679              
 -16.3                0.02638              
 -16.4                0.02911              
 -16.5                0.03079              
 -16.6                0.03082              
 -16.7                0.03217              
 -16.8                0.03248              
 -16.9                0.02976              
 -17.                 0.02950              
 -17.1                0.03223              
 -17.2                0.03511              
 -17.3                0.03669              
 -17.4                0.03543              
 -17.5                0.03400              
 -17.6                0.03399              
 -17.7                0.03405              
 -17.8                0.03403              
 -17.9                0.03679              
 -18.                 0.03967              
 -18.1                0.03973              
 -18.2                0.04113              
 -18.3                0.04395              
 -18.4                0.04678              
 -18.5                0.04821              
 -18.6                0.04965              
 -18.7                0.05389              
 -18.8                0.05665              
 -18.9                0.05671              
 -19.                 0.06105              
 -19.1                0.06660              
 -19.2                0.06940              
 -19.3                0.07368              
 -19.4                0.07786              
 -19.5                0.08386              
 -19.6                0.09972              
 -19.7                0.11619              
 -19.8                0.12571              
 -19.9                0.13754              
 -20.                 0.16086              
 -20.1                0.19380              
 -20.2                0.23149              
 -20.3                0.26311              
 -20.4                0.29086              
 -20.5                0.31943              
 -20.6                0.35684              
 -20.7                0.39485              
 -20.8                0.41727              
 -20.9                0.43513              
 -21.                 0.44628              
 -21.1                0.44295              
 -21.2                0.42955              
 -21.3                0.41191              
 -21.4                0.38945              
 -21.5                0.37257              
 -21.6                0.36170              
 -21.7                0.34857              
 -21.8                0.33736              
 -21.9                0.33783              
 -22.                 0.34619              
 -22.1                0.36823              
 -22.2                0.41227              
 -22.3                0.48757              
 -22.4                0.57513              
 -22.5                0.65495              
 -22.6                0.73764              
 -22.7                0.83329              
 -22.8                0.93118              
 -22.9                1.00848              
 -23.                 1.05245              
 -23.1                1.07249              
 -23.2                1.04691              
 -23.3                1.00084              
 -23.4                0.92890              
 -23.5                0.82892              
 -23.6                0.73842              
 -23.7                0.66775              
 -23.8                0.60173              
 -23.9                0.52319              
 -24.                 0.44904              
 -24.1                0.39881              
 -24.2                0.36887              
 -24.3                0.34426              
 -24.4                0.31410              
 -24.5                0.28815              
 -24.6                0.26907              
 -24.7                0.25554              
 -24.8                0.24706              
 -24.9                0.24020              
 -25.                 0.23322              
 -25.1                0.22598              
 -25.2                0.22012              
 -25.3                0.21868              
 -25.4                0.21884              
 -25.5                0.21884              
 -25.6                0.21863              
 -25.7                0.21968              
 -25.8                0.22620              
 -25.9                0.23701              
 -26.                 0.24817              
 -26.1                0.26357              
 -26.2                0.28760              
 -26.3                0.31437              
 -26.4                0.34172              
 -26.5                0.37254              
 -26.6                0.40495              
 -26.7                0.43688              
 -26.8                0.46561              
 -26.9                0.48816              
 -27.                 0.50580              
 -27.1                0.51932              
 -27.2                0.52865              
 -27.3                0.53354              
 -27.4                0.53534              
 -27.5                0.53680              
 -27.6                0.54241              
 -27.7                0.55588              
 -27.8                0.57461              
 -27.9                0.59385              
 -28.                 0.61094              
 -28.1                0.62879              
 -28.2                0.64968              
 -28.3                0.66900              
 -28.4                0.68298              
 -28.5                0.69079              
 -28.6                0.69048              
 -28.7                0.68288              
 -28.8                0.67125              
 -28.9                0.65821              
 -29.                 0.64704              
 -29.1                0.63820              
 -29.2                0.63027              
 -29.3                0.62517              
 -29.4                0.61985              
 -29.5                0.61090              
 -29.6                0.60058              
 -29.7                0.58607              
 -29.8                0.56114              
 -29.9                0.52105              
 -30.                 0.47472              
 -30.1                0.43408              
 -30.2                0.40522              
 -30.3                0.37334              
 -30.4                0.32170              
 -30.5                0.27551              
 -30.6                0.24841              
 -30.7                0.23135              
 -30.8                0.20879              
 -30.9                0.17909              
 -31.                 0.15955              
 -31.1                0.14532              
 -31.2                0.12819              
 -31.3                0.11482              
 -31.4                0.10615              
 -31.5                0.09661              
 -31.6                0.08834              
 -31.7                0.08351              
 -31.8                0.07944              
 -31.9                0.07502              
 -32.                 0.07181              
 -32.1                0.06907              
 -32.2                0.06616              
 -32.3                0.06350              
 -32.4                0.05948              
 -32.5                0.05613              
 -32.6                0.05370              
 -32.7                0.04857              
 -32.8                0.04375              
 -32.9                0.04061              
 -33.                 0.03879              
 -33.1                0.03847              
 -33.2                0.03800              
 -33.3                0.03107              
 -33.4                0.02301              
 -33.5                0.02175              
 -33.6                0.02075              
 -33.7                0.01793              
 -33.8                0.01598              
 -33.9                0.01689              
 -34.                 0.01844              
 -34.1                0.01867              
 -34.2                0.01752              
 -34.3                0.01475              
 -34.4                0.01295              
 -34.5                0.01276              
 -34.6                0.01274              
 -34.7                0.01266              
 -34.8                0.01270              
 -34.9                0.01143              
 -35.                 0.00986              
 -35.1                0.00957              
 -35.2                0.01078              
 -35.3                0.01224              
 -35.4                0.01231              
 -35.5                0.01222              
 -35.6                0.01217              
 -35.7                0.01211              
 -35.8                0.01205              
 -35.9                0.01198              
 -36.                 0.01198              
 -36.1                0.01063              
 -36.2                0.00908              
 -36.3                0.00895              
 -36.4                0.00890              
 -36.5                0.00883              
 -36.6                0.00877              
 -36.7                0.00871              
 -36.8                0.00862              
 -36.9                0.00986              
 -37.                 0.01258              
 -37.1                0.01404              
 -37.2                0.01127              
 -37.3                0.00834              
 -37.4                0.00824              
 -37.5                0.00818              
 -37.6                0.00811              
 -37.7                0.00804              
 -37.8                0.00797              
 -37.9                0.00790              
 -38.                 0.00783              
 -38.1                0.00775              
 -38.2                0.00768              
 -38.3                0.00761              
 -38.4                0.00754              
 -38.5                0.00746              
 -38.6                0.00739              
 -38.7                0.00732              
 -38.8                0.00723              
 -38.9                0.00720              
 -39.                 0.00863              
 -39.1                0.01140              
 -39.2                0.01405              
 -39.3                0.01526              
 -39.4                0.01508              
 -39.5                0.01345              
 -39.6                0.01058              
 -39.7                0.00929              
 -39.8                0.00926              
 -39.9                0.00918              
 -40.                 0.00904              
 -40.1                0.00919              
 -40.2                0.01215              
 -40.3                0.01454              
 -40.4                0.01430              
 -40.5                0.01421              
 -40.6                0.01225              
 -40.7                0.00803              
 -40.8                0.00717              
 -40.9                0.00845              
 -41.                 0.00821              
 -41.1                0.00822              
 -41.2                0.00786              
 -41.3                0.00654              
 -41.4                0.00866              
 -41.5                0.01240              
 -41.6                0.01142              
 -41.7                0.00871              
 -41.8                0.00766              
 -41.9                0.00740              
 -42.                 0.00740              
 -42.1                0.00723              
 -42.2                0.00733              
 -42.3                0.00909              
 -42.4                0.01167              
 -42.5                0.01258              
 -42.6                0.01218              
 -42.7                0.01022              
 -42.8                0.00745              
 -42.9                0.00644              
 -43.                 0.00644              
 -43.1                0.00633              
 -43.2                0.00618              
 -43.3                0.00633              
 -43.4                0.00820              
 -43.5                0.01071              
 -43.6                0.01153              
 -43.7                0.01106              
 -43.8                0.00898              
 -43.9                0.00627              
 -44.                 0.00535              
 -44.1                0.00534              
 -44.2                0.00526              
 -44.3                0.00498              
 -44.4                0.00570              
 -44.5                0.00888              
 -44.6                0.01066              
 -44.7                0.00994              
 -44.8                0.00781              
 -44.9                0.00514              
 -45.                 0.00431              
 -45.1                0.00430              
 -45.2                0.00419              
 -45.3                0.00401              
 -45.4                0.00428              
 -45.5                0.00634              
 -45.6                0.00870              
 -45.7                0.00934              
 -45.8                0.00872              
 -45.9                0.00644              
 -46.                 0.00386              
 -46.1                0.00311              
 -46.2                0.00309              
 -46.3                0.00297              
 -46.4                0.00278              
 -46.5                0.00311              
 -46.6                0.00528              
 -46.7                0.00751              
 -46.8                0.00823              
 -46.9                0.00679              
 -47.                 0.00334              
 -47.1                0.00182              
 -47.2                0.00198              
 -47.3                0.00177              
 -47.4                0.00174              
 -47.5                0.00135              
 -47.6                0.00259              
 -47.7                0.00576              
 -47.8                0.00718              
 -47.9                0.00542              
 -48.                 0.00200              
 -48.1                0.00064              
 -48.2                0.00077              
 -48.3                0.00057              
 -48.4                0.00049              
 -48.5                0.00026              
 -48.6                0.00076              
 -48.7                0.00304              
 -48.8                0.00525              
 -48.9                0.00492              
 -49.                 0.00225              
 -49.1               -0.00005              
 -49.2               -0.00060              
 -49.3               -0.00064              
 -49.4               -0.00079              
 -49.5               -0.00092              
 -49.6               -0.00105              
##END=
