##TITLE=              29Si CP MAS NMR spectrum of as-made pure silica Dodecasil-3C (with pyridine)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Chae et al. ACS Symp. Ser., 455, 528-540 (1991) Figure 2
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 15:40:24
##SOURCE REFERENCE=   MTN-29Si-Chae-1991-pyr
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              MTN
##NAMES=              Dodecasil-3C
##NAMES=              ZSM-39
##SAMPLE DESCRIPTION= Dodecasil-3C, as-made, pyridine

$$Bibliographic information 
##$AUTHORS=           Chae, H.K., Klemperer, W.G., Payne, D.A., Suchicital, C.T.A., Wake, D.R., Wilson, S.R.
##$TITLE=             Clathrasils: New materials for non-linear applications
##$JOURNAL=           ACS Symposium Series
##$VOLUME=            455
##$PAGES=             528-540
##$YEAR=              1991
##$DOI=               10.1021/bk-1991-0455.ch035
##$FIGURE=            Figure 2

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         5
##$PEAK LABELS=       Si3/Si4/Si5 Si3/Si4/Si5 Si3/Si4/Si5 Si2        Si1       
##$PEAK TSITES=       T1          T1          T1          T2         T3    
##$PEAK POSITIONS=    -120.408   -119.898    -119.519    -114.319   -107.169   
##$PEAK AREAS=         4.         4.          4.          4.         1.        
##$PEAK WIDTHS=        0.35073    0.37914     0.43607     0.44151    0.61371   
##$PEAK SHAPES=        0.58483    0.58483     0.58483     0.58483    0.58483   
##$NUMBERING REF=     Chae et al. ACS Symp. Ser. 455, 528-540 (1991)
##$ASSIGN REF=        Fyfe et al. J. Am. Chem. Soc. 111, 7702-7707 (1989) Figure 5
##$ASSIGN METHOD=     relative intensities, 2D correlation NMR
##$COMMENT=     

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 59.6
##.PULSE SEQUENCE=    cross polarization
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -104.66               
##LASTX=              -122.98               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            917
##FIRSTY=              0.04783              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -104.66              0.04783              
 -104.68              0.05871              
 -104.7               0.06708              
 -104.72              0.07363              
 -104.74              0.07549              
 -104.76              0.07525              
 -104.78              0.07526              
 -104.8               0.07559              
 -104.82              0.07387              
 -104.84              0.06898              
 -104.86              0.06411              
 -104.88              0.05963              
 -104.9               0.05000              
 -104.92              0.03634              
 -104.94              0.02329              
 -104.96              0.01384              
 -104.98              0.00871              
 -105.                0.00892              
 -105.02              0.01043              
 -105.04              0.01493              
 -105.06              0.01638              
 -105.08              0.01664              
 -105.1               0.02177              
 -105.12              0.03203              
 -105.14              0.04288              
 -105.16              0.05091              
 -105.18              0.06212              
 -105.2               0.07872              
 -105.22              0.08193              
 -105.24              0.07649              
 -105.26              0.06741              
 -105.28              0.05562              
 -105.3               0.03798              
 -105.32              0.03154              
 -105.34              0.03697              
 -105.36              0.03844              
 -105.38              0.03859              
 -105.4               0.04402              
 -105.42              0.05133              
 -105.44              0.05314              
 -105.46              0.04530              
 -105.48              0.03428              
 -105.5               0.02488              
 -105.52              0.01447              
 -105.54              0.01444              
 -105.56              0.02434              
 -105.58              0.03518              
 -105.6               0.04438              
 -105.62              0.05613              
 -105.64              0.06080              
 -105.66              0.05655              
 -105.68              0.04936              
 -105.7               0.04124              
 -105.72              0.03714              
 -105.74              0.03326              
 -105.76              0.03011              
 -105.78              0.02376              
 -105.8               0.01614              
 -105.82              0.01485              
 -105.84              0.01394              
 -105.86              0.02174              
 -105.88              0.03714              
 -105.9               0.05193              
 -105.92              0.06614              
 -105.94              0.07859              
 -105.96              0.07995              
 -105.98              0.07641              
 -106.                0.06980              
 -106.02              0.04998              
 -106.04              0.03351              
 -106.06              0.02798              
 -106.08              0.02950              
 -106.1               0.03130              
 -106.12              0.03093              
 -106.14              0.03184              
 -106.16              0.0342               
 -106.18              0.03685              
 -106.2               0.03864              
 -106.22              0.03831              
 -106.24              0.03914              
 -106.26              0.04160              
 -106.28              0.04883              
 -106.3               0.05773              
 -106.32              0.06157              
 -106.34              0.07425              
 -106.36              0.09048              
 -106.38              0.10951              
 -106.4               0.13723              
 -106.42              0.16624              
 -106.44              0.19025              
 -106.46              0.20807              
 -106.48              0.21717              
 -106.5               0.22277              
 -106.52              0.22164              
 -106.54              0.21725              
 -106.56              0.21515              
 -106.58              0.22296              
 -106.6               0.23432              
 -106.62              0.24772              
 -106.64              0.27344              
 -106.66              0.30263              
 -106.68              0.32730              
 -106.7               0.35670              
 -106.72              0.39447              
 -106.74              0.43071              
 -106.76              0.47098              
 -106.78              0.52060              
 -106.8               0.57368              
 -106.82              0.61601              
 -106.84              0.66631              
 -106.86              0.71308              
 -106.88              0.75354              
 -106.9               0.80463              
 -106.92              0.85565              
 -106.94              0.91013              
 -106.96              0.96330              
 -106.98              1.00479              
 -107.                1.05022              
 -107.02              1.0983               
 -107.04              1.13733              
 -107.06              1.16885              
 -107.08              1.20205              
 -107.1               1.22751              
 -107.12              1.2539               
 -107.14              1.27633              
 -107.16              1.28383              
 -107.18              1.28423              
 -107.2               1.27521              
 -107.22              1.26145              
 -107.24              1.23975              
 -107.26              1.19895              
 -107.28              1.16839              
 -107.3               1.13374              
 -107.32              1.0787               
 -107.34              1.03202              
 -107.36              0.97640              
 -107.38              0.91717              
 -107.4               0.87577              
 -107.42              0.83094              
 -107.44              0.78971              
 -107.46              0.74566              
 -107.48              0.70472              
 -107.5               0.66672              
 -107.52              0.62564              
 -107.54              0.57225              
 -107.56              0.52394              
 -107.58              0.49391              
 -107.6               0.45871              
 -107.62              0.41649              
 -107.64              0.36536              
 -107.66              0.33117              
 -107.68              0.31583              
 -107.7               0.30554              
 -107.72              0.29507              
 -107.74              0.28255              
 -107.76              0.26800              
 -107.78              0.25191              
 -107.8               0.23801              
 -107.82              0.22124              
 -107.84              0.19928              
 -107.86              0.17257              
 -107.88              0.14791              
 -107.9               0.12565              
 -107.92              0.10384              
 -107.94              0.09158              
 -107.96              0.07851              
 -107.98              0.06964              
 -108.                0.07133              
 -108.02              0.07543              
 -108.04              0.08543              
 -108.06              0.10166              
 -108.08              0.11025              
 -108.1               0.10870              
 -108.12              0.10467              
 -108.14              0.10039              
 -108.16              0.09596              
 -108.18              0.09216              
 -108.2               0.08899              
 -108.22              0.08268              
 -108.24              0.07476              
 -108.26              0.07618              
 -108.28              0.08214              
 -108.3               0.08942              
 -108.32              0.09336              
 -108.34              0.09321              
 -108.36              0.08959              
 -108.38              0.09011              
 -108.4               0.08998              
 -108.42              0.09001              
 -108.44              0.09000              
 -108.46              0.09000              
 -108.48              0.09000              
 -108.5               0.09000              
 -108.52              0.09001              
 -108.54              0.08999              
 -108.56              0.09015              
 -108.58              0.08930              
 -108.6               0.08702              
 -108.62              0.08394              
 -108.64              0.07773              
 -108.66              0.06505              
 -108.68              0.05876              
 -108.7               0.05469              
 -108.72              0.04915              
 -108.74              0.04568              
 -108.76              0.04543              
 -108.78              0.04836              
 -108.8               0.05756              
 -108.82              0.06429              
 -108.84              0.06848              
 -108.86              0.07759              
 -108.88              0.08435              
 -108.9               0.08853              
 -108.92              0.09765              
 -108.94              0.10507              
 -108.96              0.10420              
 -108.98              0.09795              
 -109.                0.08857              
 -109.02              0.08037              
 -109.04              0.07096              
 -109.06              0.05764              
 -109.08              0.04707              
 -109.1               0.04295              
 -109.12              0.04019              
 -109.14              0.03853              
 -109.16              0.04302              
 -109.18              0.04766              
 -109.2               0.05420              
 -109.22              0.06229              
 -109.24              0.06805              
 -109.26              0.07248              
 -109.28              0.07561              
 -109.3               0.07523              
 -109.32              0.07533              
 -109.34              0.07528              
 -109.36              0.07565              
 -109.38              0.07328              
 -109.4               0.06462              
 -109.42              0.06040              
 -109.44              0.06057              
 -109.46              0.06087              
 -109.48              0.06702              
 -109.5               0.07365              
 -109.52              0.07546              
 -109.54              0.07535              
 -109.56              0.07506              
 -109.58              0.06850              
 -109.6               0.05456              
 -109.62              0.04385              
 -109.64              0.03932              
 -109.66              0.03399              
 -109.68              0.03060              
 -109.7               0.03263              
 -109.72              0.03716              
 -109.74              0.04316              
 -109.76              0.05072              
 -109.78              0.05856              
 -109.8               0.06091              
 -109.82              0.06024              
 -109.84              0.05683              
 -109.86              0.05269              
 -109.88              0.04836              
 -109.9               0.04485              
 -109.92              0.04303              
 -109.94              0.03962              
 -109.96              0.03408              
 -109.98              0.02511              
 -110.                0.01837              
 -110.02              0.01624              
 -110.04              0.01646              
 -110.06              0.01643              
 -110.08              0.01617              
 -110.1               0.01763              
 -110.12              0.02216              
 -110.14              0.02807              
 -110.16              0.03543              
 -110.18              0.04344              
 -110.2               0.04667              
 -110.22              0.04865              
 -110.24              0.05159              
 -110.26              0.05317              
 -110.28              0.04846              
 -110.3               0.04496              
 -110.32              0.04324              
 -110.34              0.03921              
 -110.36              0.03078              
 -110.38              0.02286              
 -110.4               0.01849              
 -110.42              0.01332              
 -110.44              0.00755              
 -110.46              0.00159              
 -110.48             -0.00281              
 -110.5              -0.00597              
 -110.52             -0.00559              
 -110.54             -0.00148              
 -110.56              0.00910              
 -110.58              0.02592              
 -110.6               0.03230              
 -110.62              0.03817              
 -110.64              0.04462              
 -110.66              0.0412               
 -110.68              0.03297              
 -110.7               0.01850              
 -110.72              0.00346              
 -110.74             -0.00465              
 -110.76             -0.00579              
 -110.78             -0.00537              
 -110.8               0.00077              
 -110.82              0.01646              
 -110.84              0.03195              
 -110.86              0.04186              
 -110.88              0.05053              
 -110.9               0.05455              
 -110.92              0.05704              
 -110.94              0.05495              
 -110.96              0.05306              
 -110.98              0.05317              
 -111.                0.05404              
 -111.02              0.05848              
 -111.04              0.06086              
 -111.06              0.06538              
 -111.08              0.07199              
 -111.1               0.06458              
 -111.12              0.05409              
 -111.14              0.05012              
 -111.16              0.04262              
 -111.18              0.02965              
 -111.2               0.01890              
 -111.22              0.01368              
 -111.24              0.00498              
 -111.26              0.00199              
 -111.28              0.00589              
 -111.3               0.01525              
 -111.32              0.02876              
 -111.34              0.03994              
 -111.36              0.04471              
 -111.38              0.04987              
 -111.4               0.05418              
 -111.42              0.05761              
 -111.44              0.05803              
 -111.46              0.05428              
 -111.48              0.04932              
 -111.5               0.05102              
 -111.52              0.05862              
 -111.54              0.06062              
 -111.56              0.06102              
 -111.58              0.06441              
 -111.6               0.06783              
 -111.62              0.06188              
 -111.64              0.05485              
 -111.66              0.04977              
 -111.68              0.04578              
 -111.7               0.04155              
 -111.72              0.03679              
 -111.74              0.03030              
 -111.76              0.01826              
 -111.78              0.00540              
 -111.8              -0.00278              
 -111.82             -0.00683              
 -111.84             -0.01178              
 -111.86             -0.01647              
 -111.88             -0.01875              
 -111.9              -0.02052              
 -111.92             -0.02046              
 -111.94             -0.01962              
 -111.96             -0.01728              
 -111.98             -0.01423              
 -112.               -0.00760              
 -112.02              0.00406              
 -112.04              0.01478              
 -112.06              0.02986              
 -112.08              0.03690              
 -112.1               0.03922              
 -112.12              0.04847              
 -112.14              0.05593              
 -112.16              0.06199              
 -112.18              0.06642              
 -112.2               0.06807              
 -112.22              0.06738              
 -112.24              0.06117              
 -112.26              0.05478              
 -112.28              0.05178              
 -112.3               0.04487              
 -112.32              0.03728              
 -112.34              0.03281              
 -112.36              0.02790              
 -112.38              0.02558              
 -112.4               0.02365              
 -112.42              0.02417              
 -112.44              0.03079              
 -112.46              0.04002              
 -112.48              0.04869              
 -112.5               0.06202              
 -112.52              0.08290              
 -112.54              0.09187              
 -112.56              0.09567              
 -112.58              0.09631              
 -112.6               0.08947              
 -112.62              0.08110              
 -112.64              0.07160              
 -112.66              0.06175              
 -112.68              0.05288              
 -112.7               0.04168              
 -112.72              0.03327              
 -112.74              0.02497              
 -112.76              0.01776              
 -112.78              0.00586              
 -112.8              -0.00595              
 -112.82             -0.01476              
 -112.84             -0.02103              
 -112.86             -0.02023              
 -112.88             -0.02064              
 -112.9              -0.02033              
 -112.92             -0.01098              
 -112.94              0.00177              
 -112.96              0.01255              
 -112.98              0.02429              
 -113.                0.03843              
 -113.02              0.05063              
 -113.04              0.05410              
 -113.06              0.06022              
 -113.08              0.06682              
 -113.1               0.06816              
 -113.12              0.06752              
 -113.14              0.06272              
 -113.16              0.05958              
 -113.18              0.0574               
 -113.2               0.04990              
 -113.22              0.04106              
 -113.24              0.03760              
 -113.26              0.03247              
 -113.28              0.02780              
 -113.3               0.02539              
 -113.32              0.02377              
 -113.34              0.03082              
 -113.36              0.04191              
 -113.38              0.04654              
 -113.4               0.04965              
 -113.42              0.05352              
 -113.44              0.05282              
 -113.46              0.05450              
 -113.48              0.05933              
 -113.5               0.06896              
 -113.52              0.08014              
 -113.54              0.08784              
 -113.56              0.09877              
 -113.58              0.11193              
 -113.6               0.12291              
 -113.62              0.13537              
 -113.64              0.14833              
 -113.66              0.16795              
 -113.68              0.18936              
 -113.7               0.21713              
 -113.72              0.25062              
 -113.74              0.27560              
 -113.76              0.31676              
 -113.78              0.36501              
 -113.8               0.41188              
 -113.82              0.46110              
 -113.84              0.51753              
 -113.86              0.60032              
 -113.88              0.69138              
 -113.9               0.80971              
 -113.92              0.97736              
 -113.94              1.1398               
 -113.96              1.27953              
 -113.98              1.48003              
 -114.                1.70529              
 -114.02              1.9704               
 -114.04              2.25698              
 -114.06              2.53602              
 -114.08              2.86525              
 -114.1               3.22738              
 -114.12              3.62928              
 -114.14              3.97945              
 -114.16              4.40628              
 -114.18              4.85112              
 -114.2               5.24712              
 -114.22              5.69084              
 -114.24              6.07913              
 -114.26              6.4613               
 -114.28              6.77582              
 -114.3               6.97279              
 -114.32              7.01399              
 -114.34              6.91231              
 -114.36              6.70212              
 -114.38              6.41902              
 -114.4               6.0156               
 -114.42              5.64997              
 -114.44              5.20528              
 -114.46              4.68078              
 -114.48              4.19404              
 -114.5               3.74881              
 -114.52              3.35536              
 -114.54              2.97035              
 -114.56              2.74007              
 -114.58              2.48549              
 -114.6               2.22757              
 -114.62              2.02577              
 -114.64              1.80297              
 -114.66              1.61328              
 -114.68              1.4518               
 -114.7               1.32835              
 -114.72              1.22339              
 -114.74              1.1179               
 -114.76              1.05162              
 -114.78              0.96124              
 -114.8               0.88357              
 -114.82              0.81913              
 -114.84              0.75371              
 -114.86              0.69684              
 -114.88              0.64494              
 -114.9               0.59735              
 -114.92              0.56230              
 -114.94              0.53292              
 -114.96              0.50473              
 -114.98              0.48294              
 -115.                0.45873              
 -115.02              0.43143              
 -115.04              0.40899              
 -115.06              0.39127              
 -115.08              0.36393              
 -115.1               0.33942              
 -115.12              0.31713              
 -115.14              0.29531              
 -115.16              0.28323              
 -115.18              0.26856              
 -115.2               0.25236              
 -115.22              0.23945              
 -115.24              0.22962              
 -115.26              0.22108              
 -115.28              0.21250              
 -115.3               0.20428              
 -115.32              0.19278              
 -115.34              0.18196              
 -115.36              0.17325              
 -115.38              0.16488              
 -115.4               0.16490              
 -115.42              0.17005              
 -115.44              0.17505              
 -115.46              0.17899              
 -115.48              0.18393              
 -115.5               0.18440              
 -115.52              0.17954              
 -115.54              0.17283              
 -115.56              0.16114              
 -115.58              0.14382              
 -115.6               0.12746              
 -115.62              0.11396              
 -115.64              0.10394              
 -115.66              0.09668              
 -115.68              0.09881              
 -115.7               0.11072              
 -115.72              0.12483              
 -115.74              0.14025              
 -115.76              0.15827              
 -115.78              0.16393              
 -115.8               0.16291              
 -115.82              0.16046              
 -115.84              0.15341              
 -115.86              0.14412              
 -115.88              0.13549              
 -115.9               0.12877              
 -115.92              0.12639              
 -115.94              0.12310              
 -115.96              0.11908              
 -115.98              0.11344              
 -116.                0.09956              
 -116.02              0.08820              
 -116.04              0.07554              
 -116.06              0.05937              
 -116.08              0.05231              
 -116.1               0.04798              
 -116.12              0.04600              
 -116.14              0.05314              
 -116.16              0.06108              
 -116.18              0.07084              
 -116.2               0.08051              
 -116.22              0.07973              
 -116.24              0.07337              
 -116.26              0.06776              
 -116.28              0.06787              
 -116.3               0.06900              
 -116.32              0.07346              
 -116.34              0.07525              
 -116.36              0.07534              
 -116.38              0.07982              
 -116.4               0.08399              
 -116.42              0.08805              
 -116.44              0.09003              
 -116.46              0.09002              
 -116.48              0.09514              
 -116.5               0.10262              
 -116.52              0.10475              
 -116.54              0.10111              
 -116.56              0.09736              
 -116.58              0.09628              
 -116.6               0.07952              
 -116.62              0.06048              
 -116.64              0.04749              
 -116.66              0.03764              
 -116.68              0.03000              
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##END=
