##TITLE=              29Si MAS NMR spectrum of calcined pure silica ITQ-32
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Cantin et al. J. Am. Chem. Soc., 127, 11560-11561 (2005) Figure S4
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 14:35:01
##SOURCE REFERENCE=   IHW-29Si-Cantin-2005
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              IHW
##NAMES=              ITQ-32
##SAMPLE DESCRIPTION= ITQ-32, calcined

$$Bibliographic information 
##$AUTHORS=           Cantin, A., Corma, A., Leiva, S., Rey, F., Rius, J., Valencia, S.
##$TITLE=             Synthesis and structure of the bidimensional zeolite ITQ-32 with small and large pores
##$JOURNAL=           Journal of the American Chemical Society
##$VOLUME=            127
##$PAGES=             11560-11561
##$YEAR=              2005
##$DOI=               10.1021/ja053040h
##$FIGURE=            Figure S4

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         9
##$PEAK LABELS=        A          B          C          D          E          F          G          H          I         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -116.979   -115.627   -115.314   -115.114   -114.689   -113.466   -111.423   -106.283   -103.823   
##$PEAK AREAS=         2.         1.         2.         2.         1.         2.         1.         2.         1.        
##$PEAK WIDTHS=        1.548      1.18161    1.18161    1.18161    1.18161    1.11614    0.94777    0.90759    0.72492   
##$PEAK SHAPES=        1          1          1          1          1          1          1          1          1         
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -100.13               
##LASTX=              -121.92               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            2180
##FIRSTY=              0.05929              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -100.13              0.05929              
 -100.14              0.05344              
 -100.15              0.05403              
 -100.16              0.05388              
 -100.17              0.05372              
 -100.18              0.05485              
 -100.19              0.05586              
 -100.2               0.05666              
 -100.21              0.06078              
 -100.22              0.06162              
 -100.23              0.06149              
 -100.24              0.06150              
 -100.25              0.06150              
 -100.26              0.06150              
 -100.27              0.06150              
 -100.28              0.06150              
 -100.29              0.06150              
 -100.3               0.06150              
 -100.31              0.06150              
 -100.32              0.06150              
 -100.33              0.06150              
 -100.34              0.06150              
 -100.35              0.06150              
 -100.36              0.06150              
 -100.37              0.06150              
 -100.38              0.06150              
 -100.39              0.06150              
 -100.4               0.06150              
 -100.41              0.06150              
 -100.42              0.06150              
 -100.43              0.06150              
 -100.44              0.06150              
 -100.45              0.06149              
 -100.46              0.06153              
 -100.47              0.06143              
 -100.48              0.06339              
 -100.49              0.06547              
 -100.5               0.06734              
 -100.51              0.06708              
 -100.52              0.06778              
 -100.53              0.06936              
 -100.54              0.06892              
 -100.55              0.07010              
 -100.56              0.07226              
 -100.57              0.07448              
 -100.58              0.07488              
 -100.59              0.07484              
 -100.6               0.07482              
 -100.61              0.07692              
 -100.62              0.07863              
 -100.63              0.07936              
 -100.64              0.08296              
 -100.65              0.08177              
 -100.66              0.07942              
 -100.67              0.07866              
 -100.68              0.07758              
 -100.69              0.07515              
 -100.7               0.07479              
 -100.71              0.07482              
 -100.72              0.07484              
 -100.73              0.07278              
 -100.74              0.07070              
 -100.75              0.06895              
 -100.76              0.06928              
 -100.77              0.06845              
 -100.78              0.06668              
 -100.79              0.06932              
 -100.8               0.07238              
 -100.81              0.07444              
 -100.82              0.07489              
 -100.83              0.07482              
 -100.84              0.07483              
 -100.85              0.07483              
 -100.86              0.07483              
 -100.87              0.07483              
 -100.88              0.07483              
 -100.89              0.07483              
 -100.9               0.07483              
 -100.91              0.07483              
 -100.92              0.07483              
 -100.93              0.07484              
 -100.94              0.07480              
 -100.95              0.07491              
 -100.96              0.07297              
 -100.97              0.07089              
 -100.98              0.06899              
 -100.99              0.06925              
 -101.                0.06857              
 -101.01              0.06698              
 -101.02              0.06742              
 -101.03              0.06625              
 -101.04              0.06410              
 -101.05              0.06186              
 -101.06              0.06148              
 -101.07              0.06143              
 -101.08              0.06336              
 -101.09              0.06544              
 -101.1               0.06734              
 -101.11              0.06708              
 -101.12              0.06776              
 -101.13              0.06936              
 -101.14              0.06892              
 -101.15              0.07007              
 -101.16              0.07223              
 -101.17              0.07447              
 -101.18              0.07485              
 -101.19              0.07492              
 -101.2               0.07297              
 -101.21              0.07082              
 -101.22              0.06696              
 -101.23              0.06737              
 -101.24              0.06675              
 -101.25              0.06456              
 -101.26              0.06236              
 -101.27              0.06136              
 -101.28              0.06153              
 -101.29              0.0615               
 -101.3               0.06150              
 -101.31              0.06150              
 -101.32              0.06150              
 -101.33              0.06150              
 -101.34              0.06150              
 -101.35              0.06150              
 -101.36              0.06150              
 -101.37              0.06149              
 -101.38              0.06154              
 -101.39              0.06134              
 -101.4               0.06261              
 -101.41              0.06477              
 -101.42              0.06696              
 -101.43              0.06728              
 -101.44              0.06718              
 -101.45              0.06917              
 -101.46              0.06919              
 -101.47              0.07188              
 -101.48              0.07544              
 -101.49              0.07826              
 -101.5               0.08090              
 -101.51              0.08051              
 -101.52              0.08037              
 -101.53              0.08192              
 -101.54              0.08269              
 -101.55              0.08069              
 -101.56              0.08054              
 -101.57              0.08056              
 -101.58              0.08034              
 -101.59              0.07853              
 -101.6               0.07832              
 -101.61              0.07571              
 -101.62              0.07538              
 -101.63              0.07807              
 -101.64              0.07854              
 -101.65              0.08005              
 -101.66              0.08061              
 -101.67              0.08057              
 -101.68              0.08050              
 -101.69              0.08244              
 -101.7               0.08039              
 -101.71              0.08058              
 -101.72              0.08066              
 -101.73              0.07983              
 -101.74              0.07857              
 -101.75              0.07786              
 -101.76              0.07518              
 -101.77              0.07597              
 -101.78              0.07847              
 -101.79              0.07856              
 -101.8               0.08050              
 -101.81              0.08053              
 -101.82              0.08052              
 -101.83              0.08076              
 -101.84              0.08342              
 -101.85              0.08799              
 -101.86              0.09036              
 -101.87              0.09005              
 -101.88              0.08986              
 -101.89              0.09154              
 -101.9               0.09189              
 -101.91              0.09369              
 -101.92              0.09389              
 -101.93              0.09388              
 -101.94              0.09387              
 -101.95              0.09388              
 -101.96              0.09387              
 -101.97              0.09388              
 -101.98              0.09387              
 -101.99              0.09387              
 -102.                0.09387              
 -102.01              0.09388              
 -102.02              0.09387              
 -102.03              0.09388              
 -102.04              0.09387              
 -102.05              0.09386              
 -102.06              0.09404              
 -102.07              0.09612              
 -102.08              0.09882              
 -102.09              0.10190              
 -102.1               0.10125              
 -102.11              0.10242              
 -102.12              0.10457              
 -102.13              0.10680              
 -102.14              0.10727              
 -102.15              0.1072               
 -102.16              0.10721              
 -102.17              0.10721              
 -102.18              0.10721              
 -102.19              0.10719              
 -102.2               0.10730              
 -102.21              0.10664              
 -102.22              0.10444              
 -102.23              0.10217              
 -102.24              0.10157              
 -102.25              0.10011              
 -102.26              0.09950              
 -102.27              0.09959              
 -102.28              0.09960              
 -102.29              0.09964              
 -102.3               0.10161              
 -102.31              0.10145              
 -102.32              0.10156              
 -102.33              0.10611              
 -102.34              0.11266              
 -102.35              0.11272              
 -102.36              0.11415              
 -102.37              0.11493              
 -102.38              0.11486              
 -102.39              0.11467              
 -102.4               0.11672              
 -102.41              0.11477              
 -102.42              0.11485              
 -102.43              0.11489              
 -102.44              0.11432              
 -102.45              0.11283              
 -102.46              0.1123               
 -102.47              0.10982              
 -102.48              0.10885              
 -102.49              0.11032              
 -102.5               0.11271              
 -102.51              0.11283              
 -102.52              0.11476              
 -102.53              0.11480              
 -102.54              0.11493              
 -102.55              0.11740              
 -102.56              0.12162              
 -102.57              0.12587              
 -102.58              0.12912              
 -102.59              0.13124              
 -102.6               0.13192              
 -102.61              0.13321              
 -102.62              0.13524              
 -102.63              0.13904              
 -102.64              0.14319              
 -102.65              0.14729              
 -102.66              0.14929              
 -102.67              0.15145              
 -102.68              0.15308              
 -102.69              0.15275              
 -102.7               0.15363              
 -102.71              0.15582              
 -102.72              0.15805              
 -102.73              0.15871              
 -102.74              0.15864              
 -102.75              0.15853              
 -102.76              0.1604               
 -102.77              0.16245              
 -102.78              0.16257              
 -102.79              0.16450              
 -102.8               0.16431              
 -102.81              0.16423              
 -102.82              0.16503              
 -102.83              0.16725              
 -102.84              0.16945              
 -102.85              0.17019              
 -102.86              0.16989              
 -102.87              0.17165              
 -102.88              0.17376              
 -102.89              0.17582              
 -102.9               0.17789              
 -102.91              0.17986              
 -102.92              0.18249              
 -102.93              0.18606              
 -102.94              0.18867              
 -102.95              0.19306              
 -102.96              0.19712              
 -102.97              0.20126              
 -102.98              0.20538              
 -102.99              0.20950              
 -103.                0.21364              
 -103.01              0.21777              
 -103.02              0.22163              
 -103.03              0.22148              
 -103.04              0.22491              
 -103.05              0.23000              
 -103.06              0.23259              
 -103.07              0.23581              
 -103.08              0.23900              
 -103.09              0.24196              
 -103.1               0.24386              
 -103.11              0.24596              
 -103.12              0.24801              
 -103.13              0.25007              
 -103.14              0.25226              
 -103.15              0.25648              
 -103.16              0.26068              
 -103.17              0.26416              
 -103.18              0.26625              
 -103.19              0.26739              
 -103.2               0.27497              
 -103.21              0.28046              
 -103.22              0.28263              
 -103.23              0.29416              
 -103.24              0.30448              
 -103.25              0.32074              
 -103.26              0.32648              
 -103.27              0.33132              
 -103.28              0.33916              
 -103.29              0.34665              
 -103.3               0.35519              
 -103.31              0.35816              
 -103.32              0.36501              
 -103.33              0.37281              
 -103.34              0.38607              
 -103.35              0.39600              
 -103.36              0.40011              
 -103.37              0.41023              
 -103.38              0.42225              
 -103.39              0.42500              
 -103.4               0.43498              
 -103.41              0.45764              
 -103.42              0.45744              
 -103.43              0.47078              
 -103.44              0.48798              
 -103.45              0.49110              
 -103.46              0.50975              
 -103.47              0.52515              
 -103.48              0.52989              
 -103.49              0.53600              
 -103.5               0.56196              
 -103.51              0.56402              
 -103.52              0.57216              
 -103.53              0.59338              
 -103.54              0.60145              
 -103.55              0.61350              
 -103.56              0.63752              
 -103.57              0.64426              
 -103.58              0.65993              
 -103.59              0.68045              
 -103.6               0.68635              
 -103.61              0.69234              
 -103.62              0.74210              
 -103.63              0.74267              
 -103.64              0.75044              
 -103.65              0.77254              
 -103.66              0.78753              
 -103.67              0.79536              
 -103.68              0.82218              
 -103.69              0.83565              
 -103.7               0.83390              
 -103.71              0.87356              
 -103.72              0.88397              
 -103.73              0.89571              
 -103.74              0.90232              
 -103.75              0.91910              
 -103.76              0.92666              
 -103.77              0.93484              
 -103.78              0.94747              
 -103.79              0.94726              
 -103.8               0.96035              
 -103.81              0.96822              
 -103.82              0.96923              
 -103.83              0.97150              
 -103.84              0.97049              
 -103.85              0.95643              
 -103.86              0.95477              
 -103.87              0.95100              
 -103.88              0.93966              
 -103.89              0.93581              
 -103.9               0.93467              
 -103.91              0.91266              
 -103.92              0.88919              
 -103.93              0.88902              
 -103.94              0.87298              
 -103.95              0.86169              
 -103.96              0.85838              
 -103.97              0.83443              
 -103.98              0.81293              
 -103.99              0.80817              
 -104.                0.78322              
 -104.01              0.76070              
 -104.02              0.76029              
 -104.03              0.74863              
 -104.04              0.73098              
 -104.05              0.72687              
 -104.06              0.70652              
 -104.07              0.68041              
 -104.08              0.67520              
 -104.09              0.65742              
 -104.1               0.63552              
 -104.11              0.63328              
 -104.12              0.62259              
 -104.13              0.59572              
 -104.14              0.59468              
 -104.15              0.58870              
 -104.16              0.56823              
 -104.17              0.54665              
 -104.18              0.54051              
 -104.19              0.53167              
 -104.2               0.52278              
 -104.21              0.51468              
 -104.22              0.49683              
 -104.23              0.49517              
 -104.24              0.48880              
 -104.25              0.47981              
 -104.26              0.46354              
 -104.27              0.45310              
 -104.28              0.44872              
 -104.29              0.44498              
 -104.3               0.43495              
 -104.31              0.42926              
 -104.32              0.42607              
 -104.33              0.40998              
 -104.34              0.40602              
 -104.35              0.40155              
 -104.36              0.39472              
 -104.37              0.38742              
 -104.38              0.38373              
 -104.39              0.37957              
 -104.4               0.37512              
 -104.41              0.37232              
 -104.42              0.35956              
 -104.43              0.35463              
 -104.44              0.35323              
 -104.45              0.34715              
 -104.46              0.34304              
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 -104.48              0.33427              
 -104.49              0.32915              
 -104.5               0.32651              
 -104.51              0.31745              
 -104.52              0.31000              
 -104.53              0.30799              
 -104.54              0.30424              
 -104.55              0.30172              
 -104.56              0.29967              
 -104.57              0.29765              
 -104.58              0.29161              
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 -104.62              0.28891              
 -104.63              0.28351              
 -104.64              0.27698              
 -104.65              0.27428              
 -104.66              0.27133              
 -104.67              0.26942              
 -104.68              0.26733              
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 -105.1               0.25709              
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 -105.28              0.29325              
 -105.29              0.29758              
 -105.3               0.30161              
 -105.31              0.30384              
 -105.32              0.30772              
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 -105.35              0.31855              
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 -105.37              0.32798              
 -105.38              0.33315              
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 -105.4               0.34092              
 -105.41              0.34334              
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 -105.43              0.34781              
 -105.44              0.35154              
 -105.45              0.35336              
 -105.46              0.36104              
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 -105.48              0.37222              
 -105.49              0.37979              
 -105.5               0.38792              
 -105.51              0.39214              
 -105.52              0.39628              
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 -105.54              0.40435              
 -105.55              0.41026              
 -105.56              0.43007              
 -105.57              0.43637              
 -105.58              0.44265              
 -105.59              0.44961              
 -105.6               0.45824              
 -105.61              0.46528              
 -105.62              0.47020              
 -105.63              0.47324              
 -105.64              0.48817              
 -105.65              0.50130              
 -105.66              0.50606              
 -105.67              0.52835              
 -105.68              0.53444              
 -105.69              0.53946              
 -105.7               0.54922              
 -105.71              0.55704              
 -105.72              0.56112              
 -105.73              0.57894              
 -105.74              0.58917              
 -105.75              0.59074              
 -105.76              0.60995              
 -105.77              0.61943              
 -105.78              0.62404              
 -105.79              0.64728              
 -105.8               0.66030              
 -105.81              0.67221              
 -105.82              0.69835              
 -105.83              0.70628              
 -105.84              0.70480              
 -105.85              0.74079              
 -105.86              0.76359              
 -105.87              0.76400              
 -105.88              0.78405              
 -105.89              0.80964              
 -105.9               0.81702              
 -105.91              0.86258              
 -105.92              0.88263              
 -105.93              0.88175              
 -105.94              0.90819              
 -105.95              0.95156              
 -105.96              0.94872              
 -105.97              0.97302              
 -105.98              1.00293              
 -105.99              1.00846              
 -106.                1.04978              
 -106.01              1.09816              
 -106.02              1.13059              
 -106.03              1.14224              
 -106.04              1.16597              
 -106.05              1.18182              
 -106.06              1.21632              
 -106.07              1.23188              
 -106.08              1.26795              
 -106.09              1.27729              
 -106.1               1.31475              
 -106.11              1.34802              
 -106.12              1.3803               
 -106.13              1.38897              
 -106.14              1.39624              
 -106.15              1.44366              
 -106.16              1.44595              
 -106.17              1.45536              
 -106.18              1.47489              
 -106.19              1.48941              
 -106.2               1.4899               
 -106.21              1.50609              
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##END=
