##TITLE=              31P MAS NMR spectrum of as-made AlPO-11 (with dipropylamine template)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Barrie et al. Chem. Phys. Lett., 180, 6-12 (1991) Figure 3a
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/13 11:46:50
##SOURCE REFERENCE=   AEL-31P-Barrie-1991-asmade
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              AEL
##NAMES=              AlPO-11
##SAMPLE DESCRIPTION= AlPO-11, as-made

$$Bibliographic information 
##$AUTHORS=           Barrie, P.J., Smith, M.E., Klinowski, J.
##$TITLE=             Double-rotation 27Al NMR studies of the aluminophosphate molecular sieve AlPO4-11
##$JOURNAL=           Chemical Physics Letters
##$VOLUME=            180
##$PAGES=             6-12
##$YEAR=              1991
##$DOI=               10.1016/0009-2614(91)87107-M
##$FIGURE=            Figure 3a

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         3
##$PEAK LABELS=        P2/P1      P3         P1/P2     
##$PEAK TSITES=        T2/T1      T3         T1/T2
##$PEAK POSITIONS=    -32.3568   -31.9568   -26.7128   
##$PEAK AREAS=         2.         1.         2.        
##$PEAK WIDTHS=        5.80128    5.80128    5.80128   
##$PEAK SHAPES=        0.49019    0.49019    0.49019   
##$NUMBERING REF=     Pluth et al. J. Phys. Chem., 92, 2734-2738 (1988)
##$ASSIGN REF=        Barrie et al. Chem. Phys. Lett., 180, 6-12 (1991) Figure 3a
##$ASSIGN METHOD=     relative intensities
##$COMMENT=           Partial peak assignments based on relative peak areas

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 160.0
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     12000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              10.                  
##LASTX=              -54.6                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            324
##FIRSTY=             -0.00349              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  10.                -0.00349              
  9.8                -0.00348              
  9.6                -0.00351              
  9.4                -0.00379              
  9.2                -0.00398              
  9.                 -0.00362              
  8.8                -0.00348              
  8.6                -0.00348              
  8.4                -0.00330              
  8.2                -0.00309              
  8.                 -0.00299              
  7.8                -0.00300              
  7.6                -0.00300              
  7.4                -0.00300              
  7.2                -0.00300              
  7.                 -0.00300              
  6.8                -0.00300              
  6.6                -0.00300              
  6.4                -0.00299              
  6.2                -0.00301              
  6.                 -0.00319              
  5.8                -0.00339              
  5.6                -0.00351              
  5.4                -0.00346              
  5.2                -0.00321              
  5.                 -0.00297              
  4.8                -0.00301              
  4.6                -0.00300              
  4.4                -0.00300              
  4.2                -0.00300              
  4.                 -0.00260              
  3.8                -0.00184              
  3.6                -0.00124              
  3.4                -0.00096              
  3.2                -0.00082              
  3.                 -0.00060              
  2.8                -0.00052              
  2.6                -0.00053              
  2.4                -0.00051              
  2.2                -0.00021              
  2.                  0.00020              
  1.8                 0.00035              
  1.6                 0.00016              
  1.4                -0.00003              
  1.2                 0.00028              
  1.                  0.00018              
  0.8                -0.00007              
  0.6                -0.00000              
  0.4                 0.00023              
  0.2                 0.00048              
  0.00000             0.00042              
 -0.2                 0.00054              
 -0.4                 0.00084              
 -0.6                 0.00095              
 -0.8                 0.00094              
 -1.                  0.00094              
 -1.2                 0.00094              
 -1.4                 0.00094              
 -1.6                 0.00094              
 -1.8                 0.00094              
 -2.                  0.00094              
 -2.2                 0.00094              
 -2.4                 0.00094              
 -2.6                 0.00094              
 -2.8                 0.00095              
 -3.                  0.00090              
 -3.2                 0.00110              
 -3.4                 0.00178              
 -3.6                 0.00246              
 -3.8                 0.00296              
 -4.                  0.00385              
 -4.2                 0.00529              
 -4.4                 0.00646              
 -4.6                 0.00766              
 -4.8                 0.00921              
 -5.                  0.01139              
 -5.2                 0.01350              
 -5.4                 0.01457              
 -5.6                 0.01480              
 -5.8                 0.01378              
 -6.                  0.01213              
 -6.2                 0.01064              
 -6.4                 0.00960              
 -6.6                 0.00861              
 -6.8                 0.00745              
 -7.                  0.00675              
 -7.2                 0.00653              
 -7.4                 0.00633              
 -7.6                 0.00607              
 -7.8                 0.00504              
 -8.                  0.00446              
 -8.2                 0.00435              
 -8.4                 0.00406              
 -8.6                 0.00378              
 -8.8                 0.00353              
 -9.                  0.00359              
 -9.2                 0.00378              
 -9.4                 0.00398              
 -9.6                 0.00461              
 -9.8                 0.00489              
 -10.                 0.00497              
 -10.2                0.00577              
 -10.4                0.00635              
 -10.6                0.00658              
 -10.8                0.00679              
 -11.                 0.00686              
 -11.2                0.00687              
 -11.4                0.00710              
 -11.6                0.00787              
 -11.8                0.00862              
 -12.                 0.00875              
 -12.2                0.00884              
 -12.4                0.00885              
 -12.6                0.00902              
 -12.8                0.00923              
 -13.                 0.00934              
 -13.2                0.00931              
 -13.4                0.00941              
 -13.6                0.00976              
 -13.8                0.01018              
 -14.                 0.01072              
 -14.2                0.01151              
 -14.4                0.01246              
 -14.6                0.01353              
 -14.8                0.01474              
 -15.                 0.01619              
 -15.2                0.01708              
 -15.4                0.01727              
 -15.6                0.01757              
 -15.8                0.01812              
 -16.                 0.01891              
 -16.2                0.02011              
 -16.4                0.02186              
 -16.6                0.02348              
 -16.8                0.02487              
 -17.                 0.02648              
 -17.2                0.02770              
 -17.4                0.02897              
 -17.6                0.03086              
 -17.8                0.03299              
 -18.                 0.03452              
 -18.2                0.03581              
 -18.4                0.03708              
 -18.6                0.03810              
 -18.8                0.03927              
 -19.                 0.04049              
 -19.2                0.04128              
 -19.4                0.04266              
 -19.6                0.04418              
 -19.8                0.04543              
 -20.                 0.04791              
 -20.2                0.05074              
 -20.4                0.05285              
 -20.6                0.05558              
 -20.8                0.05870              
 -21.                 0.06109              
 -21.2                0.06396              
 -21.4                0.06746              
 -21.6                0.07152              
 -21.8                0.07610              
 -22.                 0.08181              
 -22.2                0.08950              
 -22.4                0.09819              
 -22.6                0.10667              
 -22.8                0.11207              
 -23.                 0.11932              
 -23.2                0.12884              
 -23.4                0.13837              
 -23.6                0.15226              
 -23.8                0.16822              
 -24.                 0.17974              
 -24.2                0.19119              
 -24.4                0.20143              
 -24.6                0.20795              
 -24.8                0.21553              
 -25.                 0.22532              
 -25.2                0.23625              
 -25.4                0.24711              
 -25.6                0.25688              
 -25.8                0.26476              
 -26.                 0.27348              
 -26.2                0.28155              
 -26.4                0.28652              
 -26.6                0.29390              
 -26.8                0.30293              
 -27.                 0.30945              
 -27.2                0.31539              
 -27.4                0.32173              
 -27.6                0.32765              
 -27.8                0.33341              
 -28.                 0.33962              
 -28.2                0.34373              
 -28.4                0.34725              
 -28.6                0.35116              
 -28.8                0.35482              
 -29.                 0.35891              
 -29.2                0.36342              
 -29.4                0.36917              
 -29.6                0.37610              
 -29.8                0.38298              
 -30.                 0.38982              
 -30.2                0.39669              
 -30.4                0.40404              
 -30.6                0.41325              
 -30.8                0.42416              
 -31.                 0.43577              
 -31.2                0.44504              
 -31.4                0.45233              
 -31.6                0.45677              
 -31.8                0.45843              
 -32.                 0.45933              
 -32.2                0.45836              
 -32.4                0.45334              
 -32.6                0.44503              
 -32.8                0.43443              
 -33.                 0.42193              
 -33.2                0.40605              
 -33.4                0.38764              
 -33.6                0.37040              
 -33.8                0.35089              
 -34.                 0.32727              
 -34.2                0.30422              
 -34.4                0.28277              
 -34.6                0.26005              
 -34.8                0.23989              
 -35.                 0.21780              
 -35.2                0.19302              
 -35.4                0.16922              
 -35.6                0.15236              
 -35.8                0.14450              
 -36.                 0.13436              
 -36.2                0.12282              
 -36.4                0.11141              
 -36.6                0.09973              
 -36.8                0.08742              
 -37.                 0.07635              
 -37.2                0.06854              
 -37.4                0.06220              
 -37.6                0.05742              
 -37.8                0.05165              
 -38.                 0.04622              
 -38.2                0.04154              
 -38.4                0.03676              
 -38.6                0.03278              
 -38.8                0.02964              
 -39.                 0.02693              
 -39.2                0.02498              
 -39.4                0.02366              
 -39.6                0.02231              
 -39.8                0.02078              
 -40.                 0.01961              
 -40.2                0.01884              
 -40.4                0.01809              
 -40.6                0.01735              
 -40.8                0.01672              
 -41.                 0.01605              
 -41.2                0.01499              
 -41.4                0.01421              
 -41.6                0.01376              
 -41.8                0.01336              
 -42                  0.01330              
 -42.2                0.01315              
 -42.4                0.01265              
 -42.6                0.01212              
 -42.8                0.01161              
 -43.                 0.01122              
 -43.2                0.01099              
 -43.4                0.01065              
 -43.6                0.01020              
 -43.8                0.00989              
 -44.                 0.00973              
 -44.2                0.00939              
 -44.4                0.00896              
 -44.6                0.00882              
 -44.8                0.00882              
 -45.                 0.00864              
 -45.2                0.00845              
 -45.4                0.00829              
 -45.6                0.00801              
 -45.8                0.00773              
 -46.                 0.00745              
 -46.2                0.00736              
 -46.4                0.00726              
 -46.6                0.00696              
 -46.8                0.00685              
 -47.                 0.00686              
 -47.2                0.00686              
 -47.4                0.00686              
 -47.6                0.00686              
 -47.8                0.00686              
 -48.                 0.00686              
 -48.2                0.00686              
 -48.4                0.00685              
 -48.6                0.00664              
 -48.8                0.00617              
 -49.                 0.00584              
 -49.2                0.00588              
 -49.4                0.00589              
 -49.6                0.00582              
 -49.8                0.00530              
 -50.                 0.00467              
 -50.2                0.00436              
 -50.4                0.00442              
 -50.6                0.00431              
 -50.8                0.00396              
 -51.                 0.00357              
 -51.2                0.00326              
 -51.4                0.00280              
 -51.6                0.00248              
 -51.8                0.00241              
 -52.                 0.00242              
 -52.2                0.00242              
 -52.4                0.00242              
 -52.6                0.00241              
 -52.8                0.00219              
 -53.                 0.00178              
 -53.2                0.00157              
 -53.4                0.00152              
 -53.6                0.00142              
 -53.8                0.00144              
 -54.                 0.00143              
 -54.2                0.00145              
 -54.4                0.00140              
 -54.6                0.00105              
##END=
