##TITLE=              31P MAS NMR spectrum of dehydrated as-made AlPO-SOD (with dimethylformamide template)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Roux et al. J. Phys. Chem. B, 105, 9083-9092 (2001) Figure 6b
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/22 13:26:34
##SOURCE REFERENCE=   SOD-31P-Roux-2001-dehydrated-asmade
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              SOD
##NAMES=              AlPO-SOD
##NAMES=              AlPO-20
##SAMPLE DESCRIPTION= AlPO-SOD, as-made, dehydrated

$$Bibliographic information 
##$AUTHORS=           Roux, M., Marichal, C., Paillaud, J.L., Fernandez, C., Baerlocher, C., Chezeau, J.M.
##$TITLE=             Structural investigation by multinuclear solid state NMR and X-ray diffraction of as-synthesized, dehydrated, and calcined ALPO4-SOD
##$JOURNAL=           Journal of Physical Chemistry B
##$VOLUME=            105
##$PAGES=             9083-9092
##$YEAR=              2001
##$DOI=               10.1021/jp010723k
##$FIGURE=            Figure 6b

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         9
##$PEAK LABELS=        A          B          C          D          E          F          G          H          I         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -37.0895   -36.8895   -36.5234   -35.7358   -33.4878   -33.2878   -32.2648   -32.0648   -31.8039   
##$PEAK AREAS=         1.         1.         1.         1.         1.         1.         1.         1.         1.        
##$PEAK WIDTHS=        2.46667    2.46667    2.46667    2.46667    2.46667    2.46667    2.46667    2.46667    2.46667   
##$PEAK SHAPES=        0.30452    0.30452    0.30452    0.30452    0.30452    0.30452    0.30452    0.30452    0.30452   
##$NUMBERING REF=     Paillaud et al. J. Phys. Chem. B, 109, 11893-11899 (2005)
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 161.9
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     3500-8000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              40                   
##LASTX=              -100.                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            281
##FIRSTY=             -0.05011              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  40                 -0.05011              
  39.5               -0.04490              
  39                 -0.03867              
  38.5               -0.03480              
  38                 -0.03366              
  37.5               -0.03448              
  37                 -0.03689              
  36.5               -0.03684              
  36                 -0.03394              
  35.5               -0.03544              
  35                 -0.03832              
  34.5               -0.03897              
  34.                -0.04063              
  33.5               -0.03758              
  33.                -0.03275              
  32.5               -0.03505              
  32.                -0.03910              
  31.5               -0.03868              
  31.                -0.03942              
  30.5               -0.04335              
  30.                -0.04396              
  29.5               -0.03806              
  29.                -0.03405              
  28.5               -0.03678              
  28.                -0.04049              
  27.5               -0.04635              
  27.                -0.04990              
  26.5               -0.04314              
  26.                -0.03951              
  25.5               -0.04386              
  25.                -0.04835              
  24.5               -0.04543              
  24.                -0.03726              
  23.5               -0.03517              
  23                 -0.04107              
  22.5               -0.04395              
  22                 -0.04031              
  21.5               -0.03901              
  21                 -0.04403              
  20.5               -0.04697              
  20                 -0.04688              
  19.5               -0.04610              
  19                 -0.04039              
  18.5               -0.03554              
  18                 -0.04001              
  17.5               -0.04496              
  17                 -0.04254              
  16.5               -0.04138              
  16                 -0.04274              
  15.5               -0.04227              
  15                 -0.04157              
  14.5               -0.03793              
  14                 -0.03245              
  13.5               -0.03067              
  13                 -0.02758              
  12.5               -0.01891              
  12                 -0.00781              
  11.5               -0.00126              
  11                  0.00150              
  10.5                0.00003              
  10                 -0.00879              
  9.5                -0.01758              
  9                  -0.01809              
  8.5                -0.01285              
  8                  -0.00719              
  7.5                -0.00222              
  7                   0.00286              
  6.5                 0.00435              
  6                  -0.00289              
  5.5                -0.01867              
  5                  -0.03313              
  4.5                -0.04074              
  4                  -0.04520              
  3.5                -0.04551              
  3                  -0.04275              
  2.5                -0.04204              
  2                  -0.04345              
  1.5                -0.04578              
  1                  -0.04869              
  0.5                -0.04850              
  0                  -0.05195              
 -0.5                -0.05909              
 -1                  -0.06005              
 -1.5                -0.05233              
 -2                  -0.04472              
 -2.5                -0.04260              
 -3                  -0.04259              
 -3.5                -0.04156              
 -4.                 -0.04170              
 -4.5                -0.04193              
 -5.                 -0.03695              
 -5.5                -0.02514              
 -6.                 -0.01060              
 -6.5                -0.00397              
 -7.                 -0.00464              
 -7.5                -0.00199              
 -8.                  0.00623              
 -8.5                 0.02803              
 -9.                  0.07051              
 -9.5                 0.13136              
 -10.                 0.19273              
 -10.5                0.23994              
 -11.                 0.25616              
 -11.5                0.22519              
 -12.                 0.17614              
 -12.5                0.13757              
 -13.                 0.11530              
 -13.5                0.13248              
 -14.                 0.18270              
 -14.5                0.24065              
 -15.                 0.27170              
 -15.5                0.25163              
 -16.                 0.19028              
 -16.5                0.11975              
 -17.                 0.05595              
 -17.5                0.01184              
 -18.                -0.01089              
 -18.5               -0.02404              
 -19.                -0.02462              
 -19.5               -0.02544              
 -20.                -0.02630              
 -20.5               -0.02278              
 -21.                -0.02089              
 -21.5               -0.02369              
 -22                 -0.02374              
 -22.5               -0.01844              
 -23.                -0.01317              
 -23.5               -0.01129              
 -24                 -0.00691              
 -24.5               -0.00101              
 -25.                -0.00150              
 -25.5                0.00041              
 -26                  0.00705              
 -26.5                0.01172              
 -27.                 0.01555              
 -27.5                0.01662              
 -28                  0.02460              
 -28.5                0.05136              
 -29.                 0.08080              
 -29.5                0.11775              
 -30                  0.21380              
 -30.5                0.41484              
 -31.                 0.71606              
 -31.5                1.04619              
 -32                  1.32844              
 -32.5                1.42143              
 -33.                 1.35125              
 -33.5                1.16699              
 -34                  0.94420              
 -34.5                0.78710              
 -35.                 0.79163              
 -35.5                0.93845              
 -36.                 1.14615              
 -36.5                1.25824              
 -37.                 1.18242              
 -37.5                0.93923              
 -38.                 0.62340              
 -38.5                0.35708              
 -39.                 0.19104              
 -39.5                0.08262              
 -40.                 0.04313              
 -40.5                0.02470              
 -41.                 0.01478              
 -41.5                0.00721              
 -42.                 0.00275              
 -42.5               -0.00090              
 -43.                -0.00990              
 -43.5               -0.02064              
 -44.                -0.02301              
 -44.5               -0.01688              
 -45.                -0.01530              
 -45.5               -0.02220              
 -46.                -0.02396              
 -46.5               -0.02293              
 -47.                -0.02361              
 -47.5               -0.01723              
 -48.                -0.00560              
 -48.5               -0.00063              
 -49.                -0.00139              
 -49.5               -0.00280              
 -50.                -0.00471              
 -50.5               -0.00344              
 -51.                 0.00063              
 -51.5                0.00454              
 -52.                 0.02150              
 -52.5                0.05609              
 -53.                 0.10349              
 -53.5                0.15187              
 -54.                 0.18908              
 -54.5                0.19836              
 -55.                 0.1744               
 -55.5                0.13749              
 -56.                 0.10726              
 -56.5                0.09698              
 -57.                 0.11367              
 -57.5                0.15294              
 -58.                 0.19565              
 -58.5                0.20929              
 -59.                 0.19145              
 -59.5                0.14582              
 -60.                 0.09183              
 -60.5                0.04556              
 -61.                 0.01741              
 -61.5                0.00387              
 -62.                -0.00142              
 -62.5               -0.00685              
 -63.                -0.01595              
 -63.5               -0.02206              
 -64.                -0.02474              
 -64.5               -0.02375              
 -65.                -0.02270              
 -65.5               -0.02469              
 -66.                -0.02370              
 -66.5               -0.01956              
 -67.                -0.01970              
 -67.5               -0.02529              
 -68.                -0.02824              
 -68.5               -0.02501              
 -69.                -0.02231              
 -69.5               -0.02213              
 -70.                -0.02211              
 -70.5               -0.02213              
 -71.                -0.02209              
 -71.5               -0.02234              
 -72.                -0.02503              
 -72.5               -0.03049              
 -73.                -0.03288              
 -73.5               -0.02601              
 -74.                -0.01198              
 -74.5                0.00370              
 -75.                 0.01811              
 -75.5                0.03056              
 -76.                 0.03883              
 -76.5                0.03708              
 -77.                 0.02700              
 -77.5                0.01640              
 -78.                 0.00874              
 -78.5                0.00263              
 -79.                 0.00589              
 -79.5                0.02204              
 -80.                 0.04177              
 -80.5                0.05172              
 -81.                 0.04400              
 -81.5                0.02499              
 -82.                 0.00422              
 -82.5               -0.01495              
 -83.                -0.02488              
 -83.5               -0.02696              
 -84.                -0.02905              
 -84.5               -0.02883              
 -85.                -0.02588              
 -85.5               -0.02281              
 -86.                -0.02305              
 -86.5               -0.02962              
 -87.                -0.03791              
 -87.5               -0.03700              
 -88.                -0.03124              
 -88.5               -0.03104              
 -89.                -0.02933              
 -89.5               -0.02618              
 -90.                -0.02817              
 -90.5               -0.02599              
 -91.                -0.02037              
 -91.5               -0.02200              
 -92.                -0.02632              
 -92.5               -0.02696              
 -93.                -0.02805              
 -93.5               -0.02976              
 -94.                -0.02813              
 -94.5               -0.02474              
 -95.                -0.02220              
 -95.5               -0.01978              
 -96.                -0.01639              
 -96.5               -0.01404              
 -97.                -0.01415              
 -97.5               -0.01542              
 -98.                -0.01523              
 -98.5               -0.01817              
 -99.                -0.02567              
 -99.5               -0.02828              
 -100.               -0.02211              
##END=
