##TITLE=              31P MAS NMR spectrum of calcined AlPO-SOD
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Roux et al. J. Phys. Chem. B, 105, 9083-9092 (2001) Figure 15a
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/22 13:30:51
##SOURCE REFERENCE=   SOD-31P-Roux-2001-calcined
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              SOD
##NAMES=              AlPO-SOD
##NAMES=              AlPO-20
##SAMPLE DESCRIPTION= AlPO-SOD, calcined

$$Bibliographic information 
##$AUTHORS=           Roux, M., Marichal, C., Paillaud, J.L., Fernandez, C., Baerlocher, C., ChA~(c)zeau, J.M.
##$TITLE=             Structural investigation by multinuclear solid state NMR and X-ray diffraction of as-synthesized, dehydrated, and calcined ALPO4-SOD
##$JOURNAL=           Journal of Physical Chemistry B
##$VOLUME=            105
##$PAGES=             9083-9092
##$YEAR=              2001
##$DOI=               10.1021/jp010723k
##$FIGURE=            Figure 15a

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         1
##$PEAK LABELS=        P1        
##$PEAK TSITES=        T1        
##$PEAK POSITIONS=    -28.88     
##$PEAK AREAS=         1.        
##$PEAK WIDTHS=        2.41214   
##$PEAK SHAPES=        0.45324   
##$NUMBERING REF=     Roux et al. J. Phys. Chem. B, 105, 9083-9092 (2001)
##$ASSIGN REF=        Roux et al. J. Phys. Chem. B, 105, 9083-9092 (2001) Figure 15a, Table 8
##$ASSIGN METHOD=     single peak
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 161.9
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     3500-8000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              39.8                 
##LASTX=              -97.9                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            460
##FIRSTY=             -0.00089              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  39.8               -0.00089              
  39.5               -0.00139              
  39.2               -0.00150              
  38.9               -0.00126              
  38.6               -0.00131              
  38.3               -0.00150              
  38.                -0.00151              
  37.7               -0.00117              
  37.4               -0.00119              
  37.1               -0.00125              
  36.8               -0.00089              
  36.5               -0.00061              
  36.2               -0.00087              
  35.9               -0.00124              
  35.6               -0.00119              
  35.3               -0.00118              
  35.                -0.00128              
  34.7               -0.00085              
  34.4               -0.00073              
  34.1               -0.00131              
  33.8               -0.00153              
  33.5               -0.00120              
  33.2               -0.00110              
  32.9               -0.00113              
  32.6               -0.00111              
  32.3               -0.00122              
  32.                -0.00147              
  31.7               -0.00157              
  31.4               -0.00155              
  31.1               -0.00156              
  30.8               -0.00155              
  30.5               -0.00157              
  30.2               -0.00147              
  29.9               -0.00131              
  29.6               -0.00136              
  29.3               -0.00122              
  29.                -0.00109              
  28.7               -0.00113              
  28.4               -0.00109              
  28.1               -0.00123              
  27.8               -0.00149              
  27.5               -0.00156              
  27.2               -0.00155              
  26.9               -0.00158              
  26.6               -0.00142              
  26.3               -0.00116              
  26.                -0.00111              
  25.7               -0.00111              
  25.4               -0.00117              
  25.1               -0.00132              
  24.8               -0.00147              
  24.5               -0.00158              
  24.2               -0.00145              
  23.9               -0.00120              
  23.6               -0.00110              
  23.3               -0.00113              
  23.                -0.00111              
  22.7               -0.00117              
  22.4               -0.00132              
  22.1               -0.00148              
  21.8               -0.00156              
  21.5               -0.00156              
  21.2               -0.00149              
  20.9               -0.00135              
  20.6               -0.00116              
  20.3               -0.00120              
  20.                -0.00135              
  19.7               -0.00120              
  19.4               -0.00112              
  19.1               -0.00108              
  18.8               -0.00074              
  18.5               -0.00080              
  18.2               -0.00107              
  17.9               -0.00113              
  17.6               -0.00110              
  17.3               -0.00118              
  17.                -0.00126              
  16.7               -0.00094              
  16.4               -0.00064              
  16.1               -0.00070              
  15.8               -0.00062              
  15.5               -0.00046              
  15.2                0.00011              
  14.9                0.00092              
  14.6                0.00150              
  14.3                0.00192              
  14.                 0.00246              
  13.7                0.00285              
  13.4                0.00274              
  13.1                0.00221              
  12.8                0.00149              
  12.5                0.00046              
  12.2               -0.00055              
  11.9               -0.00064              
  11.6               -0.00053              
  11.3               -0.00086              
  11.                -0.00116              
  10.7               -0.00111              
  10.4               -0.00112              
  10.1               -0.00112              
  9.8                -0.00112              
  9.5                -0.00111              
  9.2                -0.00117              
  8.9                -0.00131              
  8.6                -0.00147              
  8.3                -0.00157              
  8.                 -0.00155              
  7.7                -0.00155              
  7.4                -0.00157              
  7.1                -0.00148              
  6.8                -0.00123              
  6.5                -0.00110              
  6.2                -0.00111              
  5.9                -0.00117              
  5.6                -0.00142              
  5.3                -0.00149              
  5.                 -0.00121              
  4.7                -0.00109              
  4.4                -0.00118              
  4.1                -0.00148              
  3.8                -0.00137              
  3.5                -0.00086              
  3.2                -0.00120              
  2.9                -0.00157              
  2.6                -0.00119              
  2.3                -0.00111              
  2.                 -0.00110              
  1.7                -0.00122              
  1.4                -0.00132              
  1.1                -0.00092              
  0.8                -0.00065              
  0.5                -0.00068              
  0.2                -0.00071              
 -0.1                -0.00105              
 -0.4                -0.00102              
 -0.7                -0.00072              
 -1.                 -0.00076              
 -1.3                -0.00094              
 -1.6                -0.00075              
 -1.9                -0.00074              
 -2.2                -0.00086              
 -2.5                -0.00075              
 -2.8                -0.00067              
 -3.1                -0.00069              
 -3.4                -0.00068              
 -3.7                -0.00069              
 -4.                 -0.00063              
 -4.3                -0.00024              
 -4.6                 0.00025              
 -4.9                 0.00065              
 -5.2                 0.00137              
 -5.5                 0.00241              
 -5.8                 0.00507              
 -6.1                 0.00830              
 -6.4                 0.01195              
 -6.7                 0.01611              
 -7.                  0.01981              
 -7.3                 0.02248              
 -7.6                 0.02353              
 -7.9                 0.02080              
 -8.2                 0.01699              
 -8.5                 0.01330              
 -8.8                 0.00976              
 -9.1                 0.00678              
 -9.4                 0.00395              
 -9.7                 0.00252              
 -10.                 0.00163              
 -10.3                0.00089              
 -10.6                0.00029              
 -10.9               -0.00018              
 -11.2               -0.00026              
 -11.5               -0.00023              
 -11.8               -0.00030              
 -12.1               -0.00060              
 -12.4               -0.00106              
 -12.7               -0.00113              
 -13.                -0.00112              
 -13.3               -0.00112              
 -13.6               -0.00112              
 -13.9               -0.00112              
 -14.2               -0.00112              
 -14.5               -0.00112              
 -14.8               -0.00112              
 -15.1               -0.00112              
 -15.4               -0.00113              
 -15.7               -0.00108              
 -16.                -0.00083              
 -16.3               -0.00064              
 -16.6               -0.00075              
 -16.9               -0.00085              
 -17.2               -0.00077              
 -17.5               -0.00066              
 -17.8               -0.00072              
 -18.1               -0.00050              
 -18.4               -0.00004              
 -18.7               -0.00004              
 -19.                -0.00039              
 -19.3               -0.00038              
 -19.6               -0.00025              
 -19.9               -0.00047              
 -20.2               -0.00036              
 -20.5                0.00012              
 -20.8                0.00019              
 -21.1                0.00020              
 -21.4                0.00055              
 -21.7                0.00097              
 -22.                 0.00106              
 -22.3                0.00105              
 -22.6                0.00105              
 -22.9                0.00105              
 -23.2                0.00105              
 -23.5                0.00106              
 -23.8                0.00104              
 -24.1                0.00113              
 -24.4                0.00137              
 -24.7                0.00156              
 -25.                 0.00168              
 -25.3                0.00227              
 -25.6                0.00337              
 -25.9                0.00396              
 -26.2                0.00787              
 -26.5                0.01475              
 -26.8                0.03623              
 -27.1                0.06454              
 -27.4                0.11629              
 -27.7                0.17898              
 -28.                 0.23491              
 -28.3                0.29197              
 -28.6                0.33472              
 -28.9                0.33279              
 -29.2                0.30338              
 -29.5                0.25085              
 -29.8                0.19841              
 -30.1                0.16747              
 -30.4                0.13358              
 -30.7                0.09876              
 -31.                 0.06976              
 -31.3                0.05766              
 -31.6                0.04488              
 -31.9                0.03636              
 -32.2                0.03012              
 -32.5                0.02497              
 -32.8                0.02193              
 -33.1                0.01844              
 -33.4                0.01607              
 -33.7                0.01338              
 -34.                 0.01090              
 -34.3                0.00895              
 -34.6                0.00733              
 -34.9                0.00607              
 -35.2                0.00475              
 -35.5                0.00363              
 -35.8                0.00268              
 -36.1                0.00192              
 -36.4                0.00144              
 -36.7                0.00142              
 -37.                 0.00114              
 -37.3                0.00105              
 -37.6                0.00100              
 -37.9                0.00067              
 -38.2                0.00031              
 -38.5                0.00039              
 -38.8                0.00075              
 -39.1                0.00076              
 -39.4                0.00025              
 -39.7                0.00017              
 -40.                 0.00018              
 -40.3                0.00018              
 -40.6                0.00018              
 -40.9                0.00018              
 -41.2                0.00018              
 -41.5                0.00018              
 -41.8                0.00017              
 -42.1                0.00023              
 -42.4               -0.00006              
 -42.7               -0.00052              
 -43.                -0.00050              
 -43.3               -0.00048              
 -43.6               -0.00032              
 -43.9               -0.00029              
 -44.2               -0.00047              
 -44.5               -0.00061              
 -44.8               -0.00071              
 -45.1               -0.00062              
 -45.4               -0.00051              
 -45.7               -0.00060              
 -46.                -0.00068              
 -46.3               -0.00078              
 -46.6               -0.00104              
 -46.9               -0.00113              
 -47.2               -0.00112              
 -47.5               -0.00106              
 -47.8               -0.00068              
 -48.1               -0.00020              
 -48.4                0.00107              
 -48.7                0.00307              
 -49.                 0.00552              
 -49.3                0.00945              
 -49.6                0.01322              
 -49.9                0.01643              
 -50.2                0.01987              
 -50.5                0.02061              
 -50.8                0.01935              
 -51.1                0.01647              
 -51.4                0.01353              
 -51.7                0.01134              
 -52.                 0.00862              
 -52.3                0.00651              
 -52.6                0.00496              
 -52.9                0.00381              
 -53.2                0.00340              
 -53.5                0.00269              
 -53.8                0.00217              
 -54.1                0.00184              
 -54.4                0.00159              
 -54.7                0.00141              
 -55.                 0.00128              
 -55.3                0.00111              
 -55.6                0.00106              
 -55.9                0.00096              
 -56.2                0.00060              
 -56.5               -0.00022              
 -56.8               -0.00067              
 -57.1                0.00007              
 -57.4                0.00007              
 -57.7               -0.00019              
 -58.                -0.00035              
 -58.3               -0.00051              
 -58.6               -0.00037              
 -58.9               -0.00022              
 -59.2               -0.00025              
 -59.5               -0.00026              
 -59.8               -0.00014              
 -60.1                0.00003              
 -60.4                0.00000              
 -60.7               -0.00026              
 -61.                -0.00059              
 -61.3               -0.00070              
 -61.6               -0.00068              
 -61.9               -0.00068              
 -62.2               -0.00068              
 -62.5               -0.00068              
 -62.8               -0.00068              
 -63.1               -0.00068              
 -63.4               -0.00068              
 -63.7               -0.00068              
 -64.                -0.00068              
 -64.3               -0.00068              
 -64.6               -0.00068              
 -64.9               -0.00068              
 -65.2               -0.00067              
 -65.5               -0.00074              
 -65.8               -0.00089              
 -66.1               -0.00107              
 -66.4               -0.00106              
 -66.7               -0.00083              
 -67.                -0.00087              
 -67.3               -0.00098              
 -67.6               -0.00083              
 -67.9               -0.00067              
 -68.2               -0.00068              
 -68.5               -0.00072              
 -68.8               -0.00096              
 -69.1               -0.00117              
 -69.4               -0.00100              
 -69.7               -0.00077              
 -70.                -0.00056              
 -70.3               -0.00007              
 -70.6                0.00070              
 -70.9                0.00150              
 -71.2                0.00210              
 -71.5                0.00236              
 -71.8                0.00271              
 -72.1                0.00276              
 -72.4                0.00261              
 -72.7                0.00240              
 -73.                 0.00202              
 -73.3                0.00151              
 -73.6                0.00095              
 -73.9                0.00045              
 -74.2                0.00025              
 -74.5                0.00018              
 -74.8                0.00014              
 -75.1               -0.00000              
 -75.4               -0.00016              
 -75.7               -0.00026              
 -76.                -0.00023              
 -76.3               -0.00031              
 -76.6               -0.00042              
 -76.9               -0.00031              
 -77.2               -0.00029              
 -77.5               -0.00058              
 -77.8               -0.00069              
 -78.1               -0.00073              
 -78.4               -0.00097              
 -78.7               -0.00115              
 -79.                -0.00106              
 -79.3               -0.00091              
 -79.6               -0.00075              
 -79.9               -0.00067              
 -80.2               -0.00069              
 -80.5               -0.00068              
 -80.8               -0.00068              
 -81.1               -0.00068              
 -81.4               -0.00068              
 -81.7               -0.00069              
 -82.                -0.00067              
 -82.3               -0.00075              
 -82.6               -0.00101              
 -82.9               -0.00101              
 -83.2               -0.00082              
 -83.5               -0.00090              
 -83.8               -0.00098              
 -84.1               -0.00078              
 -84.4               -0.00072              
 -84.7               -0.00089              
 -85.                -0.00104              
 -85.3               -0.00113              
 -85.6               -0.00114              
 -85.9               -0.00098              
 -86.2               -0.00072              
 -86.5               -0.00068              
 -86.8               -0.00066              
 -87.1               -0.00080              
 -87.4               -0.00106              
 -87.7               -0.00113              
 -88.                -0.00112              
 -88.3               -0.00112              
 -88.6               -0.00112              
 -88.9               -0.00112              
 -89.2               -0.00111              
 -89.5               -0.00114              
 -89.8               -0.00100              
 -90.1               -0.00077              
 -90.4               -0.00096              
 -90.7               -0.00110              
 -91.                -0.00072              
 -91.3               -0.00080              
 -91.6               -0.00110              
 -91.9               -0.00104              
 -92.2               -0.00078              
 -92.5               -0.00066              
 -92.8               -0.00071              
 -93.1               -0.00097              
 -93.4               -0.00109              
 -93.7               -0.00075              
 -94.                -0.00067              
 -94.3               -0.00068              
 -94.6               -0.00068              
 -94.9               -0.00067              
 -95.2               -0.00073              
 -95.5               -0.00088              
 -95.8               -0.00104              
 -96.1               -0.00113              
 -96.4               -0.00112              
 -96.7               -0.00111              
 -97.                -0.00113              
 -97.3               -0.00104              
 -97.6               -0.00078              
 -97.9               -0.00071              
##END=
