##TITLE=              29Si MAS NMR spectrum of as-made pure silica Ferrierite (with pyridine)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Lewis et al. J. Phys. Chem., 100, 5039-5049 (1996) Figure 7
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/06/20 12:20:03
##SOURCE REFERENCE=   FER-29Si-Lewis-1996-asmade
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              FER
##NAMES=              Ferrierite
##SAMPLE DESCRIPTION= Ferrierite, pure silica, as-made

$$Bibliographic information 
##$AUTHORS=           Lewis, J.E., Freyhardt, C.C., Davis, M.E.
##$TITLE=             Location of pyridine guest molecules in an electroneutral ((3)Infinity)[SiO4/2] Host framework - single-crystal structures of the as-synthesized and calcined forms of high-silica ferrierite
##$JOURNAL=           Journal of Physical Chemistry
##$VOLUME=            100
##$PAGES=             5039-5049
##$YEAR=              1996
##$DOI=               10.1021/jp9530055
##$FIGURE=            Figure 7

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         5
##$PEAK TSITES=        T4         T2         T1         T1         T3        
##$PEAK LABELS=        Si1        Si5        Si4        Si3        Si2       
##$PEAK POSITIONS=    -118.707   -118.189   -116.492   -114.243   -113.093   
##$PEAK AREAS=         1.         2.         2.         2.         2.        
##$PEAK WIDTHS=        0.74035    0.74962    1.12758    1.42033    0.63676   
##$PEAK SHAPES=        1          1          1          1          1         
##$NUMBERING REF=     Lewis et al. J. Phys. Chem., 100, 5039-5049 (1996)
##$ASSIGN REF=        Lewis et al. J. Phys. Chem., 100, 5039-5049 (1996); Brouwer et al. J. Am. Chem. Soc. 127, 10366 (2005)
##$ASSIGN METHOD=     Relative intensities and bond angles; 2D correlation NMR

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 59.63
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     3500

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -107.98               
##LASTX=              -123.31               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            1534
##FIRSTY=              0.02876              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -107.98              0.02876              
 -107.99              0.03015              
 -108.                0.03060              
 -108.01              0.03042              
 -108.02              0.03058              
 -108.03              0.03033              
 -108.04              0.02903              
 -108.05              0.02787              
 -108.06              0.02779              
 -108.07              0.02882              
 -108.08              0.03018              
 -108.09              0.03065              
 -108.1               0.03043              
 -108.11              0.03037              
 -108.12              0.03043              
 -108.13              0.03043              
 -108.14              0.03042              
 -108.15              0.03042              
 -108.16              0.03041              
 -108.17              0.03041              
 -108.18              0.03049              
 -108.19              0.03042              
 -108.2               0.03013              
 -108.21              0.03064              
 -108.22              0.03218              
 -108.23              0.03261              
 -108.24              0.03224              
 -108.25              0.03461              
 -108.26              0.03888              
 -108.27              0.04126              
 -108.28              0.04180              
 -108.29              0.04188              
 -108.3               0.04174              
 -108.31              0.04160              
 -108.32              0.04217              
 -108.33              0.04353              
 -108.34              0.04500              
 -108.35              0.04620              
 -108.36              0.04714              
 -108.37              0.04877              
 -108.38              0.05160              
 -108.39              0.05341              
 -108.4               0.05325              
 -108.41              0.05346              
 -108.42              0.05490              
 -108.43              0.05656              
 -108.44              0.05766              
 -108.45              0.05783              
 -108.46              0.05772              
 -108.47              0.05787              
 -108.48              0.05747              
 -108.49              0.05616              
 -108.5               0.05474              
 -108.51              0.05351              
 -108.52              0.05222              
 -108.53              0.05096              
 -108.54              0.04989              
 -108.55              0.04833              
 -108.56              0.04586              
 -108.57              0.04314              
 -108.58              0.04061              
 -108.59              0.03812              
 -108.6               0.03557              
 -108.61              0.03302              
 -108.62              0.03049              
 -108.63              0.02795              
 -108.64              0.02541              
 -108.65              0.02287              
 -108.66              0.02033              
 -108.67              0.01779              
 -108.68              0.01526              
 -108.69              0.01272              
 -108.7               0.01017              
 -108.71              0.00764              
 -108.72              0.00517              
 -108.73              0.00251              
 -108.74             -0.00021              
 -108.75             -0.00202              
 -108.76             -0.00312              
 -108.77             -0.00516              
 -108.78             -0.00786              
 -108.79             -0.00974              
 -108.8              -0.01053              
 -108.81             -0.01056              
 -108.82             -0.01054              
 -108.83             -0.01066              
 -108.84             -0.01013              
 -108.85             -0.00876              
 -108.86             -0.00718              
 -108.87             -0.00604              
 -108.88             -0.00552              
 -108.89             -0.00334              
 -108.9               0.00191              
 -108.91              0.00640              
 -108.92              0.00855              
 -108.93              0.01220              
 -108.94              0.01767              
 -108.95              0.02170              
 -108.96              0.02548              
 -108.97              0.03173              
 -108.98              0.03789              
 -108.99              0.04161              
 -109.                0.04568              
 -109.01              0.05109              
 -109.02              0.05489              
 -109.03              0.05709              
 -109.04              0.06026              
 -109.05              0.06438              
 -109.06              0.06828              
 -109.07              0.07199              
 -109.08              0.07577              
 -109.09              0.07966              
 -109.1               0.08351              
 -109.11              0.08694              
 -109.12              0.08929              
 -109.13              0.08988              
 -109.14              0.08956              
 -109.15              0.08951              
 -109.16              0.08955              
 -109.17              0.08947              
 -109.18              0.08973              
 -109.19              0.08987              
 -109.2               0.08837              
 -109.21              0.08551              
 -109.22              0.08274              
 -109.23              0.08037              
 -109.24              0.07809              
 -109.25              0.07504              
 -109.26              0.07110              
 -109.27              0.06770              
 -109.28              0.06528              
 -109.29              0.06301              
 -109.3               0.06037              
 -109.31              0.05737              
 -109.32              0.05536              
 -109.33              0.05532              
 -109.34              0.05530              
 -109.35              0.05403              
 -109.36              0.05236              
 -109.37              0.05111              
 -109.38              0.05072              
 -109.39              0.05088              
 -109.4               0.05093              
 -109.41              0.05089              
 -109.42              0.05088              
 -109.43              0.05089              
 -109.44              0.05089              
 -109.45              0.05089              
 -109.46              0.05089              
 -109.47              0.05089              
 -109.48              0.05089              
 -109.49              0.05089              
 -109.5               0.05089              
 -109.51              0.05089              
 -109.52              0.05089              
 -109.53              0.05089              
 -109.54              0.05090              
 -109.55              0.05090              
 -109.56              0.05084              
 -109.57              0.05089              
 -109.58              0.05113              
 -109.59              0.05071              
 -109.6               0.04931              
 -109.61              0.04841              
 -109.62              0.04851              
 -109.63              0.04868              
 -109.64              0.04863              
 -109.65              0.04860              
 -109.66              0.04862              
 -109.67              0.04862              
 -109.68              0.04862              
 -109.69              0.04861              
 -109.7               0.04862              
 -109.71              0.04862              
 -109.72              0.04860              
 -109.73              0.04861              
 -109.74              0.04868              
 -109.75              0.04860              
 -109.76              0.04838              
 -109.77              0.04888              
 -109.78              0.05029              
 -109.79              0.05116              
 -109.8               0.05102              
 -109.81              0.05063              
 -109.82              0.05081              
 -109.83              0.05208              
 -109.84              0.05323              
 -109.85              0.05321              
 -109.86              0.05330              
 -109.87              0.05451              
 -109.88              0.05665              
 -109.89              0.05927              
 -109.9               0.06181              
 -109.91              0.06436              
 -109.92              0.06715              
 -109.93              0.06931              
 -109.94              0.07043              
 -109.95              0.07213              
 -109.96              0.07484              
 -109.97              0.07687              
 -109.98              0.07795              
 -109.99              0.07910              
 -110.                0.08043              
 -110.01              0.08166              
 -110.02              0.08300              
 -110.03              0.08442              
 -110.04              0.08518              
 -110.05              0.08510              
 -110.06              0.08493              
 -110.07              0.08498              
 -110.08              0.08513              
 -110.09              0.08500              
 -110.1               0.08413              
 -110.11              0.08221              
 -110.12              0.07954              
 -110.13              0.07744              
 -110.14              0.07628              
 -110.15              0.07517              
 -110.16              0.07384              
 -110.17              0.07255              
 -110.18              0.07130              
 -110.19              0.07004              
 -110.2               0.06875              
 -110.21              0.06747              
 -110.22              0.06626              
 -110.23              0.06502              
 -110.24              0.06344              
 -110.25              0.06230              
 -110.26              0.06251              
 -110.27              0.06213              
 -110.28              0.05956              
 -110.29              0.05721              
 -110.3               0.05617              
 -110.31              0.05420              
 -110.32              0.05143              
 -110.33              0.05043              
 -110.34              0.05086              
 -110.35              0.05100              
 -110.36              0.05088              
 -110.37              0.05087              
 -110.38              0.05089              
 -110.39              0.05088              
 -110.4               0.05092              
 -110.41              0.05093              
 -110.42              0.05072              
 -110.43              0.05087              
 -110.44              0.05201              
 -110.45              0.05336              
 -110.46              0.05442              
 -110.47              0.05633              
 -110.48              0.05907              
 -110.49              0.06081              
 -110.5               0.06191              
 -110.51              0.06423              
 -110.52              0.06681              
 -110.53              0.06812              
 -110.54              0.06947              
 -110.55              0.07198              
 -110.56              0.07475              
 -110.57              0.07726              
 -110.58              0.07975              
 -110.59              0.08230              
 -110.6               0.08483              
 -110.61              0.08738              
 -110.62              0.08998              
 -110.63              0.09240              
 -110.64              0.09476              
 -110.65              0.09803              
 -110.66              0.10200              
 -110.67              0.10513              
 -110.68              0.10745              
 -110.69              0.10991              
 -110.7               0.11250              
 -110.71              0.11500              
 -110.72              0.11763              
 -110.73              0.12029              
 -110.74              0.12222              
 -110.75              0.12337              
 -110.76              0.12446              
 -110.77              0.12581              
 -110.78              0.12736              
 -110.79              0.12826              
 -110.8               0.12814              
 -110.81              0.1285               
 -110.82              0.12989              
 -110.83              0.13091              
 -110.84              0.13074              
 -110.85              0.12947              
 -110.86              0.12826              
 -110.87              0.12827              
 -110.88              0.12810              
 -110.89              0.12670              
 -110.9               0.12581              
 -110.91              0.12599              
 -110.92              0.12551              
 -110.93              0.12404              
 -110.94              0.12247              
 -110.95              0.12141              
 -110.96              0.12119              
 -110.97              0.12148              
 -110.98              0.12168              
 -110.99              0.12095              
 -111.                0.11952              
 -111.01              0.11893              
 -111.02              0.11912              
 -111.03              0.11897              
 -111.04              0.11915              
 -111.05              0.12048              
 -111.06              0.12152              
 -111.07              0.12144              
 -111.08              0.12160              
 -111.09              0.12293              
 -111.1               0.12538              
 -111.11              0.12795              
 -111.12              0.12935              
 -111.13              0.13061              
 -111.14              0.13302              
 -111.15              0.13577              
 -111.16              0.13825              
 -111.17              0.14093              
 -111.18              0.14353              
 -111.19              0.14506              
 -111.2               0.14624              
 -111.21              0.14852              
 -111.22              0.15123              
 -111.23              0.1536               
 -111.24              0.15659              
 -111.25              0.16052              
 -111.26              0.16405              
 -111.27              0.16644              
 -111.28              0.16776              
 -111.29              0.16905              
 -111.3               0.17144              
 -111.31              0.17404              
 -111.32              0.17565              
 -111.33              0.17595              
 -111.34              0.17571              
 -111.35              0.17691              
 -111.36              0.17833              
 -111.37              0.17659              
 -111.38              0.17376              
 -111.39              0.1734               
 -111.4               0.17367              
 -111.41              0.17252              
 -111.42              0.17076              
 -111.43              0.16943              
 -111.44              0.16913              
 -111.45              0.16924              
 -111.46              0.16837              
 -111.47              0.16687              
 -111.48              0.16561              
 -111.49              0.16430              
 -111.5               0.16287              
 -111.51              0.16220              
 -111.52              0.16232              
 -111.53              0.16223              
 -111.54              0.16225              
 -111.55              0.16337              
 -111.56              0.16466              
 -111.57              0.16489              
 -111.58              0.16450              
 -111.59              0.16433              
 -111.6               0.16518              
 -111.61              0.16661              
 -111.62              0.16697              
 -111.63              0.16685              
 -111.64              0.16783              
 -111.65              0.16928              
 -111.66              0.17036              
 -111.67              0.17211              
 -111.68              0.17481              
 -111.69              0.17684              
 -111.7               0.17794              
 -111.71              0.17926              
 -111.72              0.18048              
 -111.73              0.18073              
 -111.74              0.18052              
 -111.75              0.18050              
 -111.76              0.18054              
 -111.77              0.18053              
 -111.78              0.18058              
 -111.79              0.18058              
 -111.8               0.18034              
 -111.81              0.18051              
 -111.82              0.18177              
 -111.83              0.18293              
 -111.84              0.18299              
 -111.85              0.18275              
 -111.86              0.18277              
 -111.87              0.18288              
 -111.88              0.18286              
 -111.89              0.18259              
 -111.9               0.18281              
 -111.91              0.18416              
 -111.92              0.18518              
 -111.93              0.18506              
 -111.94              0.18538              
 -111.95              0.18676              
 -111.96              0.18826              
 -111.97              0.18946              
 -111.98              0.19048              
 -111.99              0.19199              
 -112.                0.1945               
 -112.01              0.19702              
 -112.02              0.19928              
 -112.03              0.20295              
 -112.04              0.20824              
 -112.05              0.21359              
 -112.06              0.21857              
 -112.07              0.22353              
 -112.08              0.22872              
 -112.09              0.23403              
 -112.1               0.23856              
 -112.11              0.24222              
 -112.12              0.24651              
 -112.13              0.25174              
 -112.14              0.25690              
 -112.15              0.26195              
 -112.16              0.26725              
 -112.17              0.27201              
 -112.18              0.27572              
 -112.19              0.27982              
 -112.2               0.28497              
 -112.21              0.29013              
 -112.22              0.29516              
 -112.23              0.30066              
 -112.24              0.30545              
 -112.25              0.30809              
 -112.26              0.31072              
 -112.27              0.31546              
 -112.28              0.32162              
 -112.29              0.32808              
 -112.3               0.33376              
 -112.31              0.33868              
 -112.32              0.34365              
 -112.33              0.34879              
 -112.34              0.35391              
 -112.35              0.35891              
 -112.36              0.36388              
 -112.37              0.36934              
 -112.38              0.37569              
 -112.39              0.38298              
 -112.4               0.39070              
 -112.41              0.39806              
 -112.42              0.40594              
 -112.43              0.41552              
 -112.44              0.42661              
 -112.45              0.43829              
 -112.46              0.44878              
 -112.47              0.45864              
 -112.48              0.471                
 -112.49              0.48551              
 -112.5               0.49977              
 -112.51              0.51350              
 -112.52              0.52776              
 -112.53              0.54509              
 -112.54              0.56575              
 -112.55              0.5853               
 -112.56              0.60269              
 -112.57              0.62076              
 -112.58              0.64019              
 -112.59              0.66032              
 -112.6               0.68079              
 -112.61              0.70181              
 -112.62              0.72477              
 -112.63              0.75015              
 -112.64              0.77660              
 -112.65              0.80328              
 -112.66              0.83016              
 -112.67              0.85865              
 -112.68              0.89044              
 -112.69              0.92475              
 -112.7               0.96079              
 -112.71              0.99981              
 -112.72              1.04184              
 -112.73              1.08476              
 -112.74              1.12936              
 -112.75              1.1784               
 -112.76              1.23002              
 -112.77              1.2809               
 -112.78              1.33162              
 -112.79              1.38273              
 -112.8               1.43231              
 -112.81              1.4782               
 -112.82              1.51892              
 -112.83              1.55932              
 -112.84              1.60754              
 -112.85              1.65963              
 -112.86              1.70813              
 -112.87              1.75269              
 -112.88              1.79402              
 -112.89              1.83142              
 -112.9               1.8654               
 -112.91              1.89797              
 -112.92              1.92945              
 -112.93              1.95914              
 -112.94              1.98801              
 -112.95              2.0163               
 -112.96              2.03955              
 -112.97              2.05759              
 -112.98              2.07987              
 -112.99              2.10632              
 -113.                2.12624              
 -113.01              2.1397               
 -113.02              2.15273              
 -113.03              2.16493              
 -113.04              2.17494              
 -113.05              2.18553              
 -113.06              2.19659              
 -113.07              2.20205              
 -113.08              2.2011               
 -113.09              2.1982               
 -113.1               2.19394              
 -113.11              2.18704              
 -113.12              2.17878              
 -113.13              2.17032              
 -113.14              2.16024              
 -113.15              2.14762              
 -113.16              2.13305              
 -113.17              2.11765              
 -113.18              2.10265              
 -113.19              2.08723              
 -113.2               2.07002              
 -113.21              2.05161              
 -113.22              2.03275              
 -113.23              2.01315              
 -113.24              1.9928               
 -113.25              1.97217              
 -113.26              1.95042              
 -113.27              1.92598              
 -113.28              1.90009              
 -113.29              1.8747               
 -113.3               1.84925              
 -113.31              1.82284              
 -113.32              1.7952               
 -113.33              1.76711              
 -113.34              1.74028              
 -113.35              1.71371              
 -113.36              1.68496              
 -113.37              1.6556               
 -113.38              1.62776              
 -113.39              1.59954              
 -113.4               1.57005              
 -113.41              1.5419               
 -113.42              1.51553              
 -113.43              1.48871              
 -113.44              1.46213              
 -113.45              1.43806              
 -113.46              1.41624              
 -113.47              1.39566              
 -113.48              1.37593              
 -113.49              1.35602              
 -113.5               1.33363              
 -113.51              1.30913              
 -113.52              1.28554              
 -113.53              1.263                
 -113.54              1.24023              
 -113.55              1.21735              
 -113.56              1.19518              
 -113.57              1.17516              
 -113.58              1.15749              
 -113.59              1.14033              
 -113.6               1.12384              
 -113.61              1.10988              
 -113.62              1.0978               
 -113.63              1.086                
 -113.64              1.07513              
 -113.65              1.06596              
 -113.66              1.05798              
 -113.67              1.05043              
 -113.68              1.04262              
 -113.69              1.035                
 -113.7               1.0289               
 -113.71              1.02444              
 -113.72              1.02129              
 -113.73              1.01966              
 -113.74              1.01953              
 -113.75              1.02011              
 -113.76              1.0213               
 -113.77              1.02394              
 -113.78              1.02808              
 -113.79              1.03304              
 -113.8               1.03817              
 -113.81              1.04308              
 -113.82              1.0485               
 -113.83              1.05484              
 -113.84              1.06136              
 -113.85              1.06767              
 -113.86              1.07399              
 -113.87              1.08035              
 -113.88              1.08666              
 -113.89              1.09305              
 -113.9               1.09952              
 -113.91              1.10557              
 -113.92              1.11076              
 -113.93              1.11506              
 -113.94              1.11878              
 -113.95              1.12251              
 -113.96              1.12635              
 -113.97              1.13012              
 -113.98              1.13398              
 -113.99              1.13797              
 -114.                1.14132              
 -114.01              1.14379              
 -114.02              1.14628              
 -114.03              1.14887              
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##END=
