Camblor et al. Angew. Chem. Int. Ed., 36, 2659-2661 (1997) Figure 1 ##freq 1 ##col_ ppm Spectrum Model A B C D ----- -98.96 0.00873 0.00073 0.00013 0.00014 0.00014 0.00032 -98.975 0.00815 0.00074 0.00013 0.00014 0.00014 0.00032 -98.99 0.01114 0.00074 0.00013 0.00014 0.00014 0.00032 -99.005 0.01522 0.00074 0.00013 0.00014 0.00014 0.00032 -99.02 0.01555 0.00074 0.00013 0.00014 0.00014 0.00032 -99.035 0.01371 0.00074 0.00013 0.00014 0.00014 0.00032 -99.05 0.01342 0.00074 0.00013 0.00014 0.00014 0.00032 -99.065 0.01041 0.00075 0.00013 0.00014 0.00014 0.00032 -99.08 0.00240 0.00075 0.00013 0.00014 0.00014 0.00032 -99.095 -0.00310 0.00075 0.00013 0.00014 0.00014 0.00032 -99.11 -0.00256 0.00075 0.00013 0.00014 0.00014 0.00033 -99.125 0.00128 0.00075 0.00013 0.00014 0.00014 0.00033 -99.14 0.00665 0.00076 0.00013 0.00014 0.00014 0.00033 -99.155 0.01266 0.00076 0.00013 0.00014 0.00014 0.00033 -99.17 0.01902 0.00076 0.00013 0.00014 0.00014 0.00033 -99.185 0.02417 0.00076 0.00013 0.00014 0.00014 0.00033 -99.2 0.02299 0.00076 0.00014 0.00014 0.00014 0.00033 -99.215 0.01522 0.00077 0.00014 0.00014 0.00014 0.00033 -99.23 0.00727 0.00077 0.00014 0.00014 0.00014 0.00033 -99.245 0.00161 0.00077 0.00014 0.00014 0.00014 0.00033 -99.26 -0.00194 0.00077 0.00014 0.00014 0.00014 0.00034 -99.275 -0.00109 0.00077 0.00014 0.00014 0.00014 0.00034 -99.29 0.00452 0.00077 0.00014 0.00014 0.00014 0.00034 -99.305 0.00737 0.00078 0.00014 0.00014 0.00014 0.00034 -99.32 0.00640 0.00078 0.00014 0.00014 0.00014 0.00034 -99.335 0.01094 0.00078 0.00014 0.00014 0.00014 0.00034 -99.35 0.01925 0.00078 0.00014 0.00014 0.00014 0.00034 -99.365 0.02233 0.00078 0.00014 0.00014 0.00014 0.00034 -99.38 0.02241 0.00079 0.00014 0.00014 0.00014 0.00034 -99.395 0.02392 0.00079 0.00014 0.00014 0.00014 0.00035 -99.41 0.02432 0.00079 0.00014 0.00014 0.00015 0.00035 -99.425 0.02272 0.00079 0.00014 0.00015 0.00015 0.00035 -99.44 0.02273 0.00079 0.00014 0.00015 0.00015 0.00035 -99.455 0.02432 0.00080 0.00014 0.00015 0.00015 0.00035 -99.47 0.02466 0.00080 0.00014 0.00015 0.00015 0.00035 -99.485 0.02455 0.00080 0.00014 0.00015 0.00015 0.00035 -99.5 0.02518 0.00080 0.00014 0.00015 0.00015 0.00035 -99.515 0.02363 0.00081 0.00014 0.00015 0.00015 0.00035 -99.53 0.01859 0.00081 0.00014 0.00015 0.00015 0.00036 -99.545 0.01282 0.00081 0.00014 0.00015 0.00015 0.00036 -99.56 0.00803 0.00081 0.00014 0.00015 0.00015 0.00036 -99.575 0.00459 0.00081 0.00014 0.00015 0.00015 0.00036 -99.59 0.00278 0.00082 0.00014 0.00015 0.00015 0.00036 -99.605 0.00260 0.00082 0.00014 0.00015 0.00015 0.00036 -99.62 0.00282 0.00082 0.00014 0.00015 0.00015 0.00036 -99.635 0.00273 0.00082 0.00014 0.00015 0.00015 0.00036 -99.65 0.00308 0.00082 0.00014 0.00015 0.00015 0.00037 -99.665 0.00443 0.00083 0.00014 0.00015 0.00015 0.00037 -99.68 0.00691 0.00083 0.00014 0.00015 0.00015 0.00037 -99.695 0.00929 0.00083 0.00014 0.00015 0.00015 0.00037 -99.71 0.01002 0.00083 0.00014 0.00015 0.00015 0.00037 -99.725 0.00892 0.00083 0.00014 0.00015 0.00015 0.00037 -99.74 0.00646 0.00084 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