##TITLE=              31P MAS NMR spectrum of calcined and rehydrated AlPO-SOD
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Roux et al. J. Phys. Chem. B, 105, 9083-9092 (2001) Figure 15c
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/22 13:33:00
##SOURCE REFERENCE=   SOD-31P-Roux-2001-rehydrated
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              SOD
##NAMES=              AlPO-SOD
##NAMES=              AlPO-20
##SAMPLE DESCRIPTION= AlPO-SOD, calcined, hydrated

$$Bibliographic information 
##$AUTHORS=           Roux, M., Marichal, C., Paillaud, J.L., Fernandez, C., Baerlocher, C., ChA~(c)zeau, J.M.
##$TITLE=             Structural investigation by multinuclear solid state NMR and X-ray diffraction of as-synthesized, dehydrated, and calcined ALPO4-SOD
##$JOURNAL=           Journal of Physical Chemistry B
##$VOLUME=            105
##$PAGES=             9083-9092
##$YEAR=              2001
##$DOI=               10.1021/jp010723k
##$FIGURE=            Figure 15c

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         6
##$PEAK LABELS=        A          B          C          D          E          F         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -33.3317   -31.1349   -29.8266   -29.2054   -29.0054   -25.4494   
##$PEAK AREAS=         1.         1.         1.         1.         1.         1.        
##$PEAK WIDTHS=        2.88079    2.88079    2.88079    2.88079    2.88079    2.88079   
##$PEAK SHAPES=        0.44261    0.44261    0.44261    0.44261    0.44261    0.44261   
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 161.9
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     3500-8000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              39.5                 
##LASTX=              -98                   
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            276
##FIRSTY=             -0.03123              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  39.5               -0.03123              
  39                 -0.03007              
  38.5               -0.02430              
  38                 -0.01978              
  37.5               -0.02553              
  37                 -0.03405              
  36.5               -0.03464              
  36                 -0.03092              
  35.5               -0.03028              
  35.                -0.02974              
  34.5               -0.02841              
  34                 -0.02956              
  33.5               -0.03467              
  33                 -0.03828              
  32.5               -0.03524              
  32                 -0.03194              
  31.5               -0.03406              
  31.                -0.03800              
  30.5               -0.03916              
  30.                -0.04009              
  29.5               -0.04230              
  29.                -0.03976              
  28.5               -0.03372              
  28.                -0.03221              
  27.5               -0.03461              
  27.                -0.03430              
  26.5               -0.03181              
  26.                -0.03238              
  25.5               -0.03438              
  25.                -0.03347              
  24.5               -0.03064              
  24                 -0.02786              
  23.5               -0.02469              
  23.                -0.02297              
  22.5               -0.02642              
  22.                -0.03076              
  21.5               -0.02740              
  21.                -0.01826              
  20.5               -0.01005              
  20.                -0.00760              
  19.5               -0.00820              
  19                 -0.00579              
  18.5               -0.00326              
  18                 -0.00130              
  17.5                0.00477              
  17.                 0.01188              
  16.5                0.01026              
  16.                 0.00226              
  15.5               -0.00615              
  15.                -0.01201              
  14.5               -0.01133              
  14.                -0.00426              
  13.5                0.00238              
  13                  0.00537              
  12.5                0.00857              
  12.                 0.01090              
  11.5                0.00570              
  11.                -0.00714              
  10.5               -0.02295              
  10                 -0.03597              
  9.5                -0.04174              
  9.                 -0.04529              
  8.5                -0.04965              
  8.                 -0.05116              
  7.5                -0.04968              
  7.                 -0.04661              
  6.5                -0.04455              
  6                  -0.04364              
  5.5                -0.04149              
  5.                 -0.03733              
  4.5                -0.03386              
  4.                 -0.03331              
  3.5                -0.03134              
  3.                 -0.02804              
  2.5                -0.02759              
  2.                 -0.02607              
  1.5                -0.02015              
  1.                 -0.01319              
  0.5                -0.00552              
  0.00000             0.00232              
 -0.5                 0.00873              
 -1.                  0.01292              
 -1.5                 0.02086              
 -2.                  0.03945              
 -2.5                 0.06318              
 -3.                  0.08712              
 -3.5                 0.11036              
 -4.                  0.12678              
 -4.5                 0.12844              
 -5.                  0.11858              
 -5.5                 0.10499              
 -6.                  0.09069              
 -6.5                 0.08092              
 -7.                  0.08703              
 -7.5                 0.11394              
 -8.                  0.15103              
 -8.5                 0.18711              
 -9.                  0.20405              
 -9.5                 0.18954              
 -10                  0.15792              
 -10.5                0.12515              
 -11                  0.08616              
 -11.5                0.04822              
 -12.                 0.02156              
 -12.5               -0.00112              
 -13                 -0.01944              
 -13.5               -0.03140              
 -14                 -0.03737              
 -14.5               -0.03801              
 -15                 -0.03840              
 -15.5               -0.04327              
 -16.                -0.04819              
 -16.5               -0.04933              
 -17.                -0.04371              
 -17.5               -0.03421              
 -18.                -0.02785              
 -18.5               -0.02800              
 -19                 -0.02853              
 -19.5               -0.02371              
 -20.                -0.01749              
 -20.5               -0.01323              
 -21.                -0.01143              
 -21.5               -0.00778              
 -22.                 0.00127              
 -22.5                0.01726              
 -23.                 0.04276              
 -23.5                0.09099              
 -24.                 0.16484              
 -24.5                0.24616              
 -25                  0.31518              
 -25.5                0.35031              
 -26.                 0.34229              
 -26.5                0.32137              
 -27                  0.28478              
 -27.5                0.34761              
 -28.                 0.55995              
 -28.5                0.75031              
 -29.                 0.88153              
 -29.5                0.92504              
 -30.                 0.87860              
 -30.5                0.79903              
 -31.                 0.71156              
 -31.5                0.61575              
 -32.                 0.52381              
 -32.5                0.44239              
 -33.                 0.37669              
 -33.5                0.31821              
 -34.                 0.25837              
 -34.5                0.21120              
 -35                  0.17554              
 -35.5                0.14065              
 -36.                 0.11387              
 -36.5                0.08864              
 -37.                 0.06105              
 -37.5                0.04212              
 -38.                 0.03082              
 -38.5                0.02235              
 -39.                 0.01564              
 -39.5                0.00726              
 -40.                -0.00300              
 -40.5               -0.01163              
 -41                 -0.01725              
 -41.5               -0.02198              
 -42.                -0.02572              
 -42.5               -0.02763              
 -43.                -0.03151              
 -43.5               -0.03981              
 -44                 -0.04606              
 -44.5               -0.04391              
 -45.                -0.04031              
 -45.5               -0.03966              
 -46.                -0.02667              
 -46.5               -0.00448              
 -47                  0.01912              
 -47.5                0.04162              
 -48.                 0.05184              
 -48.5                0.04838              
 -49.                 0.04058              
 -49.5                0.03170              
 -50.                 0.02784              
 -50.5                0.03679              
 -51.                 0.06011              
 -51.5                0.10379              
 -52.                 0.15353              
 -52.5                0.19578              
 -53.                 0.21907              
 -53.5                0.21433              
 -54.                 0.19711              
 -54.5                0.17524              
 -55.                 0.15414              
 -55.5                0.13259              
 -56.                 0.10873              
 -56.5                0.09023              
 -57.                 0.07526              
 -57.5                0.05884              
 -58.                 0.04479              
 -58.5                0.03714              
 -59.                 0.03370              
 -59.5                0.02773              
 -60.                 0.01946              
 -60.5                0.01184              
 -61.                 0.00414              
 -61.5               -0.00150              
 -62.                -0.00375              
 -62.5               -0.00778              
 -63.                -0.01353              
 -63.5               -0.01710              
 -64                 -0.01915              
 -64.5               -0.02281              
 -65.                -0.02943              
 -65.5               -0.03583              
 -66.                -0.03923              
 -66.5               -0.03812              
 -67.                -0.03551              
 -67.5               -0.03597              
 -68.                -0.03741              
 -68.5               -0.03453              
 -69.                -0.02741              
 -69.5               -0.01942              
 -70.                -0.01532              
 -70.5               -0.01627              
 -71.                -0.01962              
 -71.5               -0.02233              
 -72                 -0.02264              
 -72.5               -0.02091              
 -73                 -0.01726              
 -73.5               -0.00874              
 -74.                 0.00378              
 -74.5                0.01662              
 -75.                 0.02733              
 -75.5                0.03380              
 -76.                 0.03489              
 -76.5                0.03181              
 -77.                 0.02591              
 -77.5                0.02015              
 -78.                 0.01671              
 -78.5                0.01165              
 -79.                 0.00384              
 -79.5               -0.00324              
 -80.                -0.00665              
 -80.5               -0.00360              
 -81                  0.00200              
 -81.5                0.00302              
 -82.                -0.00125              
 -82.5               -0.00837              
 -83.                -0.01184              
 -83.5               -0.01403              
 -84                 -0.01778              
 -84.5               -0.02012              
 -85                 -0.02492              
 -85.5               -0.03364              
 -86.                -0.03836              
 -86.5               -0.03696              
 -87.                -0.03576              
 -87.5               -0.03814              
 -88.                -0.04076              
 -88.5               -0.04075              
 -89.                -0.04085              
 -89.5               -0.03985              
 -90                 -0.03780              
 -90.5               -0.03990              
 -91.                -0.04452              
 -91.5               -0.04623              
 -92.                -0.04362              
 -92.5               -0.03999              
 -93                 -0.03943              
 -93.5               -0.04171              
 -94.                -0.04329              
 -94.5               -0.04434              
 -95.                -0.04479              
 -95.5               -0.04231              
 -96.                -0.03845              
 -96.5               -0.03517              
 -97                 -0.03155              
 -97.5               -0.03130              
 -98                 -0.03253              
##END=
