##TITLE=	"29Si MAS NMR spectrum of nonbasic hydrosodalite 6:0:8"
##JCAMP-DX=	5.01
##DATA TYPE=	NMR SPECTRUM
##DATA CLASS=	XYDATA
##ORIGIN=	"Engelhardt et al. J. Am. Chem. Soc., 114, 1173-1182 (1992) Figure 10e"
##OWNER=	"processed by H. Koller, University of Münster"
##LONG DATE=	15.07.2022 15:20
##SOURCE REFERENCE=	SOD-29Si-Engelhardt-1992_SOD_608
##DATA PROCESSING=	"Spectrum digitized with WebPlotDigitizer and deconvoluted with dmfit: D. Massiot et al., Magn. Reson. Chem., 40, 70-76 (2002)"
	
$$Sample information	
##NAMES=	SOD
##NAMES=	nonbasic hydrosodalite
##NAMES=	nonbasic hydrosodalite
##SAMPLE DESCRIPTION=	"nonbasic hydrosodalite prepared from basic hydrosodalite by washing with water"
##TEMPERATURE=	N.A.
	
"
$$Bibliographic information"	
##$AUTHORS=	"Engelhardt, G., Felsche, J., Sieger, P."
##$TITLE=	"The Hydrosodalite System Na6+x[SiAlO4]6(OH)x*nH2O: Formation, Phase Composition, and De- and Rehydration Studied by 1H, 23Na, and 29Si MAS-NMR Spectroscopy in Tandem with Thermal Analysis, X-ray Diffraction, and IR Spectroscopy"
##$JOURNAL=	J. Am. Chem. Soc.
##$VOLUME=	114
##$PAGES=	1173-1182
##$YEAR=	1992
##$DOI=	10.1021/ja00030a008
##$FIGURE=	Figure 10e
	
$$Peak information	(Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=	1
##$PEAK TSITES=	0                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                        
##$PEAK LABELS=	A                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                       
##$Q TYPE=	Q4(4Al)                                                                                                                                                                        
##$PEAK POSITIONS=	-82.99                                                                                                                                                                                            
##$PEAK AREAS=	1                                                                                                                                                                                                                                              
##$PEAK WIDTHS=	1.4                                                                                                                                                                                                                                                                  
##$PEAK SHAPES=	0.6                                                                                                                                                                                                                                                                  
##$PEAK_CQ=	
##$PEAK_etaQ=	
##$NUMBERING REF=	
##$ASSIGN REF=	
##$ASSIGN METHOD=	
	
$$Spectrum acquisition information	
##.OBSERVE NUCLEUS=	29Si
##.OBSERVE FREQUENCY=	79.49
##.PULSE SEQUENCE=	single pulse
##.MAS FREQUENCY=	4
	
$$Spectrum data information	
##XUNITS=	ppm
##YUNITS=	arbitrary units
##FIRSTX=	-60.10
##LASTX=	-109.90
##XFACTOR=	1
##YFACTOR=	1
##NPOINTS=	997
##FIRSTY=	0.0033
	
$$Spectrum data	
##XYDATA=	(X++(Y..Y))
-60.1000	0.0034
-60.1500	0.0020
-60.2000	0.0020
-60.2500	0.0020
-60.3000	0.0020
-60.3500	0.0024
-60.4000	0.0030
-60.4500	0.0030
-60.5000	0.0030
-60.5500	0.0024
-60.6000	0.0020
-60.6500	0.0019
-60.7000	0.0012
-60.7500	0.0010
-60.8000	0.0015
-60.8500	0.0020
-60.9000	0.0020
-60.9500	0.0020
-61.0000	0.0020
-61.0500	0.0020
-61.1000	0.0020
-61.1500	0.0020
-61.2000	0.0020
-61.2500	0.0020
-61.3000	0.0020
-61.3500	0.0020
-61.4000	0.0020
-61.4500	0.0020
-61.5000	0.0020
-61.5500	0.0021
-61.6000	0.0033
-61.6500	0.0042
-61.7000	0.0048
-61.7500	0.0049
-61.8000	0.0049
-61.8500	0.0041
-61.9000	0.0025
-61.9500	0.0020
-62.0000	0.0021
-62.0500	0.0028
-62.1000	0.0032
-62.1500	0.0040
-62.2000	0.0047
-62.2500	0.0049
-62.3000	0.0049
-62.3500	0.0049
-62.4000	0.0049
-62.4500	0.0048
-62.5000	0.0039
-62.5500	0.0030
-62.6000	0.0026
-62.6500	0.0018
-62.7000	0.0002
-62.7500	0.0001
-62.8000	0.0006
-62.8500	0.0014
-62.9000	0.0030
-62.9500	0.0034
-63.0000	0.0042
-63.0500	0.0048
-63.1000	0.0049
-63.1500	0.0049
-63.2000	0.0049
-63.2500	0.0049
-63.3000	0.0049
-63.3500	0.0048
-63.4000	0.0044
-63.4500	0.0039
-63.5000	0.0038
-63.5500	0.0032
-63.6000	0.0030
-63.6500	0.0030
-63.7000	0.0030
-63.7500	0.0030
-63.8000	0.0030
-63.8500	0.0030
-63.9000	0.0030
-63.9500	0.0026
-64.0000	0.0021
-64.0500	0.0020
-64.1000	0.0020
-64.1500	0.0024
-64.2000	0.0030
-64.2500	0.0030
-64.3000	0.0030
-64.3500	0.0030
-64.4000	0.0030
-64.4500	0.0028
-64.5000	0.0021
-64.5500	0.0020
-64.6000	0.0020
-64.6500	0.0020
-64.7000	0.0020
-64.7500	0.0020
-64.8000	0.0020
-64.8500	0.0020
-64.9000	0.0021
-64.9500	0.0039
-65.0000	0.0051
-65.0500	0.0058
-65.1000	0.0058
-65.1500	0.0072
-65.2000	0.0077
-65.2500	0.0077
-65.3000	0.0077
-65.3500	0.0077
-65.4000	0.0072
-65.4500	0.0065
-65.5000	0.0058
-65.5500	0.0050
-65.6000	0.0016
-65.6500	0.0001
-65.7000	0.0001
-65.7500	0.0005
-65.8000	0.0021
-65.8500	0.0028
-65.9000	0.0030
-65.9500	0.0030
-66.0000	0.0030
-66.0500	0.0030
-66.1000	0.0030
-66.1500	0.0030
-66.2000	0.0030
-66.2500	0.0030
-66.3000	0.0030
-66.3500	0.0032
-66.4000	0.0040
-66.4500	0.0047
-66.5000	0.0049
-66.5500	0.0049
-66.6000	0.0049
-66.6500	0.0048
-66.7000	0.0042
-66.7500	0.0034
-66.8000	0.0024
-66.8500	0.0017
-66.9000	0.0009
-66.9500	0.0002
-67.0000	0.0001
-67.0500	0.0002
-67.1000	0.0003
-67.1500	0.0005
-67.2000	0.0007
-67.2500	0.0009
-67.3000	0.0011
-67.3500	0.0014
-67.4000	0.0015
-67.4500	0.0018
-67.5000	0.0025
-67.5500	0.0030
-67.6000	0.0030
-67.6500	0.0029
-67.7000	0.0024
-67.7500	0.0017
-67.8000	0.0009
-67.8500	0.0002
-67.9000	0.0001
-67.9500	0.0001
-68.0000	0.0001
-68.0500	0.0001
-68.1000	0.0001
-68.1500	0.0001
-68.2000	0.0001
-68.2500	0.0001
-68.3000	0.0001
-68.3500	0.0001
-68.4000	0.0001
-68.4500	0.0001
-68.5000	0.0001
-68.5500	0.0001
-68.6000	0.0001
-68.6500	0.0001
-68.7000	0.0001
-68.7500	0.0001
-68.8000	0.0001
-68.8500	0.0001
-68.9000	0.0001
-68.9500	0.0001
-69.0000	0.0001
-69.0500	0.0001
-69.1000	0.0001
-69.1500	0.0001
-69.2000	0.0001
-69.2500	0.0001
-69.3000	0.0001
-69.3500	0.0001
-69.4000	0.0001
-69.4500	0.0001
-69.5000	0.0006
-69.5500	0.0015
-69.6000	0.0029
-69.6500	0.0040
-69.7000	0.0049
-69.7500	0.0051
-69.8000	0.0076
-69.8500	0.0083
-69.9000	0.0087
-69.9500	0.0087
-70.0000	0.0087
-70.0500	0.0087
-70.1000	0.0073
-70.1500	0.0052
-70.2000	0.0019
-70.2500	0.0018
-70.3000	0.0011
-70.3500	0.0004
-70.4000	0.0001
-70.4500	0.0001
-70.5000	0.0001
-70.5500	0.0001
-70.6000	0.0007
-70.6500	0.0011
-70.7000	0.0013
-70.7500	0.0019
-70.8000	0.0020
-70.8500	0.0020
-70.9000	0.0020
-70.9500	0.0020
-71.0000	0.0020
-71.0500	0.0020
-71.1000	0.0023
-71.1500	0.0029
-71.2000	0.0035
-71.2500	0.0043
-71.3000	0.0050
-71.3500	0.0057
-71.4000	0.0059
-71.4500	0.0063
-71.5000	0.0070
-71.5500	0.0086
-71.6000	0.0106
-71.6500	0.0115
-71.7000	0.0119
-71.7500	0.0119
-71.8000	0.0119
-71.8500	0.0116
-71.9000	0.0101
-71.9500	0.0094
-72.0000	0.0088
-72.0500	0.0087
-72.1000	0.0087
-72.1500	0.0079
-72.2000	0.0047
-72.2500	0.0040
-72.3000	0.0033
-72.3500	0.0029
-72.4000	0.0032
-72.4500	0.0039
-72.5000	0.0047
-72.5500	0.0049
-72.6000	0.0049
-72.6500	0.0049
-72.7000	0.0049
-72.7500	0.0049
-72.8000	0.0049
-72.8500	0.0051
-72.9000	0.0058
-72.9500	0.0058
-73.0000	0.0058
-73.0500	0.0055
-73.1000	0.0049
-73.1500	0.0049
-73.2000	0.0048
-73.2500	0.0053
-73.3000	0.0058
-73.3500	0.0058
-73.4000	0.0073
-73.4500	0.0082
-73.5000	0.0089
-73.5500	0.0104
-73.6000	0.0121
-73.6500	0.0141
-73.7000	0.0147
-73.7500	0.0142
-73.8000	0.0138
-73.8500	0.0138
-73.9000	0.0133
-73.9500	0.0113
-74.0000	0.0096
-74.0500	0.0060
-74.1000	0.0058
-74.1500	0.0054
-74.2000	0.0047
-74.2500	0.0030
-74.3000	0.0030
-74.3500	0.0030
-74.4000	0.0034
-74.4500	0.0058
-74.5000	0.0059
-74.5500	0.0064
-74.6000	0.0076
-74.6500	0.0096
-74.7000	0.0096
-74.7500	0.0096
-74.8000	0.0097
-74.8500	0.0094
-74.9000	0.0088
-74.9500	0.0087
-75.0000	0.0086
-75.0500	0.0076
-75.1000	0.0009
-75.1500	0.0022
-75.2000	0.0029
-75.2500	0.0059
-75.3000	0.0086
-75.3500	0.0087
-75.4000	0.0087
-75.4500	0.0092
-75.5000	0.0097
-75.5500	0.0096
-75.6000	0.0096
-75.6500	0.0096
-75.7000	0.0087
-75.7500	0.0075
-75.8000	0.0069
-75.8500	0.0068
-75.9000	0.0062
-75.9500	0.0058
-76.0000	0.0058
-76.0500	0.0058
-76.1000	0.0067
-76.1500	0.0071
-76.2000	0.0073
-76.2500	0.0080
-76.3000	0.0083
-76.3500	0.0104
-76.4000	0.0112
-76.4500	0.0122
-76.5000	0.0179
-76.5500	0.0191
-76.6000	0.0199
-76.6500	0.0203
-76.7000	0.0193
-76.7500	0.0177
-76.8000	0.0167
-76.8500	0.0157
-76.9000	0.0144
-76.9500	0.0088
-77.0000	0.0087
-77.0500	0.0083
-77.1000	0.0075
-77.1500	0.0049
-77.2000	0.0034
-77.2500	0.0030
-77.3000	0.0030
-77.3500	0.0030
-77.4000	0.0030
-77.4500	0.0029
-77.5000	0.0037
-77.5500	0.0051
-77.6000	0.0058
-77.6500	0.0065
-77.7000	0.0073
-77.7500	0.0080
-77.8000	0.0095
-77.8500	0.0109
-77.9000	0.0118
-77.9500	0.0119
-78.0000	0.0112
-78.0500	0.0098
-78.1000	0.0091
-78.1500	0.0090
-78.2000	0.0090
-78.2500	0.0094
-78.3000	0.0101
-78.3500	0.0109
-78.4000	0.0116
-78.4500	0.0119
-78.5000	0.0119
-78.5500	0.0125
-78.6000	0.0128
-78.6500	0.0128
-78.7000	0.0128
-78.7500	0.0126
-78.8000	0.0119
-78.8500	0.0112
-78.9000	0.0105
-78.9500	0.0097
-79.0000	0.0090
-79.0500	0.0087
-79.1000	0.0087
-79.1500	0.0087
-79.2000	0.0087
-79.2500	0.0089
-79.3000	0.0104
-79.3500	0.0131
-79.4000	0.0159
-79.4500	0.0173
-79.5000	0.0183
-79.5500	0.0191
-79.6000	0.0247
-79.6500	0.0265
-79.7000	0.0277
-79.7500	0.0288
-79.8000	0.0313
-79.8500	0.0326
-79.9000	0.0335
-79.9500	0.0356
-80.0000	0.0379
-80.0500	0.0397
-80.1000	0.0417
-80.1500	0.0446
-80.2000	0.0467
-80.2500	0.0482
-80.3000	0.0490
-80.3500	0.0502
-80.4000	0.0533
-80.4500	0.0577
-80.5000	0.0605
-80.5500	0.0635
-80.6000	0.0656
-80.6500	0.0677
-80.7000	0.0693
-80.7500	0.0719
-80.8000	0.0729
-80.8500	0.0760
-80.9000	0.0786
-80.9500	0.0830
-81.0000	0.0848
-81.0500	0.0859
-81.1000	0.0919
-81.1500	0.0966
-81.2000	0.0983
-81.2500	0.0993
-81.3000	0.1016
-81.3500	0.1092
-81.4000	0.1148
-81.4500	0.1176
-81.5000	0.1375
-81.5500	0.1490
-81.6000	0.1512
-81.6500	0.1542
-81.7000	0.1726
-81.7500	0.1837
-81.8000	0.1941
-81.8500	0.1986
-81.9000	0.2216
-81.9500	0.2293
-82.0000	0.2724
-82.0500	0.3154
-82.1000	0.3496
-82.1500	0.3772
-82.2000	0.4091
-82.2500	0.4587
-82.3000	0.5119
-82.3500	0.5181
-82.4000	0.5302
-82.4500	0.6011
-82.5000	0.6782
-82.5500	0.7376
-82.6000	0.8137
-82.6500	0.8459
-82.7000	0.8760
-82.7500	0.9286
-82.8000	0.9351
-82.8500	0.9742
-82.9000	1.0001
-82.9500	0.9867
-83.0000	0.9809
-83.0500	0.9752
-83.1000	0.9443
-83.1500	0.9015
-83.2000	0.8856
-83.2500	0.8663
-83.3000	0.8623
-83.3500	0.8411
-83.4000	0.7492
-83.4500	0.7157
-83.5000	0.7098
-83.5500	0.6414
-83.6000	0.5802
-83.6500	0.5520
-83.7000	0.5130
-83.7500	0.5053
-83.8000	0.4441
-83.8500	0.3785
-83.9000	0.3348
-83.9500	0.3296
-84.0000	0.3002
-84.0500	0.2573
-84.1000	0.2120
-84.1500	0.2110
-84.2000	0.2078
-84.2500	0.1677
-84.3000	0.1599
-84.3500	0.1437
-84.4000	0.1138
-84.4500	0.1057
-84.5000	0.1051
-84.5500	0.0998
-84.6000	0.0890
-84.6500	0.0822
-84.7000	0.0816
-84.7500	0.0803
-84.8000	0.0776
-84.8500	0.0734
-84.9000	0.0710
-84.9500	0.0659
-85.0000	0.0590
-85.0500	0.0577
-85.1000	0.0565
-85.1500	0.0545
-85.2000	0.0430
-85.2500	0.0424
-85.3000	0.0414
-85.3500	0.0396
-85.4000	0.0355
-85.4500	0.0349
-85.5000	0.0344
-85.5500	0.0299
-85.6000	0.0242
-85.6500	0.0238
-85.7000	0.0216
-85.7500	0.0186
-85.8000	0.0164
-85.8500	0.0154
-85.9000	0.0146
-85.9500	0.0103
-86.0000	0.0087
-86.0500	0.0087
-86.1000	0.0087
-86.1500	0.0091
-86.2000	0.0108
-86.2500	0.0109
-86.3000	0.0113
-86.3500	0.0119
-86.4000	0.0125
-86.4500	0.0132
-86.5000	0.0139
-86.5500	0.0147
-86.6000	0.0154
-86.6500	0.0166
-86.7000	0.0177
-86.7500	0.0182
-86.8000	0.0176
-86.8500	0.0170
-86.9000	0.0151
-86.9500	0.0099
-87.0000	0.0088
-87.0500	0.0087
-87.1000	0.0082
-87.1500	0.0074
-87.2000	0.0059
-87.2500	0.0058
-87.3000	0.0058
-87.3500	0.0055
-87.4000	0.0047
-87.4500	0.0030
-87.5000	0.0030
-87.5500	0.0030
-87.6000	0.0032
-87.6500	0.0038
-87.7000	0.0039
-87.7500	0.0045
-87.8000	0.0052
-87.8500	0.0061
-87.9000	0.0086
-87.9500	0.0087
-88.0000	0.0087
-88.0500	0.0101
-88.1000	0.0118
-88.1500	0.0120
-88.2000	0.0127
-88.2500	0.0128
-88.3000	0.0127
-88.3500	0.0118
-88.4000	0.0110
-88.4500	0.0109
-88.5000	0.0109
-88.5500	0.0104
-88.6000	0.0081
-88.6500	0.0077
-88.7000	0.0073
-88.7500	0.0058
-88.8000	0.0058
-88.8500	0.0064
-88.9000	0.0072
-88.9500	0.0077
-89.0000	0.0077
-89.0500	0.0077
-89.1000	0.0077
-89.1500	0.0077
-89.2000	0.0076
-89.2500	0.0069
-89.3000	0.0031
-89.3500	0.0021
-89.4000	0.0015
-89.4500	0.0008
-89.5000	0.0002
-89.5500	0.0001
-89.6000	0.0001
-89.6500	0.0005
-89.7000	0.0012
-89.7500	0.0019
-89.8000	0.0020
-89.8500	0.0027
-89.9000	0.0048
-89.9500	0.0049
-90.0000	0.0049
-90.0500	0.0049
-90.1000	0.0049
-90.1500	0.0049
-90.2000	0.0043
-90.2500	0.0035
-90.3000	0.0026
-90.3500	0.0025
-90.4000	0.0023
-90.4500	0.0022
-90.5000	0.0020
-90.5500	0.0019
-90.6000	0.0017
-90.6500	0.0015
-90.7000	0.0013
-90.7500	0.0011
-90.8000	0.0010
-90.8500	0.0008
-90.9000	0.0006
-90.9500	0.0005
-91.0000	0.0003
-91.0500	0.0002
-91.1000	0.0001
-91.1500	0.0001
-91.2000	0.0005
-91.2500	0.0013
-91.3000	0.0019
-91.3500	0.0020
-91.4000	0.0020
-91.4500	0.0023
-91.5000	0.0029
-91.5500	0.0030
-91.6000	0.0033
-91.6500	0.0040
-91.7000	0.0048
-91.7500	0.0049
-91.8000	0.0049
-91.8500	0.0046
-91.9000	0.0030
-91.9500	0.0030
-92.0000	0.0029
-92.0500	0.0023
-92.1000	0.0016
-92.1500	0.0009
-92.2000	0.0007
-92.2500	0.0007
-92.3000	0.0006
-92.3500	0.0006
-92.4000	0.0005
-92.4500	0.0005
-92.5000	0.0004
-92.5500	0.0004
-92.6000	0.0003
-92.6500	0.0003
-92.7000	0.0002
-92.7500	0.0002
-92.8000	0.0001
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##END=	
