##TITLE=              29Si MAS NMR spectrum of calcined dealuminated ZSM-11 at 342K
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Fyfe et al. J. Phys. Chem., 95, 3747-3751 (1991) Figure 3b
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 15:07:16
##SOURCE REFERENCE=   MEL-29Si-Fyfe-1991-342K
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              MEL
##NAMES=              ZSM-11
##SAMPLE DESCRIPTION= ZSM-11, dealuminated, high-temp phase
##TEMPERATURE=        342K

$$Bibliographic information 
##$AUTHORS=           Fyfe, C.A., Feng, Y., Grondey, H., Kokotailo, C.T., Mar, A.
##$TITLE=             Natural Abundance, Two-Dimensional 29Si MAS NMR Investigation of the Three-Dimensional Bonding Connectivities in the High- and Low-Temperature Forms of Zeolite ZSM-11
##$JOURNAL=           Journal of Physical Chemistry
##$VOLUME=            95
##$PAGES=             3747-3751
##$YEAR=              1991
##$DOI=               10.1021/j100162a057
##$FIGURE=            Figure 3b

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         7
##$PEAK LABELS=        Si2        Si4        Si6        Si5        Si7        Si3        Si1       
##$PEAK TSITES=        T1         T3         T7         T4         T5         T2         T6        
##$PEAK POSITIONS=    -116.145   -115.776   -113.831   -113.503   -111.92    -111.822   -111.376   
##$PEAK AREAS=         2.         2.         1.         2.         2.         2.         1.        
##$PEAK WIDTHS=        0.20173    0.15706    0.14876    0.17132    0.18953    0.17765    0.10951   
##$PEAK SHAPES=        1          1          1          1          1          1          1         
##$NUMBERING REF=     Fyfe et al. J. Am. Chem. Soc. 111, 2470-2474 (1989)
##$ASSIGN REF=        Fyfe et al. J. Phys. Chem. 95, 3747-3751 (1991) Figure 4
##$ASSIGN METHOD=     2D correlation NMR, relative intensities
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 79.5
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     3000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -108.5                
##LASTX=              -117.94               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            945
##FIRSTY=              0.06901              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -108.5               0.06901              
 -108.51              0.05186              
 -108.52              0.05485              
 -108.53              0.07541              
 -108.54              0.08950              
 -108.55              0.07567              
 -108.56              0.03902              
 -108.57             -0.00557              
 -108.58             -0.04416              
 -108.59             -0.06392              
 -108.6              -0.05669              
 -108.61             -0.03563              
 -108.62             -0.01971              
 -108.63             -0.01737              
 -108.64             -0.02612              
 -108.65             -0.04219              
 -108.66             -0.05876              
 -108.67             -0.06859              
 -108.68             -0.06944              
 -108.69             -0.06328              
 -108.7              -0.05153              
 -108.71             -0.03371              
 -108.72             -0.00909              
 -108.73              0.02190              
 -108.74              0.05808              
 -108.75              0.09542              
 -108.76              0.12339              
 -108.77              0.13228              
 -108.78              0.12893              
 -108.79              0.12917              
 -108.8               0.13666              
 -108.81              0.13212              
 -108.82              0.09776              
 -108.83              0.04520              
 -108.84             -0.00113              
 -108.85             -0.03184              
 -108.86             -0.06029              
 -108.87             -0.09759              
 -108.88             -0.13132              
 -108.89             -0.14105              
 -108.9              -0.11779              
 -108.91             -0.06667              
 -108.92              0.00311              
 -108.93              0.06779              
 -108.94              0.10062              
 -108.95              0.09994              
 -108.96              0.08918              
 -108.97              0.08382              
 -108.98              0.06717              
 -108.99              0.01751              
 -109.               -0.05342              
 -109.01             -0.10676              
 -109.02             -0.11824              
 -109.03             -0.10694              
 -109.04             -0.09799              
 -109.05             -0.09853              
 -109.06             -0.10381              
 -109.07             -0.10837              
 -109.08             -0.10548              
 -109.09             -0.08986              
 -109.1              -0.07071              
 -109.11             -0.06479              
 -109.12             -0.07848              
 -109.13             -0.09921              
 -109.14             -0.11328              
 -109.15             -0.11293              
 -109.16             -0.09311              
 -109.17             -0.05850              
 -109.18             -0.02793              
 -109.19             -0.01744              
 -109.2              -0.02167              
 -109.21             -0.02832              
 -109.22             -0.03734              
 -109.23             -0.06318              
 -109.24             -0.11371              
 -109.25             -0.16455              
 -109.26             -0.18394              
 -109.27             -0.16799              
 -109.28             -0.13962              
 -109.29             -0.11796              
 -109.3              -0.10540              
 -109.31             -0.10067              
 -109.32             -0.10108              
 -109.33             -0.10279              
 -109.34             -0.10317              
 -109.35             -0.10275              
 -109.36             -0.10256              
 -109.37             -0.10267              
 -109.38             -0.10256              
 -109.39             -0.10216              
 -109.4              -0.10236              
 -109.41             -0.10386              
 -109.42             -0.10456              
 -109.43             -0.10098              
 -109.44             -0.09537              
 -109.45             -0.09990              
 -109.46             -0.12475              
 -109.47             -0.16004              
 -109.48             -0.18788              
 -109.49             -0.20269              
 -109.5              -0.21627              
 -109.51             -0.23777              
 -109.52             -0.25525              
 -109.53             -0.25043              
 -109.54             -0.22042              
 -109.55             -0.17997              
 -109.56             -0.14266              
 -109.57             -0.11316              
 -109.58             -0.09395              
 -109.59             -0.08914              
 -109.6              -0.10438              
 -109.61             -0.13912              
 -109.62             -0.17234              
 -109.63             -0.18041              
 -109.64             -0.16303              
 -109.65             -0.13750              
 -109.66             -0.11733              
 -109.67             -0.10486              
 -109.68             -0.10040              
 -109.69             -0.10124              
 -109.7              -0.10282              
 -109.71             -0.10264              
 -109.72             -0.10243              
 -109.73             -0.10397              
 -109.74             -0.10482              
 -109.75             -0.10052              
 -109.76             -0.08826              
 -109.77             -0.06806              
 -109.78             -0.04209              
 -109.79             -0.02439              
 -109.8              -0.03330              
 -109.81             -0.06787              
 -109.82             -0.10096              
 -109.83             -0.10992              
 -109.84             -0.10450              
 -109.85             -0.10427              
 -109.86             -0.11772              
 -109.87             -0.14108              
 -109.88             -0.16772              
 -109.89             -0.18199              
 -109.9              -0.16725              
 -109.91             -0.13074              
 -109.92             -0.10121              
 -109.93             -0.09719              
 -109.94             -0.10274              
 -109.95             -0.09662              
 -109.96             -0.07832              
 -109.97             -0.06244              
 -109.98             -0.05849              
 -109.99             -0.06241              
 -110.               -0.06803              
 -110.01             -0.06946              
 -110.02             -0.06105              
 -110.03             -0.04785              
 -110.04             -0.05641              
 -110.05             -0.10972              
 -110.06             -0.18228              
 -110.07             -0.22585              
 -110.08             -0.21920              
 -110.09             -0.18506              
 -110.1              -0.14778              
 -110.11             -0.11676              
 -110.12             -0.09574              
 -110.13             -0.08890              
 -110.14             -0.10108              
 -110.15             -0.13329              
 -110.16             -0.16803              
 -110.17             -0.18302              
 -110.18             -0.17868              
 -110.19             -0.17966              
 -110.2              -0.20140              
 -110.21             -0.21971              
 -110.22             -0.20273              
 -110.23             -0.15205              
 -110.24             -0.09832              
 -110.25             -0.06632              
 -110.26             -0.06004              
 -110.27             -0.07885              
 -110.28             -0.11293              
 -110.29             -0.14598              
 -110.3              -0.16695              
 -110.31             -0.17773              
 -110.32             -0.18197              
 -110.33             -0.18178              
 -110.34             -0.17837              
 -110.35             -0.16978              
 -110.36             -0.14806              
 -110.37             -0.10674              
 -110.38             -0.05605              
 -110.39             -0.01378              
 -110.4               0.00929              
 -110.41              0.01343              
 -110.42              0.00117              
 -110.43             -0.01726              
 -110.44             -0.02908              
 -110.45             -0.02988              
 -110.46             -0.02597              
 -110.47             -0.02341              
 -110.48             -0.02404              
 -110.49             -0.02853              
 -110.5              -0.04021              
 -110.51             -0.06513              
 -110.52             -0.10377              
 -110.53             -0.13568              
 -110.54             -0.13691              
 -110.55             -0.10572              
 -110.56             -0.05899              
 -110.57             -0.01065              
 -110.58              0.03558              
 -110.59              0.07765              
 -110.6               0.11115              
 -110.61              0.13006              
 -110.62              0.12863              
 -110.63              0.10191              
 -110.64              0.04697              
 -110.65             -0.02086              
 -110.66             -0.07629              
 -110.67             -0.10358              
 -110.68             -0.10501              
 -110.69             -0.08521              
 -110.7              -0.05145              
 -110.71             -0.01218              
 -110.72              0.02418              
 -110.73              0.04926              
 -110.74              0.05693              
 -110.75              0.05365              
 -110.76              0.05021              
 -110.77              0.05070              
 -110.78              0.05112              
 -110.79              0.04866              
 -110.8               0.04828              
 -110.81              0.05675              
 -110.82              0.07339              
 -110.83              0.09008              
 -110.84              0.10206              
 -110.85              0.11764              
 -110.86              0.14746              
 -110.87              0.19345              
 -110.88              0.25047              
 -110.89              0.31319              
 -110.9               0.37630              
 -110.91              0.43451              
 -110.92              0.48312              
 -110.93              0.51780              
 -110.94              0.53747              
 -110.95              0.54834              
 -110.96              0.55755              
 -110.97              0.57185              
 -110.98              0.59774              
 -110.99              0.63349              
 -111.                0.66270              
 -111.01              0.67074              
 -111.02              0.66644              
 -111.03              0.66839              
 -111.04              0.68367              
 -111.05              0.70261              
 -111.06              0.71667              
 -111.07              0.73094              
 -111.08              0.75508              
 -111.09              0.79579              
 -111.1               0.85629              
 -111.11              0.93578              
 -111.12              1.01684              
 -111.13              1.07859              
 -111.14              1.12189              
 -111.15              1.16847              
 -111.16              1.23522              
 -111.17              1.31972              
 -111.18              1.41581              
 -111.19              1.52267              
 -111.2               1.64369              
 -111.21              1.77598              
 -111.22              1.89943              
 -111.23              1.99357              
 -111.24              2.0665               
 -111.25              2.14442              
 -111.26              2.24898              
 -111.27              2.39129              
 -111.28              2.58128              
 -111.29              2.83009              
 -111.3               3.14938              
 -111.31              3.54324              
 -111.32              4.00257              
 -111.33              4.51492              
 -111.34              5.05391              
 -111.35              5.58706              
 -111.36              6.0638               
 -111.37              6.40814              
 -111.38              6.55041              
 -111.39              6.46417              
 -111.4               6.13881              
 -111.41              5.61421              
 -111.42              4.98783              
 -111.43              4.35252              
 -111.44              3.7689               
 -111.45              3.28784              
 -111.46              2.93035              
 -111.47              2.68974              
 -111.48              2.54938              
 -111.49              2.46358              
 -111.5               2.38288              
 -111.51              2.28914              
 -111.52              2.1879               
 -111.53              2.09441              
 -111.54              2.04758              
 -111.55              2.08494              
 -111.56              2.18813              
 -111.57              2.30469              
 -111.58              2.40201              
 -111.59              2.48965              
 -111.6               2.58088              
 -111.61              2.67593              
 -111.62              2.76868              
 -111.63              2.85873              
 -111.64              2.95527              
 -111.65              3.06708              
 -111.66              3.1943               
 -111.67              3.33374              
 -111.68              3.48471              
 -111.69              3.64989              
 -111.7               3.83276              
 -111.71              4.03947              
 -111.72              4.27814              
 -111.73              4.58906              
 -111.74              5.04789              
 -111.75              5.68183              
 -111.76              6.31828              
 -111.77              6.75157              
 -111.78              7.09092              
 -111.79              7.72777              
 -111.8               8.87821              
 -111.81              10.1764              
 -111.82              11.1656              
 -111.83              11.7078              
 -111.84              11.8973              
 -111.85              11.8153              
 -111.86              11.497               
 -111.87              10.9756              
 -111.88              10.333               
 -111.89              9.68019              
 -111.9               9.14542              
 -111.91              8.89106              
 -111.92              9.04449              
 -111.93              9.42436              
 -111.94              9.70426              
 -111.95              9.6742               
 -111.96              9.31354              
 -111.97              8.63203              
 -111.98              7.72072              
 -111.99              6.7011               
 -112.                5.67596              
 -112.01              4.72353              
 -112.02              3.90698              
 -112.03              3.22475              
 -112.04              2.65599              
 -112.05              2.18737              
 -112.06              1.81357              
 -112.07              1.52785              
 -112.08              1.31648              
 -112.09              1.16397              
 -112.1               1.05318              
 -112.11              0.96551              
 -112.12              0.88914              
 -112.13              0.83277              
 -112.14              0.80773              
 -112.15              0.80939              
 -112.16              0.82185              
 -112.17              0.83064              
 -112.18              0.82520              
 -112.19              0.79676              
 -112.2               0.74816              
 -112.21              0.68885              
 -112.22              0.62620              
 -112.23              0.56343              
 -112.24              0.50395              
 -112.25              0.45592              
 -112.26              0.42957              
 -112.27              0.42637              
 -112.28              0.43422              
 -112.29              0.44086              
 -112.3               0.44039              
 -112.31              0.42942              
 -112.32              0.41118              
 -112.33              0.39728              
 -112.34              0.39613              
 -112.35              0.39871              
 -112.36              0.39146              
 -112.37              0.37374              
 -112.38              0.35819              
 -112.39              0.35422              
 -112.4               0.35711              
 -112.41              0.35926              
 -112.42              0.35879              
 -112.43              0.35857              
 -112.44              0.36001              
 -112.45              0.35976              
 -112.46              0.35445              
 -112.47              0.35082              
 -112.48              0.36242              
 -112.49              0.39376              
 -112.5               0.42806              
 -112.51              0.44703              
 -112.52              0.44637              
 -112.53              0.42951              
 -112.54              0.40583              
 -112.55              0.39554              
 -112.56              0.41584              
 -112.57              0.45314              
 -112.58              0.48055              
 -112.59              0.48520              
 -112.6               0.47538              
 -112.61              0.46027              
 -112.62              0.44413              
 -112.63              0.42938              
 -112.64              0.41537              
 -112.65              0.39769              
 -112.66              0.37247              
 -112.67              0.33932              
 -112.68              0.29917              
 -112.69              0.26126              
 -112.7               0.24307              
 -112.71              0.25428              
 -112.72              0.27573              
 -112.73              0.28348              
 -112.74              0.27883              
 -112.75              0.28342              
 -112.76              0.31030              
 -112.77              0.34689              
 -112.78              0.37695              
 -112.79              0.39365              
 -112.8               0.39630              
 -112.81              0.38559              
 -112.82              0.36499              
 -112.83              0.33919              
 -112.84              0.32032              
 -112.85              0.32433              
 -112.86              0.35450              
 -112.87              0.39126              
 -112.88              0.41556              
 -112.89              0.42851              
 -112.9               0.43973              
 -112.91              0.45452              
 -112.92              0.47191              
 -112.93              0.49013              
 -112.94              0.50588              
 -112.95              0.51535              
 -112.96              0.51709              
 -112.97              0.51237              
 -112.98              0.50211              
 -112.99              0.48503              
 -113.                0.45946              
 -113.01              0.42756              
 -113.02              0.39520              
 -113.03              0.36895              
 -113.04              0.35716              
 -113.05              0.36792              
 -113.06              0.39924              
 -113.07              0.44127              
 -113.08              0.48652              
 -113.09              0.53438              
 -113.1               0.58496              
 -113.11              0.63372              
 -113.12              0.67322              
 -113.13              0.70226              
 -113.14              0.73321              
 -113.15              0.77787              
 -113.16              0.82843              
 -113.17              0.86718              
 -113.18              0.88630              
 -113.19              0.89519              
 -113.2               0.90433              
 -113.21              0.91988              
 -113.22              0.94608              
 -113.23              0.98020              
 -113.24              1.00979              
 -113.25              1.02746              
 -113.26              1.05621              
 -113.27              1.12779              
 -113.28              1.24089              
 -113.29              1.35658              
 -113.3               1.44668              
 -113.31              1.53575              
 -113.32              1.65977              
 -113.33              1.81101              
 -113.34              1.94131              
 -113.35              2.02804              
 -113.36              2.13654              
 -113.37              2.34322              
 -113.38              2.62635              
 -113.39              2.89045              
 -113.4               3.08498              
 -113.41              3.2804               
 -113.42              3.56178              
 -113.43              3.96443              
 -113.44              4.49314              
 -113.45              5.12998              
 -113.46              5.81098              
 -113.47              6.46849              
 -113.48              7.05181              
 -113.49              7.51843              
 -113.5               7.81493              
 -113.51              7.8696               
 -113.52              7.62999              
 -113.53              7.17792              
 -113.54              6.6465               
 -113.55              6.10269              
 -113.56              5.52379              
 -113.57              4.89299              
 -113.58              4.25495              
 -113.59              3.67279              
 -113.6               3.18769              
 -113.61              2.81676              
 -113.62              2.5668               
 -113.63              2.40872              
 -113.64              2.30546              
 -113.65              2.23752              
 -113.66              2.20111              
 -113.67              2.19136              
 -113.68              2.19829              
 -113.69              2.21203              
 -113.7               2.23764              
 -113.71              2.291                
 -113.72              2.38222              
 -113.73              2.50638              
 -113.74              2.65475              
 -113.75              2.80293              
 -113.76              2.91763              
 -113.77              3.01192              
 -113.78              3.19151              
 -113.79              3.55282              
 -113.8               4.03227              
 -113.81              4.49079              
 -113.82              4.81524              
 -113.83              4.93479              
 -113.84              4.80116              
 -113.85              4.48067              
 -113.86              4.08189              
 -113.87              3.6667               
 -113.88              3.23587              
 -113.89              2.79414              
 -113.9               2.38517              
 -113.91              2.0626               
 -113.92              1.83485              
 -113.93              1.66234              
 -113.94              1.50804              
 -113.95              1.35329              
 -113.96              1.18524              
 -113.97              1.01751              
 -113.98              0.88653              
 -113.99              0.81562              
 -114.                0.78652              
 -114.01              0.77447              
 -114.02              0.77219              
 -114.03              0.78463              
 -114.04              0.80871              
 -114.05              0.82159              
 -114.06              0.80034              
 -114.07              0.74951              
 -114.08              0.68920              
 -114.09              0.63028              
 -114.1               0.56557              
 -114.11              0.48800              
 -114.12              0.40668              
 -114.13              0.33804              
 -114.14              0.29426              
 -114.15              0.28090              
 -114.16              0.30005              
 -114.17              0.33695              
 -114.18              0.37088              
 -114.19              0.39064              
 -114.2               0.39693              
 -114.21              0.39096              
 -114.22              0.37267              
 -114.23              0.34197              
 -114.24              0.30637              
 -114.25              0.28118              
 -114.26              0.27633              
 -114.27              0.28079              
 -114.28              0.27976              
 -114.29              0.27532              
 -114.3               0.28367              
 -114.31              0.31317              
 -114.32              0.34841              
 -114.33              0.37059              
 -114.34              0.37221              
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##END=
