##TITLE=              29Si MAS NMR spectrum of calcined ITQ-50
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Jorda et al. Angew. Chem. Int. Ed., 52, 10458-10462 (2013) Figure S2
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 14:27:30
##SOURCE REFERENCE=   IFY-29Si-Jorda-2013
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              IFY
##NAMES=              ITQ-50
##SAMPLE DESCRIPTION= ITQ-50, calcined

$$Bibliographic information 
##$AUTHORS=           Jorda, J.L., Rey, F., Sastre, G., Valencia, S., Palomino, M., Corma, A., Segura, A., Errandonea, D., Lacomba, R., Manjon, F.J., Gomis, O., Kleppe, A.K., Jephcoat, A.P., Amboage, M., Rodriguez-Velamazan, J.A.
##$TITLE=             Synthesis of a novel zeolite through a pressure-induced reconstructive phase transition process
##$JOURNAL=           Angewandte Chemie, International Edition
##$VOLUME=            52
##$PAGES=             10458-10462
##$YEAR=              2013
##$DOI=               10.1002/anie.201305230
##$FIGURE=            Figure S2

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         4
##$PEAK LABELS=        Si4/Si1    Si3/Si2    Si2/Si3    Si1/Si4       
##$PEAK TSITES=        T2/T1      T4/T3      T3/T4      T1/T2        
##$PEAK POSITIONS=    -111.355   -109.588   -106.771   -105.648   
##$PEAK AREAS=         2.         1.         1.         2.        
##$PEAK WIDTHS=        1.16137    1.2076     1.01273    1.9171    
##$PEAK SHAPES=        1          1          1          1         
##$NUMBERING REF=     Jorda et al. Angew. Chem. Int. Ed., 52, 10458-10462 (2013)
##$ASSIGN REF=        Jorda et al. Angew. Chem. Int. Ed., 52, 10458-10462 (2013) Figure S2
##$ASSIGN METHOD=     relative intensities
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -80.28                
##LASTX=              -139.68               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            1468
##FIRSTY=              0.01597              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -80.28               0.01597              
 -80.32               0.01691              
 -80.36               0.01658              
 -80.4                0.01642              
 -80.44               0.01538              
 -80.48               0.01378              
 -80.52               0.01426              
 -80.56               0.01489              
 -80.6                0.00847              
 -80.64               0.00628              
 -80.68               0.00307              
 -80.72               0.00066              
 -80.76               0.00004              
 -80.8               -0.00216              
 -80.84              -0.00295              
 -80.88              -0.00466              
 -80.92              -0.00431              
 -80.96              -0.00073              
 -81.                -0.00023              
 -81.04               0.00269              
 -81.08               0.00219              
 -81.12               0.00820              
 -81.16               0.01091              
 -81.2                0.01465              
 -81.24               0.01845              
 -81.28               0.01385              
 -81.32               0.01015              
 -81.36               0.00872              
 -81.4                0.00625              
 -81.44               0.00394              
 -81.48               0.00311              
 -81.52               0.00094              
 -81.56              -0.00145              
 -81.6               -0.00381              
 -81.64              -0.00562              
 -81.68              -0.00457              
 -81.72              -0.00302              
 -81.76              -0.00216              
 -81.8                0.00000              
 -81.84               0.00102              
 -81.88               0.00171              
 -81.92               0.00304              
 -81.96               0.00075              
 -82.                -0.00091              
 -82.04              -0.00321              
 -82.08              -0.00443              
 -82.12              -0.00572              
 -82.16              -0.00696              
 -82.2               -0.00806              
 -82.24              -0.00962              
 -82.28              -0.00863              
 -82.32              -0.00624              
 -82.36              -0.00626              
 -82.4               -0.00187              
 -82.44              -0.00127              
 -82.48               0.00133              
 -82.52               0.00283              
 -82.56               0.00547              
 -82.6                0.00643              
 -82.64               0.00947              
 -82.68               0.01334              
 -82.72               0.01267              
 -82.76               0.01215              
 -82.8                0.01168              
 -82.84               0.00934              
 -82.88               0.00929              
 -82.92               0.00843              
 -82.96               0.00818              
 -83.                 0.00811              
 -83.04               0.00793              
 -83.08               0.00789              
 -83.12               0.00735              
 -83.16               0.00648              
 -83.2                0.00537              
 -83.24               0.00380              
 -83.28               0.00315              
 -83.32               0.00302              
 -83.36               0.00288              
 -83.4                0.00417              
 -83.44               0.00503              
 -83.48               0.00429              
 -83.52               0.00397              
 -83.56               0.00344              
 -83.6                0.00259              
 -83.64               0.00132              
 -83.68               0.00011              
 -83.72               0.00012              
 -83.76               0.00005              
 -83.8               -0.00024              
 -83.84              -0.00262              
 -83.88              -0.00267              
 -83.92              -0.00549              
 -83.96              -0.00706              
 -84.                -0.00706              
 -84.04              -0.00750              
 -84.08              -0.00361              
 -84.12               0.00045              
 -84.16               0.00059              
 -84.2                0.00201              
 -84.24               0.00372              
 -84.28               0.00714              
 -84.32               0.00761              
 -84.36               0.01290              
 -84.4                0.01008              
 -84.44               0.00717              
 -84.48               0.00393              
 -84.52               0.00083              
 -84.56              -0.00136              
 -84.6               -0.00550              
 -84.64              -0.00902              
 -84.68              -0.01083              
 -84.72              -0.01231              
 -84.76              -0.00784              
 -84.8               -0.00737              
 -84.84              -0.00523              
 -84.88              -0.00539              
 -84.92              -0.00253              
 -84.96              -0.00015              
 -85.                 0.00041              
 -85.04               0.00101              
 -85.08              -0.00044              
 -85.12              -0.00184              
 -85.16              -0.00302              
 -85.2               -0.00813              
 -85.24              -0.00788              
 -85.28              -0.00878              
 -85.32              -0.00854              
 -85.36              -0.00428              
 -85.4               -0.00293              
 -85.44              -0.00185              
 -85.48              -0.00166              
 -85.52              -0.00015              
 -85.56               0.00160              
 -85.6                0.00013              
 -85.64              -0.00033              
 -85.68              -0.00062              
 -85.72              -0.00226              
 -85.76              -0.00308              
 -85.8               -0.00406              
 -85.84              -0.00295              
 -85.88              -0.00197              
 -85.92              -0.00205              
 -85.96              -0.00191              
 -86.                -0.00326              
 -86.04              -0.00527              
 -86.08              -0.00581              
 -86.12              -0.00692              
 -86.16              -0.00843              
 -86.2               -0.00927              
 -86.24              -0.01018              
 -86.28              -0.00812              
 -86.32              -0.00747              
 -86.36              -0.00509              
 -86.4               -0.00308              
 -86.44              -0.00200              
 -86.48              -0.00047              
 -86.52              -0.00173              
 -86.56              -0.00410              
 -86.6               -0.00437              
 -86.64              -0.00667              
 -86.68              -0.00667              
 -86.72              -0.00828              
 -86.76              -0.00872              
 -86.8               -0.00603              
 -86.84              -0.00476              
 -86.88              -0.00481              
 -86.92              -0.00497              
 -86.96              -0.00237              
 -87.                -0.00021              
 -87.04               0.00175              
 -87.08               0.00729              
 -87.12               0.00807              
 -87.16               0.00868              
 -87.2                0.00850              
 -87.24               0.01008              
 -87.28               0.00742              
 -87.32               0.00604              
 -87.36               0.00428              
 -87.4                0.00265              
 -87.44               0.00183              
 -87.48              -0.00046              
 -87.52              -0.00354              
 -87.56              -0.00539              
 -87.6               -0.00516              
 -87.64              -0.00379              
 -87.68              -0.00317              
 -87.72              -0.00261              
 -87.76              -0.00174              
 -87.8               -0.00299              
 -87.84              -0.00376              
 -87.88              -0.00356              
 -87.92              -0.00413              
 -87.96              -0.00280              
 -88.                -0.00066              
 -88.04              -0.00065              
 -88.08               0.00148              
 -88.12               0.00205              
 -88.16               0.00419              
 -88.2                0.00423              
 -88.24               0.00408              
 -88.28               0.00404              
 -88.32               0.00770              
 -88.36               0.00986              
 -88.4                0.01131              
 -88.44               0.01351              
 -88.48               0.01435              
 -88.52               0.01621              
 -88.56               0.01707              
 -88.6                0.02066              
 -88.64               0.02049              
 -88.68               0.02187              
 -88.72               0.02082              
 -88.76               0.01902              
 -88.8                0.01760              
 -88.84               0.01565              
 -88.88               0.01307              
 -88.92               0.01153              
 -88.96               0.01028              
 -89.                 0.00825              
 -89.04               0.00718              
 -89.08               0.00337              
 -89.12               0.00203              
 -89.16              -0.00540              
 -89.2               -0.00773              
 -89.24              -0.01101              
 -89.28              -0.01235              
 -89.32              -0.01338              
 -89.36              -0.01547              
 -89.4               -0.01569              
 -89.44              -0.01598              
 -89.48              -0.01556              
 -89.52              -0.01358              
 -89.56              -0.01373              
 -89.6               -0.01156              
 -89.64              -0.01171              
 -89.68              -0.00922              
 -89.72              -0.00810              
 -89.76              -0.01022              
 -89.8               -0.01154              
 -89.84              -0.01316              
 -89.88              -0.01462              
 -89.92              -0.01521              
 -89.96              -0.01722              
 -90.                -0.01434              
 -90.04              -0.00853              
 -90.08              -0.00424              
 -90.12              -0.00052              
 -90.16               0.00117              
 -90.2                0.00235              
 -90.24               0.00410              
 -90.28               0.00685              
 -90.32               0.00904              
 -90.36               0.01225              
 -90.4                0.01544              
 -90.44               0.01411              
 -90.48               0.01322              
 -90.52               0.01090              
 -90.56               0.01019              
 -90.6                0.00645              
 -90.64               0.00557              
 -90.68               0.00634              
 -90.72               0.00662              
 -90.76               0.00577              
 -90.8                0.00589              
 -90.84               0.00357              
 -90.88              -0.00067              
 -90.92              -0.00075              
 -90.96              -0.00380              
 -91.                -0.00379              
 -91.04              -0.00685              
 -91.08              -0.00735              
 -91.12              -0.00651              
 -91.16              -0.00679              
 -91.2               -0.00513              
 -91.24              -0.00444              
 -91.28              -0.00318              
 -91.32              -0.00110              
 -91.36               0.00037              
 -91.4                0.00440              
 -91.44               0.00387              
 -91.48               0.00384              
 -91.52               0.00375              
 -91.56               0.00363              
 -91.6                0.00399              
 -91.64               0.00558              
 -91.68               0.00499              
 -91.72               0.00358              
 -91.76               0.00280              
 -91.8                0.00237              
 -91.84               0.00180              
 -91.88              -0.00063              
 -91.92              -0.00102              
 -91.96               0.00114              
 -92.                 0.00169              
 -92.04               0.00448              
 -92.08               0.00550              
 -92.12               0.00660              
 -92.16               0.00754              
 -92.2                0.00847              
 -92.24               0.00989              
 -92.28               0.00952              
 -92.32               0.00818              
 -92.36               0.00813              
 -92.4                0.00730              
 -92.44               0.00802              
 -92.48               0.00947              
 -92.52               0.00937              
 -92.56               0.01057              
 -92.6                0.01079              
 -92.64               0.00797              
 -92.68               0.00647              
 -92.72               0.00647              
 -92.76               0.00534              
 -92.8                0.00340              
 -92.84               0.00151              
 -92.88               0.00039              
 -92.92              -0.00570              
 -92.96              -0.00890              
 -93.                -0.00972              
 -93.04              -0.01126              
 -93.08              -0.01174              
 -93.12              -0.01202              
 -93.16              -0.01351              
 -93.2               -0.01446              
 -93.24              -0.01437              
 -93.28              -0.01449              
 -93.32              -0.01459              
 -93.36              -0.01463              
 -93.4               -0.01472              
 -93.44              -0.01581              
 -93.48              -0.01164              
 -93.52              -0.01046              
 -93.56              -0.00803              
 -93.6               -0.00741              
 -93.64              -0.00510              
 -93.68              -0.00403              
 -93.72               0.00014              
 -93.76               0.00883              
 -93.8                0.00980              
 -93.84               0.02311              
 -93.88               0.02250              
 -93.92               0.02528              
 -93.96               0.02567              
 -94.                 0.02542              
 -94.04               0.02473              
 -94.08               0.02123              
 -94.12               0.01915              
 -94.16               0.01773              
 -94.2                0.01637              
 -94.24               0.01523              
 -94.28               0.00995              
 -94.32               0.00789              
 -94.36               0.00483              
 -94.4                0.00536              
 -94.44               0.00570              
 -94.48               0.00351              
 -94.52               0.00272              
 -94.56               0.00287              
 -94.6                0.00274              
 -94.64               0.00261              
 -94.68               0.00276              
 -94.72               0.00351              
 -94.76               0.00410              
 -94.8                0.00483              
 -94.84               0.00698              
 -94.88               0.00928              
 -94.92               0.00862              
 -94.96               0.00866              
 -95.                 0.00627              
 -95.04               0.00456              
 -95.08               0.00315              
 -95.12               0.00123              
 -95.16               0.00068              
 -95.2               -0.00020              
 -95.24               0.00026              
 -95.28               0.00317              
 -95.32               0.00450              
 -95.36               0.00671              
 -95.4                0.00674              
 -95.44               0.00792              
 -95.48               0.00846              
 -95.52               0.01129              
 -95.56               0.01312              
 -95.6                0.01327              
 -95.64               0.01450              
 -95.68               0.01422              
 -95.72               0.01413              
 -95.76               0.01323              
 -95.8                0.01169              
 -95.84               0.01007              
 -95.88               0.00989              
 -95.92               0.00940              
 -95.96               0.00812              
 -96.                 0.00936              
 -96.04               0.01083              
 -96.08               0.01196              
 -96.12               0.01389              
 -96.16               0.01428              
 -96.2                0.01510              
 -96.24               0.01557              
 -96.28               0.01324              
 -96.32               0.01241              
 -96.36               0.01094              
 -96.4                0.00976              
 -96.44               0.00577              
 -96.48               0.00324              
 -96.52               0.00305              
 -96.56               0.00170              
 -96.6                0.00405              
 -96.64               0.00899              
 -96.68               0.00872              
 -96.72               0.01172              
 -96.76               0.01157              
 -96.8                0.01211              
 -96.84               0.01268              
 -96.88               0.00861              
 -96.92               0.00660              
 -96.96               0.00553              
 -97.                 0.00485              
 -97.04               0.00387              
 -97.08               0.00217              
 -97.12               0.00325              
 -97.16               0.00378              
 -97.2                0.00453              
 -97.24               0.00668              
 -97.28               0.00820              
 -97.32               0.00833              
 -97.36               0.00768              
 -97.4                0.00683              
 -97.44               0.00944              
 -97.48               0.01172              
 -97.52               0.01270              
 -97.56               0.01455              
 -97.6                0.01536              
 -97.64               0.01750              
 -97.68               0.01983              
 -97.72               0.02645              
 -97.76               0.02903              
 -97.8                0.02880              
 -97.84               0.03009              
 -97.88               0.02608              
 -97.92               0.02372              
 -97.96               0.02306              
 -98.                 0.02120              
 -98.04               0.02153              
 -98.08               0.02136              
 -98.12               0.02248              
 -98.16               0.02529              
 -98.2                0.02514              
 -98.24               0.02732              
 -98.28               0.02725              
 -98.32               0.02982              
 -98.36               0.02989              
 -98.4                0.02813              
 -98.44               0.02825              
 -98.48               0.02705              
 -98.52               0.02553              
 -98.56               0.02760              
 -98.6                0.03177              
 -98.64               0.03822              
 -98.68               0.03953              
 -98.72               0.04231              
 -98.76               0.04410              
 -98.8                0.04492              
 -98.84               0.04872              
 -98.88               0.04836              
 -98.92               0.04578              
 -98.96               0.04511              
 -99.                 0.04363              
 -99.04               0.04287              
 -99.08               0.04118              
 -99.12               0.03804              
 -99.16               0.03350              
 -99.2                0.03321              
 -99.24               0.03316              
 -99.28               0.03401              
 -99.32               0.03245              
 -99.36               0.03139              
 -99.4                0.03081              
 -99.44               0.02960              
 -99.48               0.02975              
 -99.52               0.02972              
 -99.56               0.03059              
 -99.6                0.03198              
 -99.64               0.03324              
 -99.68               0.03860              
 -99.72               0.03877              
 -99.76               0.04821              
 -99.8                0.05342              
 -99.84               0.05726              
 -99.88               0.06083              
 -99.92               0.06048              
 -99.96               0.06219              
 -100.                0.06376              
 -100.04              0.06572              
 -100.08              0.06474              
 -100.12              0.06251              
 -100.16              0.06013              
 -100.2               0.05928              
 -100.24              0.05753              
 -100.28              0.05485              
 -100.32              0.05406              
 -100.36              0.05374              
 -100.4               0.05538              
 -100.44              0.05818              
 -100.48              0.05829              
 -100.52              0.06125              
 -100.56              0.06097              
 -100.6               0.06014              
 -100.64              0.06033              
 -100.68              0.05741              
 -100.72              0.05696              
 -100.76              0.05475              
 -100.8               0.05352              
 -100.84              0.04968              
 -100.88              0.04472              
 -100.92              0.04559              
 -100.96              0.04543              
 -101.                0.04517              
 -101.04              0.04287              
 -101.08              0.04215              
 -101.12              0.03993              
 -101.16              0.03967              
 -101.2               0.04371              
 -101.24              0.04619              
 -101.28              0.04776              
 -101.32              0.04972              
 -101.36              0.05109              
 -101.4               0.05227              
 -101.44              0.05441              
 -101.48              0.05957              
 -101.52              0.06147              
 -101.56              0.06071              
 -101.6               0.05989              
 -101.64              0.05918              
 -101.68              0.05798              
 -101.72              0.05571              
 -101.76              0.05456              
 -101.8               0.05518              
 -101.84              0.05563              
 -101.88              0.05545              
 -101.92              0.05556              
 -101.96              0.05629              
 -102.                0.05780              
 -102.04              0.06154              
 -102.08              0.06161              
 -102.12              0.06346              
 -102.16              0.06447              
 -102.2               0.06619              
 -102.24              0.06741              
 -102.28              0.06914              
 -102.32              0.07138              
 -102.36              0.07066              
 -102.4               0.07012              
 -102.44              0.07101              
 -102.48              0.07242              
 -102.52              0.07370              
 -102.56              0.07812              
 -102.6               0.07966              
 -102.64              0.08399              
 -102.68              0.08733              
 -102.72              0.08984              
 -102.76              0.09153              
 -102.8               0.09330              
 -102.84              0.09622              
 -102.88              0.09618              
 -102.92              0.09837              
 -102.96              0.09744              
 -103.                0.09661              
 -103.04              0.09675              
 -103.08              0.09497              
 -103.12              0.09708              
 -103.16              0.09811              
 -103.2               0.09916              
 -103.24              0.10064              
 -103.28              0.1043               
 -103.32              0.10956              
 -103.36              0.11317              
 -103.4               0.12465              
 -103.44              0.12568              
 -103.48              0.13390              
 -103.52              0.13436              
 -103.56              0.13749              
 -103.6               0.13818              
 -103.64              0.14447              
 -103.68              0.14792              
 -103.72              0.15293              
 -103.76              0.16055              
 -103.8               0.16195              
 -103.84              0.16888              
 -103.88              0.16846              
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##END=
