##TITLE=              29Si MAS NMR spectrum of calcined dealuminated ZSM-11 at 302K
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Fyfe et al. J. Phys. Chem, 95, 3747-3751 (1991) Figure 3a
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 15:05:42
##SOURCE REFERENCE=   MEL-29Si-Fyfe-1991-302K
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              MEL
##NAMES=              ZSM-11
##SAMPLE DESCRIPTION= ZSM-11, dealuminated, low-temp phase
##TEMPERATURE=        302K

$$Bibliographic information 
##$AUTHORS=           Fyfe, C.A., Feng, Y., Grondey, H., Kokotailo, C.T., Mar, A.
##$TITLE=             Natural Abundance, Two-Dimensional 29Si MAS NMR Investigation of the Three-Dimensional Bonding Connectivities in the High- and Low-Temperature Forms of Zeolite ZSM-11
##$JOURNAL=           J. Phys. Chem
##$VOLUME=            95
##$PAGES=             3747-3751
##$YEAR=              1991
##$DOI=               10.1021/j100162a057
##$FIGURE=            Figure 3a

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         12
##$PEAK LABELS=        Si3        Si7        Si2        Si6        Si9        Si10       Si8        Si4        Si12       Si5        Si1        Si11      
##$PEAK TSITES=        T1         T3         T1         T3         T4         T7         T4         T2         T5         T2         T6         T5        
##$PEAK POSITIONS=    -116.695   -116.549   -115.572   -114.541   -114.358   -113.971   -112.505   -111.963   -111.85    -111.648   -111.479   -111.033   
##$PEAK AREAS=         1.         1.         1.         1.         1.         1.         1.         1.         1.         1.         1.         1.        
##$PEAK WIDTHS=        0.1479     0.14735    0.2056     0.2102     0.16416    0.13486    0.19399    0.17808    0.17808    0.12573    0.09468    0.21443   
##$PEAK SHAPES=        1          1          1          1          1          1          1          1          1          1          1          1         
##$NUMBERING REF=     Hochegrafe et al., Z. Kristallogr., 211, 221-227 (1996)
##$ASSIGN REF=        Fyfe et al. J. Phys. Chem, 95, 3747-3751 (1991) Figure 5
##$ASSIGN METHOD=     2D correlation NMR, average Si-Si distances
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 79.5
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     3000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -109.51               
##LASTX=              -118.51               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            901
##FIRSTY=             -0.11241              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -109.51             -0.11241              
 -109.52             -0.10012              
 -109.53             -0.08657              
 -109.54             -0.07564              
 -109.55             -0.06488              
 -109.56             -0.05231              
 -109.57             -0.04123              
 -109.58             -0.03613              
 -109.59             -0.03667              
 -109.6              -0.03888              
 -109.61             -0.03980              
 -109.62             -0.03854              
 -109.63             -0.03540              
 -109.64             -0.03566              
 -109.65             -0.04583              
 -109.66             -0.06757              
 -109.67             -0.09870              
 -109.68             -0.13454              
 -109.69             -0.16572              
 -109.7              -0.18427              
 -109.71             -0.19232              
 -109.72             -0.19515              
 -109.73             -0.19535              
 -109.74             -0.19322              
 -109.75             -0.18697              
 -109.76             -0.17067              
 -109.77             -0.14021              
 -109.78             -0.10446              
 -109.79             -0.07647              
 -109.8              -0.06323              
 -109.81             -0.06635              
 -109.82             -0.08481              
 -109.83             -0.11226              
 -109.84             -0.14135              
 -109.85             -0.16306              
 -109.86             -0.16823              
 -109.87             -0.15705              
 -109.88             -0.13833              
 -109.89             -0.11794              
 -109.9              -0.09421              
 -109.91             -0.06614              
 -109.92             -0.04337              
 -109.93             -0.03881              
 -109.94             -0.04489              
 -109.95             -0.03415              
 -109.96              0.00396              
 -109.97              0.03709              
 -109.98              0.03294              
 -109.99              0.00312              
 -110.               -0.02346              
 -110.01             -0.03526              
 -110.02             -0.03858              
 -110.03             -0.03905              
 -110.04             -0.03847              
 -110.05             -0.03797              
 -110.06             -0.03803              
 -110.07             -0.03879              
 -110.08             -0.03942              
 -110.09             -0.03797              
 -110.1              -0.03187              
 -110.11             -0.01703              
 -110.12              0.00892              
 -110.13              0.03351              
 -110.14              0.03783              
 -110.15              0.01728              
 -110.16             -0.01642              
 -110.17             -0.05232              
 -110.18             -0.08408              
 -110.19             -0.10648              
 -110.2              -0.11657              
 -110.21             -0.11274              
 -110.22             -0.09970              
 -110.23             -0.08975              
 -110.24             -0.09013              
 -110.25             -0.09128              
 -110.26             -0.08147              
 -110.27             -0.05792              
 -110.28             -0.02245              
 -110.29              0.02152              
 -110.3               0.06871              
 -110.31              0.11214              
 -110.32              0.13997              
 -110.33              0.14154              
 -110.34              0.12621              
 -110.35              0.11390              
 -110.36              0.11319              
 -110.37              0.11742              
 -110.38              0.12009              
 -110.39              0.11863              
 -110.4               0.11233              
 -110.41              0.11009              
 -110.42              0.12602              
 -110.43              0.16074              
 -110.44              0.19591              
 -110.45              0.21609              
 -110.46              0.22158              
 -110.47              0.21629              
 -110.48              0.20433              
 -110.49              0.18988              
 -110.5               0.17690              
 -110.51              0.16901              
 -110.52              0.16805              
 -110.53              0.16926              
 -110.54              0.16711              
 -110.55              0.16531              
 -110.56              0.17337              
 -110.57              0.19428              
 -110.58              0.22071              
 -110.59              0.24362              
 -110.6               0.25059              
 -110.61              0.23008              
 -110.62              0.19226              
 -110.63              0.16173              
 -110.64              0.15383              
 -110.65              0.16836              
 -110.66              0.20297              
 -110.67              0.25223              
 -110.68              0.30975              
 -110.69              0.36716              
 -110.7               0.41481              
 -110.71              0.44941              
 -110.72              0.47877              
 -110.73              0.51030              
 -110.74              0.54441              
 -110.75              0.57946              
 -110.76              0.61331              
 -110.77              0.64350              
 -110.78              0.67225              
 -110.79              0.71035              
 -110.8               0.76521              
 -110.81              0.82324              
 -110.82              0.86579              
 -110.83              0.89553              
 -110.84              0.93176              
 -110.85              0.98453              
 -110.86              1.04528              
 -110.87              1.10606              
 -110.88              1.17303              
 -110.89              1.25636              
 -110.9               1.35637              
 -110.91              1.46528              
 -110.92              1.57665              
 -110.93              1.68715              
 -110.94              1.79944              
 -110.95              1.94697              
 -110.96              2.17036              
 -110.97              2.44879              
 -110.98              2.70823              
 -110.99              2.91066              
 -111.                3.0992               
 -111.01              3.31017              
 -111.02              3.47842              
 -111.03              3.5071               
 -111.04              3.40006              
 -111.05              3.25322              
 -111.06              3.11994              
 -111.07              2.94925              
 -111.08              2.69184              
 -111.09              2.39824              
 -111.1               2.15459              
 -111.11              1.98619              
 -111.12              1.85966              
 -111.13              1.75027              
 -111.14              1.65969              
 -111.15              1.59191              
 -111.16              1.54046              
 -111.17              1.49511              
 -111.18              1.45692              
 -111.19              1.43841              
 -111.2               1.44494              
 -111.21              1.46235              
 -111.22              1.47564              
 -111.23              1.48529              
 -111.24              1.49837              
 -111.25              1.51887              
 -111.26              1.54754              
 -111.27              1.58545              
 -111.28              1.63503              
 -111.29              1.69877              
 -111.3               1.77815              
 -111.31              1.87387              
 -111.32              1.9777               
 -111.33              2.07137              
 -111.34              2.14911              
 -111.35              2.2422               
 -111.36              2.38186              
 -111.37              2.54622              
 -111.38              2.69                 
 -111.39              2.83393              
 -111.4               3.07717              
 -111.41              3.49036              
 -111.42              4.04449              
 -111.43              4.69465              
 -111.44              5.41986              
 -111.45              6.20944              
 -111.46              6.98707              
 -111.47              7.5944               
 -111.48              7.89538              
 -111.49              7.84173              
 -111.5               7.41997              
 -111.51              6.77522              
 -111.52              6.13462              
 -111.53              5.60766              
 -111.54              5.14817              
 -111.55              4.72689              
 -111.56              4.40773              
 -111.57              4.26571              
 -111.58              4.29214              
 -111.59              4.43186              
 -111.6               4.67001              
 -111.61              5.04829              
 -111.62              5.57421              
 -111.63              6.11766              
 -111.64              6.52457              
 -111.65              6.71372              
 -111.66              6.64854              
 -111.67              6.35483              
 -111.68              5.94854              
 -111.69              5.52843              
 -111.7               5.10067              
 -111.71              4.65488              
 -111.72              4.24272              
 -111.73              3.95384              
 -111.74              3.81819              
 -111.75              3.77297              
 -111.76              3.76527              
 -111.77              3.81412              
 -111.78              3.95212              
 -111.79              4.15622              
 -111.8               4.36692              
 -111.81              4.55336              
 -111.82              4.73223              
 -111.83              4.92674              
 -111.84              5.16957              
 -111.85              5.48645              
 -111.86              5.7798               
 -111.87              5.86753              
 -111.88              5.69738              
 -111.89              5.44214              
 -111.9               5.26833              
 -111.91              5.21381              
 -111.92              5.2781               
 -111.93              5.43715              
 -111.94              5.64931              
 -111.95              5.85285              
 -111.96              5.95045              
 -111.97              5.85645              
 -111.98              5.55937              
 -111.99              5.07467              
 -112.                4.48687              
 -112.01              3.93342              
 -112.02              3.48863              
 -112.03              3.10391              
 -112.04              2.73227              
 -112.05              2.40566              
 -112.06              2.17751              
 -112.07              2.03935              
 -112.08              1.93227              
 -112.09              1.8153               
 -112.1               1.68656              
 -112.11              1.55005              
 -112.12              1.41648              
 -112.13              1.29824              
 -112.14              1.19798              
 -112.15              1.10994              
 -112.16              1.03318              
 -112.17              0.97758              
 -112.18              0.95148              
 -112.19              0.94628              
 -112.2               0.94765              
 -112.21              0.94809              
 -112.22              0.94627              
 -112.23              0.93992              
 -112.24              0.92422              
 -112.25              0.89681              
 -112.26              0.87290              
 -112.27              0.87334              
 -112.28              0.89767              
 -112.29              0.92511              
 -112.3               0.94093              
 -112.31              0.94663              
 -112.32              0.94749              
 -112.33              0.95807              
 -112.34              0.99596              
 -112.35              1.06217              
 -112.36              1.14104              
 -112.37              1.22319              
 -112.38              1.31673              
 -112.39              1.43014              
 -112.4               1.55564              
 -112.41              1.67967              
 -112.42              1.81791              
 -112.43              2.0169               
 -112.44              2.29328              
 -112.45              2.58023              
 -112.46              2.80982              
 -112.47              3.00739              
 -112.48              3.23729              
 -112.49              3.48061              
 -112.5               3.62563              
 -112.51              3.59942              
 -112.52              3.45179              
 -112.53              3.24755              
 -112.54              3.00058              
 -112.55              2.70168              
 -112.56              2.37524              
 -112.57              2.08524              
 -112.58              1.87629              
 -112.59              1.72865              
 -112.6               1.61089              
 -112.61              1.49323              
 -112.62              1.34776              
 -112.63              1.18095              
 -112.64              1.04172              
 -112.65              0.95912              
 -112.66              0.89125              
 -112.67              0.79023              
 -112.68              0.68020              
 -112.69              0.62217              
 -112.7               0.62614              
 -112.71              0.63533              
 -112.72              0.60787              
 -112.73              0.56688              
 -112.74              0.54520              
 -112.75              0.53892              
 -112.76              0.52391              
 -112.77              0.49118              
 -112.78              0.45278              
 -112.79              0.41873              
 -112.8               0.38655              
 -112.81              0.35169              
 -112.82              0.31717              
 -112.83              0.29038              
 -112.84              0.27565              
 -112.85              0.27282              
 -112.86              0.28049              
 -112.87              0.29402              
 -112.88              0.30816              
 -112.89              0.31959              
 -112.9               0.32622              
 -112.91              0.32738              
 -112.92              0.32462              
 -112.93              0.31857              
 -112.94              0.30555              
 -112.95              0.28125              
 -112.96              0.24710              
 -112.97              0.20829              
 -112.98              0.17110              
 -112.99              0.14352              
 -113.                0.13217              
 -113.01              0.13744              
 -113.02              0.15740              
 -113.03              0.18245              
 -113.04              0.19773              
 -113.05              0.19810              
 -113.06              0.19500              
 -113.07              0.19943              
 -113.08              0.21331              
 -113.09              0.23561              
 -113.1               0.25989              
 -113.11              0.27579              
 -113.12              0.27433              
 -113.13              0.24919              
 -113.14              0.19828              
 -113.15              0.13850              
 -113.16              0.09159              
 -113.17              0.06764              
 -113.18              0.06771              
 -113.19              0.08787              
 -113.2               0.11517              
 -113.21              0.13830              
 -113.22              0.15935              
 -113.23              0.18406              
 -113.24              0.20885              
 -113.25              0.22268              
 -113.26              0.22234              
 -113.27              0.22060              
 -113.28              0.22901              
 -113.29              0.24228              
 -113.3               0.24997              
 -113.31              0.24970              
 -113.32              0.24592              
 -113.33              0.23958              
 -113.34              0.22377              
 -113.35              0.19319              
 -113.36              0.15731              
 -113.37              0.13040              
 -113.38              0.11807              
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 -113.4               0.12731              
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 -113.43              0.16576              
 -113.44              0.17099              
 -113.45              0.17097              
 -113.46              0.16858              
 -113.47              0.16676              
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 -113.5               0.18775              
 -113.51              0.20291              
 -113.52              0.22276              
 -113.53              0.25257              
 -113.54              0.29126              
 -113.55              0.32160              
 -113.56              0.32804              
 -113.57              0.32332              
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 -113.59              0.35566              
 -113.6               0.37907              
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 -113.64              0.33270              
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 -113.66              0.33256              
 -113.67              0.35340              
 -113.68              0.37999              
 -113.69              0.41789              
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 -113.71              0.53097              
 -113.72              0.57400              
 -113.73              0.59656              
 -113.74              0.61138              
 -113.75              0.62957              
 -113.76              0.65454              
 -113.77              0.68745              
 -113.78              0.72225              
 -113.79              0.74980              
 -113.8               0.77550              
 -113.81              0.82256              
 -113.82              0.90445              
 -113.83              1.00085              
 -113.84              1.08824              
 -113.85              1.17326              
 -113.86              1.27805              
 -113.87              1.41439              
 -113.88              1.58053              
 -113.89              1.79521              
 -113.9               2.14782              
 -113.91              2.71991              
 -113.92              3.37952              
 -113.93              3.88104              
 -113.94              4.16678              
 -113.95              4.43547              
 -113.96              4.80922              
 -113.97              5.07754              
 -113.98              4.98717              
 -113.99              4.59123              
 -114.                4.11953              
 -114.01              3.70277              
 -114.02              3.32685              
 -114.03              2.97222              
 -114.04              2.64038              
 -114.05              2.33871              
 -114.06              2.08557              
 -114.07              1.90563              
 -114.08              1.7982               
 -114.09              1.72435              
 -114.1               1.64968              
 -114.11              1.57026              
 -114.12              1.48967              
 -114.13              1.41144              
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 -114.15              1.27726              
 -114.16              1.23258              
 -114.17              1.2097               
 -114.18              1.20474              
 -114.19              1.21317              
 -114.2               1.25078              
 -114.21              1.34685              
 -114.22              1.49745              
 -114.23              1.64269              
 -114.24              1.73443              
 -114.25              1.80035              
 -114.26              1.88948              
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 -114.29              2.76778              
 -114.3               3.20616              
 -114.31              3.57411              
 -114.32              3.9139               
 -114.33              4.29798              
 -114.34              4.67387              
 -114.35              4.89496              
 -114.36              4.89233              
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 -114.38              4.54219              
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 -114.42              3.63062              
 -114.43              3.46033              
 -114.44              3.34044              
 -114.45              3.28217              
 -114.46              3.29843              
 -114.47              3.40061              
 -114.48              3.56332              
 -114.49              3.73031              
 -114.5               3.86436              
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 -114.52              4.04843              
 -114.53              4.06189              
 -114.54              3.96039              
 -114.55              3.75619              
 -114.56              3.51644              
 -114.57              3.28192              
 -114.58              3.03142              
 -114.59              2.74525              
 -114.6               2.46235              
 -114.61              2.24084              
 -114.62              2.08734              
 -114.63              1.96034              
 -114.64              1.83272              
 -114.65              1.71495              
 -114.66              1.61926              
 -114.67              1.53487              
 -114.68              1.44301              
 -114.69              1.3475               
 -114.7               1.2744               
 -114.71              1.23323              
 -114.72              1.19066              
 -114.73              1.11395              
 -114.74              1.01809              
 -114.75              0.93699              
 -114.76              0.88115              
 -114.77              0.83680              
 -114.78              0.79589              
 -114.79              0.76816              
 -114.8               0.76302              
 -114.81              0.76727              
 -114.82              0.75825              
 -114.83              0.72732              
 -114.84              0.68115              
 -114.85              0.62962              
 -114.86              0.58933              
 -114.87              0.57511              
 -114.88              0.57969              
 -114.89              0.58584              
 -114.9               0.58598              
 -114.91              0.58364              
 -114.92              0.58229              
 -114.93              0.58323              
 -114.94              0.58677              
 -114.95              0.58765              
 -114.96              0.57811              
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 -114.99              0.50327              
 -115.                0.48347              
 -115.01              0.47513              
 -115.02              0.47664              
 -115.03              0.48302              
 -115.04              0.48710              
 -115.05              0.47905              
 -115.06              0.45508              
 -115.07              0.43181              
 -115.08              0.42789              
 -115.09              0.44199              
 -115.1               0.46202              
 -115.11              0.48260              
 -115.12              0.50746              
 -115.13              0.53682              
 -115.14              0.55652              
 -115.15              0.55127              
 -115.16              0.52562              
 -115.17              0.49542              
 -115.18              0.47085              
 -115.19              0.45389              
 -115.2               0.44614              
 -115.21              0.45016              
 -115.22              0.46790              
 -115.23              0.49240              
 -115.24              0.51134              
 -115.25              0.51651              
 -115.26              0.50595              
 -115.27              0.47950              
 -115.28              0.44209              
 -115.29              0.40084              
 -115.3               0.37391              
 -115.31              0.38620              
 -115.32              0.44064              
 -115.33              0.50545              
 -115.34              0.55609              
 -115.35              0.61042              
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##END=
