##TITLE=              29Si MAS NMR spectrum of calcined pure silica ITQ-12
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Khay et al. PCCP, 15, 20320-20325 (2013) Figure 6
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 14:38:58
##SOURCE REFERENCE=   ITW-29Si-Khay-2013
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              ITW
##NAMES=              ITQ-12
##SAMPLE DESCRIPTION= ITQ-12, calcined

$$Bibliographic information 
##$AUTHORS=           Khay, I., Tzanis, L., Daou, T.J., Nouali, H., Ryzhikov, A., Patarin, J.
##$TITLE=             Energetic behavior of the pure silica ITQ-12 (ITW) zeolite under high pressure water intrusion
##$JOURNAL=           Physical Chemistry Chemical Physics
##$VOLUME=            15
##$PAGES=             20320-20325
##$YEAR=              2013
##$DOI=               10.1039/c3cp53570c
##$FIGURE=            Figure 6

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         6
##$PEAK LABELS=        A          B          C          D          E          F         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -118.317   -114.533   -112.255   -111.868   -111.051   -110.055   
##$PEAK AREAS=         1.         1.         1.         1.         1.         1.        
##$PEAK WIDTHS=        0.43623    0.74267    0.44525    0.45285    0.43315    0.48804   
##$PEAK SHAPES=        0.40189    0.40189    0.40189    0.40189    0.40189    0.40189   
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 59.6
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     4000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -80.                  
##LASTX=              -130.                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            1001
##FIRSTY=             -0.00222              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -80.                -0.00222              
 -80.05              -0.00476              
 -80.1               -0.00754              
 -80.15              -0.00782              
 -80.2               -0.00387              
 -80.25              -0.00484              
 -80.3               -0.00287              
 -80.35              -0.00231              
 -80.4               -0.00021              
 -80.45               0.00005              
 -80.5               -0.00006              
 -80.55              -0.00482              
 -80.6               -0.00836              
 -80.65              -0.00817              
 -80.7                0.00203              
 -80.75               0.00439              
 -80.8                0.00922              
 -80.85               0.00469              
 -80.9               -0.00728              
 -80.95              -0.01784              
 -81.                -0.02060              
 -81.05              -0.02763              
 -81.1               -0.02679              
 -81.15              -0.02243              
 -81.2               -0.01686              
 -81.25              -0.01243              
 -81.3               -0.00424              
 -81.35               0.00151              
 -81.4                0.00433              
 -81.45               0.00679              
 -81.5                0.00930              
 -81.55               0.01155              
 -81.6                0.01114              
 -81.65               0.00676              
 -81.7               -0.00005              
 -81.75              -0.00493              
 -81.8               -0.00844              
 -81.85              -0.01062              
 -81.9               -0.01354              
 -81.95              -0.01126              
 -82.                -0.01359              
 -82.05              -0.01037              
 -82.1               -0.00594              
 -82.15              -0.00332              
 -82.2               -0.00301              
 -82.25              -0.00510              
 -82.3               -0.00144              
 -82.35               0.00348              
 -82.4                0.01077              
 -82.45               0.01591              
 -82.5                0.02340              
 -82.55               0.02716              
 -82.6                0.01945              
 -82.65               0.00807              
 -82.7                0.00194              
 -82.75              -0.00094              
 -82.8               -0.00718              
 -82.85              -0.00962              
 -82.9               -0.00474              
 -82.95              -0.00448              
 -83.                -0.00709              
 -83.05              -0.00869              
 -83.1               -0.00673              
 -83.15              -0.00507              
 -83.2               -0.00132              
 -83.25              -0.00501              
 -83.3               -0.00850              
 -83.35              -0.01085              
 -83.4               -0.01332              
 -83.45              -0.01579              
 -83.5               -0.01136              
 -83.55              -0.00385              
 -83.6               -0.00448              
 -83.65              -0.00542              
 -83.7               -0.00634              
 -83.75              -0.00073              
 -83.8               -0.00332              
 -83.85              -0.00433              
 -83.9               -0.00874              
 -83.95              -0.01139              
 -84.                -0.01628              
 -84.05              -0.01850              
 -84.1               -0.01591              
 -84.15              -0.01008              
 -84.2               -0.00599              
 -84.25              -0.00639              
 -84.3               -0.00155              
 -84.35               0.00023              
 -84.4                0.00013              
 -84.45              -0.00480              
 -84.5               -0.00906              
 -84.55              -0.01008              
 -84.6               -0.01310              
 -84.65              -0.01190              
 -84.7               -0.01388              
 -84.75              -0.01323              
 -84.8               -0.01531              
 -84.85              -0.01445              
 -84.9               -0.00460              
 -84.95              -0.00690              
 -85.                -0.00664              
 -85.05              -0.00669              
 -85.1               -0.00719              
 -85.15              -0.01115              
 -85.2               -0.01514              
 -85.25              -0.01611              
 -85.3               -0.01393              
 -85.35              -0.01347              
 -85.4               -0.01352              
 -85.45              -0.01634              
 -85.5               -0.01901              
 -85.55              -0.00727              
 -85.6               -0.00612              
 -85.65              -0.00342              
 -85.7                0.00017              
 -85.75               0.00595              
 -85.8                0.00675              
 -85.85               0.00905              
 -85.9                0.00686              
 -85.95               0.00686              
 -86.                 0.00717              
 -86.05               0.00961              
 -86.1                0.00753              
 -86.15               0.00290              
 -86.2                0.00269              
 -86.25              -0.00090              
 -86.3               -0.00266              
 -86.35               0.00182              
 -86.4                0.00688              
 -86.45               0.00990              
 -86.5                0.01941              
 -86.55               0.02021              
 -86.6                0.02171              
 -86.65               0.02077              
 -86.7                0.01647              
 -86.75               0.01446              
 -86.8                0.01016              
 -86.85               0.00458              
 -86.9                0.00920              
 -86.95               0.00918              
 -87.                 0.01212              
 -87.05               0.01342              
 -87.1                0.00936              
 -87.15               0.00550              
 -87.2                0.00302              
 -87.25               0.00217              
 -87.3                0.00247              
 -87.35               0.00023              
 -87.4               -0.00225              
 -87.45              -0.00190              
 -87.5                0.00014              
 -87.55               0.00074              
 -87.6                0.00245              
 -87.65               0.00280              
 -87.7               -0.00155              
 -87.75              -0.00994              
 -87.8               -0.01339              
 -87.85              -0.01356              
 -87.9               -0.01366              
 -87.95              -0.01533              
 -88.                -0.00681              
 -88.05              -0.00131              
 -88.1                0.00236              
 -88.15               0.00435              
 -88.2                0.00822              
 -88.25               0.00439              
 -88.3               -0.00198              
 -88.35              -0.00217              
 -88.4               -0.00459              
 -88.45              -0.00400              
 -88.5                0.00184              
 -88.55               0.00344              
 -88.6                0.00623              
 -88.65               0.01232              
 -88.7                0.01102              
 -88.75               0.01305              
 -88.8                0.01577              
 -88.85               0.01592              
 -88.9                0.01581              
 -88.95               0.01323              
 -89.                 0.01047              
 -89.05               0.00404              
 -89.1               -0.00126              
 -89.15              -0.00461              
 -89.2               -0.00994              
 -89.25              -0.01360              
 -89.3               -0.00956              
 -89.35              -0.00226              
 -89.4                0.01204              
 -89.45               0.01083              
 -89.5                0.00839              
 -89.55               0.00656              
 -89.6                0.00759              
 -89.65               0.01208              
 -89.7                0.01402              
 -89.75               0.01207              
 -89.8                0.00717              
 -89.85               0.00455              
 -89.9               -0.00296              
 -89.95              -0.00673              
 -90.                -0.00312              
 -90.05               0.00206              
 -90.1                0.00615              
 -90.15               0.00680              
 -90.2                0.00741              
 -90.25               0.00266              
 -90.3                0.00645              
 -90.35               0.00916              
 -90.4                0.01172              
 -90.45               0.01387              
 -90.5                0.01321              
 -90.55               0.00942              
 -90.6                0.00550              
 -90.65               0.00300              
 -90.7                0.00227              
 -90.75               0.00217              
 -90.8                0.00448              
 -90.85               0.00456              
 -90.9                0.00489              
 -90.95               0.00669              
 -91.                 0.00373              
 -91.05               0.00123              
 -91.1               -0.00028              
 -91.15               0.00138              
 -91.2                0.00418              
 -91.25               0.00472              
 -91.3                0.00254              
 -91.35              -0.00229              
 -91.4               -0.00238              
 -91.45              -0.00477              
 -91.5               -0.00407              
 -91.55              -0.00637              
 -91.6               -0.01040              
 -91.65              -0.01309              
 -91.7               -0.01295              
 -91.75              -0.01966              
 -91.8               -0.01824              
 -91.85              -0.01334              
 -91.9               -0.01061              
 -91.95              -0.00588              
 -92.                -0.00371              
 -92.05              -0.00103              
 -92.1                0.00103              
 -92.15               0.00575              
 -92.2                0.00666              
 -92.25               0.01087              
 -92.3                0.01358              
 -92.35               0.01843              
 -92.4                0.02120              
 -92.45               0.02539              
 -92.5                0.02496              
 -92.55               0.02430              
 -92.6                0.01959              
 -92.65               0.00752              
 -92.7                0.00259              
 -92.75              -0.00157              
 -92.8               -0.00671              
 -92.85              -0.00661              
 -92.9               -0.00355              
 -92.95               0.00041              
 -93.                 0.00040              
 -93.05               0.00493              
 -93.1                0.00683              
 -93.15               0.00963              
 -93.2                0.01541              
 -93.25               0.01593              
 -93.3                0.01590              
 -93.35               0.01089              
 -93.4                0.00555              
 -93.45              -0.00166              
 -93.5               -0.00574              
 -93.55              -0.00661              
 -93.6               -0.00826              
 -93.65              -0.00785              
 -93.7               -0.00291              
 -93.75              -0.00005              
 -93.8                0.00000              
 -93.85              -0.00484              
 -93.9               -0.00762              
 -93.95              -0.01204              
 -94.                -0.00918              
 -94.05              -0.00665              
 -94.1               -0.00437              
 -94.15               0.00161              
 -94.2                0.00224              
 -94.25               0.00452              
 -94.3                0.00217              
 -94.35              -0.00266              
 -94.4               -0.00479              
 -94.45              -0.00314              
 -94.5                0.00153              
 -94.55               0.01071              
 -94.6                0.01956              
 -94.65               0.02212              
 -94.7                0.02467              
 -94.75               0.02513              
 -94.8                0.02031              
 -94.85               0.01723              
 -94.9                0.00684              
 -94.95               0.00144              
 -95.                -0.00204              
 -95.05              -0.00499              
 -95.1               -0.00323              
 -95.15               0.00123              
 -95.2                0.00459              
 -95.25               0.00242              
 -95.3               -0.00011              
 -95.35              -0.00205              
 -95.4                0.00040              
 -95.45              -0.00033              
 -95.5                0.00199              
 -95.55               0.00621              
 -95.6                0.00800              
 -95.65               0.01299              
 -95.7                0.01346              
 -95.75               0.01811              
 -95.8                0.01813              
 -95.85               0.01447              
 -95.9                0.00589              
 -95.95               0.00771              
 -96.                 0.01049              
 -96.05               0.01109              
 -96.1                0.01447              
 -96.15               0.01651              
 -96.2                0.01178              
 -96.25               0.00916              
 -96.3                0.00175              
 -96.35              -0.00282              
 -96.4               -0.00437              
 -96.45               0.00010              
 -96.5                0.00080              
 -96.55              -0.00503              
 -96.6               -0.01002              
 -96.65              -0.01324              
 -96.7               -0.01369              
 -96.75              -0.00896              
 -96.8               -0.00172              
 -96.85               0.00023              
 -96.9               -0.00058              
 -96.95              -0.00244              
 -97.                -0.00211              
 -97.05              -0.00233              
 -97.1               -0.00094              
 -97.15               0.00392              
 -97.2                0.00657              
 -97.25               0.01143              
 -97.3                0.01150              
 -97.35               0.01410              
 -97.4                0.01742              
 -97.45               0.02090              
 -97.5                0.01993              
 -97.55               0.01268              
 -97.6                0.00412              
 -97.65              -0.00367              
 -97.7               -0.00457              
 -97.75              -0.00206              
 -97.8                0.00261              
 -97.85               0.00213              
 -97.9                0.00293              
 -97.95               0.00561              
 -98.                 0.00814              
 -98.05               0.00970              
 -98.1                0.00573              
 -98.15               0.00265              
 -98.2                0.00010              
 -98.25               0.00253              
 -98.3                0.00732              
 -98.35               0.00974              
 -98.4                0.01153              
 -98.45               0.01160              
 -98.5                0.00951              
 -98.55               0.00209              
 -98.6               -0.00188              
 -98.65              -0.00400              
 -98.7               -0.00879              
 -98.75              -0.01101              
 -98.8               -0.00382              
 -98.85              -0.00081              
 -98.9                0.00667              
 -98.95               0.01052              
 -99.                 0.01081              
 -99.05               0.00466              
 -99.1               -0.00158              
 -99.15              -0.00235              
 -99.2               -0.00211              
 -99.25              -0.00400              
 -99.3                0.00838              
 -99.35               0.01205              
 -99.4                0.01401              
 -99.45               0.01266              
 -99.5                0.00971              
 -99.55              -0.00151              
 -99.6               -0.00486              
 -99.65              -0.00457              
 -99.7               -0.00220              
 -99.75              -0.00455              
 -99.8               -0.00489              
 -99.85              -0.00601              
 -99.9               -0.00029              
 -99.95               0.00477              
 -100.                0.00809              
 -100.05              0.01245              
 -100.1               0.01401              
 -100.15              0.01157              
 -100.2               0.01139              
 -100.25              0.01365              
 -100.3               0.01455              
 -100.35              0.01750              
 -100.4               0.01245              
 -100.45              0.00939              
 -100.5               0.00392              
 -100.55              0.00031              
 -100.6               0.00160              
 -100.65              0.00652              
 -100.7               0.00914              
 -100.75              0.00895              
 -100.8               0.00627              
 -100.85              0.00421              
 -100.9               0.00593              
 -100.95              0.01261              
 -101.                0.00966              
 -101.05              0.00506              
 -101.1               0.00090              
 -101.15             -0.00404              
 -101.2              -0.01139              
 -101.25             -0.01072              
 -101.3              -0.00612              
 -101.35             -0.00289              
 -101.4               0.00030              
 -101.45              0.00119              
 -101.5               0.00252              
 -101.55              0.00229              
 -101.6               0.00232              
 -101.65              0.00234              
 -101.7               0.00238              
 -101.75              0.00502              
 -101.8               0.00693              
 -101.85              0.00738              
 -101.9               0.01034              
 -101.95              0.01166              
 -102.                0.01025              
 -102.05              0.00560              
 -102.1               0.00401              
 -102.15              0.01118              
 -102.2               0.01392              
 -102.25              0.02134              
 -102.3               0.02205              
 -102.35              0.01564              
 -102.4               0.00911              
 -102.45              0.00418              
 -102.5               0.00055              
 -102.55             -0.00020              
 -102.6               0.00209              
 -102.65              0.00235              
 -102.7               0.00256              
 -102.75              0.00736              
 -102.8               0.01041              
 -102.85              0.01359              
 -102.9               0.00924              
 -102.95              0.00418              
 -103.                0.00010              
 -103.05              0.00335              
 -103.1               0.00872              
 -103.15              0.01354              
 -103.2               0.02305              
 -103.25              0.02295              
 -103.3               0.02480              
 -103.35              0.02169              
 -103.4               0.01938              
 -103.45              0.01676              
 -103.5               0.01458              
 -103.55              0.00996              
 -103.6               0.00704              
 -103.65              0.00459              
 -103.7               0.00210              
 -103.75             -0.00045              
 -103.8              -0.00247              
 -103.85             -0.00156              
 -103.9               0.00186              
 -103.95             -0.00027              
 -104.               -0.00286              
 -104.05              0.00134              
 -104.1               0.00657              
 -104.15              0.00916              
 -104.2               0.01136              
 -104.25              0.00841              
 -104.3               0.00703              
 -104.35              0.01131              
 -104.4               0.01375              
 -104.45              0.01518              
 -104.5               0.01467              
 -104.55              0.01006              
 -104.6               0.00467              
 -104.65              0.00689              
 -104.7               0.00715              
 -104.75              0.01259              
 -104.8               0.01711              
 -104.85              0.01742              
 -104.9               0.01545              
 -104.95              0.01738              
 -105.                0.01952              
 -105.05              0.02468              
 -105.1               0.02088              
 -105.15              0.01345              
 -105.2               0.01126              
 -105.25              0.01182              
 -105.3               0.00890              
 -105.35              0.00561              
 -105.4               0.01119              
 -105.45              0.01001              
 -105.5               0.00763              
 -105.55              0.00425              
 -105.6               0.01270              
 -105.65              0.01598              
 -105.7               0.01883              
 -105.75              0.01918              
 -105.8               0.01222              
 -105.85              0.01060              
 -105.9               0.00695              
 -105.95             -0.00010              
 -106.               -0.00448              
 -106.05             -0.00253              
 -106.1              -0.00002              
 -106.15              0.00500              
 -106.2               0.01285              
 -106.25              0.01825              
 -106.3               0.01496              
 -106.35              0.01191              
 -106.4               0.00567              
 -106.45              0.00723              
 -106.5               0.01263              
 -106.55              0.01794              
 -106.6               0.01598              
 -106.65              0.01094              
 -106.7               0.00644              
 -106.75              0.00299              
 -106.8               0.00135              
 -106.85              0.00490              
 -106.9               0.00647              
 -106.95              0.01447              
 -107.                0.01586              
 -107.05              0.01984              
 -107.1               0.02497              
 -107.15              0.02482              
 -107.2               0.02203              
 -107.25              0.01613              
 -107.3               0.00955              
 -107.35              0.01113              
 -107.4               0.01541              
 -107.45              0.01617              
 -107.5               0.01412              
 -107.55              0.01162              
 -107.6               0.00912              
 -107.65              0.01172              
 -107.7               0.01399              
 -107.75              0.01745              
 -107.8               0.02075              
 -107.85              0.02122              
 -107.9               0.02467              
 -107.95              0.02319              
 -108.                0.02440              
 -108.05              0.02713              
 -108.1               0.02964              
 -108.15              0.03395              
 -108.2               0.02826              
 -108.25              0.02884              
 -108.3               0.03048              
 -108.35              0.02587              
 -108.4               0.02276              
 -108.45              0.02762              
 -108.5               0.03171              
 -108.55              0.03181              
 -108.6               0.03186              
 -108.65              0.03715              
 -108.7               0.04097              
 -108.75              0.04725              
 -108.8               0.05344              
 -108.85              0.04984              
 -108.9               0.04572              
 -108.95              0.04086              
 -109.                0.04243              
 -109.05              0.04959              
 -109.1               0.05456              
 -109.15              0.05739              
 -109.2               0.06589              
 -109.25              0.07490              
 -109.3               0.07740              
 -109.35              0.08676              
 -109.4               0.11979              
 -109.45              0.13748              
 -109.5               0.14054              
 -109.55              0.15057              
 -109.6               0.23309              
 -109.65              0.33480              
 -109.7               0.43751              
 -109.75              0.58783              
 -109.8               0.77478              
 -109.85              1.05662              
 -109.9               1.28736              
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##END=
