##TITLE=              29Si CP MAS NMR spectrum of as-made pure silica Dodecasil-3C (with THF and xenon)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Ripmeester et al. J. Chem. Soc., Chem. Commun., 608-610 (1988) Figure 2
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 15:44:25
##SOURCE REFERENCE=   MTN-29Si-Ripmeester-1988-thf
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              MTN
##NAMES=              Dodecasil-3C
##NAMES=              ZSM-39
##SAMPLE DESCRIPTION= Dodecasil-3C, as-made, THF/Xe
##TEMPERATURE=        295 K

$$Bibliographic information 
##$AUTHORS=           Ripmeester, J.A., Desando, M.A., Handa, Y.P., Tse, J.S.
##$TITLE=             Thermally induced phase transitions in the clathrasil dodecasil-3C (zeolite ZSM-39)
##$JOURNAL=           Journal of the Chemical Society, Chemical Communications
##$VOLUME=            
##$PAGES=             608-610
##$YEAR=              1988
##$DOI=               10.1039/C39880000608
##$FIGURE=            Figure 2

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         5
##$PEAK LABELS=      Si1/Si2/Si3 Si1/Si2/Si3 Si1/Si2/Si3 Si4       Si5         
##$PEAK TSITES=        T1         T1         T1         T2         T3
##$PEAK POSITIONS=    -121.641   -120.173   -119.31    -116.359   -111.084   
##$PEAK AREAS=         4.         4.         4.         4.         1.        
##$PEAK WIDTHS=        0.64814    0.59738    0.53019    0.85047    1.21084   
##$PEAK SHAPES=        0.5812     0.5812     0.5812     0.5812     0.5812    
##$NUMBERING REF=     Knorr and Depmeier, Acta Cryst. B53, 18-24 (1997)
##$ASSIGN REF=        Fyfe et al. J. Am. Chem. Soc. 111, 7702-7707 (1989) Figure 5
##$ASSIGN METHOD=     relative intensities, 2D correlation NMR
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 35.8
##.PULSE SEQUENCE=    cross polarization
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -107.62               
##LASTX=              -129.88               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            1114
##FIRSTY=              0.16188              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -107.62              0.16188              
 -107.64              0.15755              
 -107.66              0.15253              
 -107.68              0.15266              
 -107.7               0.15401              
 -107.72              0.15099              
 -107.74              0.14535              
 -107.76              0.14499              
 -107.78              0.14565              
 -107.8               0.14534              
 -107.82              0.14536              
 -107.84              0.14581              
 -107.86              0.14410              
 -107.88              0.13675              
 -107.9               0.12488              
 -107.92              0.12130              
 -107.94              0.12294              
 -107.96              0.12263              
 -107.98              0.12252              
 -108.                0.12268              
 -108.02              0.12255              
 -108.04              0.12245              
 -108.06              0.12342              
 -108.08              0.12060              
 -108.1               0.11492              
 -108.12              0.11458              
 -108.14              0.11519              
 -108.16              0.11498              
 -108.18              0.11502              
 -108.2               0.11473              
 -108.22              0.11572              
 -108.24              0.11450              
 -108.26              0.10801              
 -108.28              0.11062              
 -108.3               0.11590              
 -108.32              0.11505              
 -108.34              0.11498              
 -108.36              0.11459              
 -108.38              0.11554              
 -108.4               0.12117              
 -108.42              0.12776              
 -108.44              0.13078              
 -108.46              0.13019              
 -108.48              0.13013              
 -108.5               0.13025              
 -108.52              0.13020              
 -108.54              0.13021              
 -108.56              0.13021              
 -108.58              0.13021              
 -108.6               0.13021              
 -108.62              0.13021              
 -108.64              0.13019              
 -108.66              0.13024              
 -108.68              0.13022              
 -108.7               0.12999              
 -108.72              0.13090              
 -108.74              0.12941              
 -108.76              0.12338              
 -108.78              0.12244              
 -108.8               0.12144              
 -108.82              0.11476              
 -108.84              0.10769              
 -108.86              0.11105              
 -108.88              0.11459              
 -108.9               0.10805              
 -108.92              0.10660              
 -108.94              0.10768              
 -108.96              0.10736              
 -108.98              0.10736              
 -109.                0.10743              
 -109.02              0.10736              
 -109.04              0.10738              
 -109.06              0.10763              
 -109.08              0.10667              
 -109.1               0.10824              
 -109.12              0.11432              
 -109.14              0.11465              
 -109.16              0.11733              
 -109.18              0.12260              
 -109.2               0.11712              
 -109.22              0.11401              
 -109.24              0.11517              
 -109.26              0.11499              
 -109.28              0.11538              
 -109.3               0.11386              
 -109.32              0.11585              
 -109.34              0.12768              
 -109.36              0.13184              
 -109.38              0.12953              
 -109.4               0.13008              
 -109.42              0.13491              
 -109.44              0.14179              
 -109.46              0.14561              
 -109.48              0.14509              
 -109.5               0.14958              
 -109.52              0.15436              
 -109.54              0.15287              
 -109.56              0.14694              
 -109.58              0.14480              
 -109.6               0.14541              
 -109.62              0.14526              
 -109.64              0.14706              
 -109.66              0.14023              
 -109.68              0.12962              
 -109.7               0.13006              
 -109.72              0.12736              
 -109.74              0.12014              
 -109.76              0.11510              
 -109.78              0.11464              
 -109.8               0.11515              
 -109.82              0.11497              
 -109.84              0.11498              
 -109.86              0.11506              
 -109.88              0.11486              
 -109.9               0.11503              
 -109.92              0.11574              
 -109.94              0.11146              
 -109.96              0.10675              
 -109.98              0.10727              
 -110.                0.10755              
 -110.02              0.10733              
 -110.04              0.10740              
 -110.06              0.10740              
 -110.08              0.10738              
 -110.1               0.10741              
 -110.12              0.10740              
 -110.14              0.10727              
 -110.16              0.10777              
 -110.18              0.10694              
 -110.2               0.10630              
 -110.22              0.11684              
 -110.24              0.12340              
 -110.26              0.12276              
 -110.28              0.13315              
 -110.3               0.14548              
 -110.32              0.15585              
 -110.34              0.16692              
 -110.36              0.17841              
 -110.38              0.18748              
 -110.4               0.19113              
 -110.42              0.19056              
 -110.44              0.19627              
 -110.46              0.21371              
 -110.48              0.23603              
 -110.5               0.24846              
 -110.52              0.25711              
 -110.54              0.27025              
 -110.56              0.28730              
 -110.58              0.29818              
 -110.6               0.31332              
 -110.62              0.34485              
 -110.64              0.38961              
 -110.66              0.42584              
 -110.68              0.44659              
 -110.7               0.47429              
 -110.72              0.54459              
 -110.74              0.60143              
 -110.76              0.63788              
 -110.78              0.69533              
 -110.8               0.72948              
 -110.82              0.74370              
 -110.84              0.76790              
 -110.86              0.81187              
 -110.88              0.84919              
 -110.9               0.87206              
 -110.92              0.88885              
 -110.94              0.89519              
 -110.96              0.90305              
 -110.98              0.91389              
 -111.                0.91418              
 -111.02              0.91402              
 -111.04              0.91240              
 -111.06              0.90639              
 -111.08              0.90612              
 -111.1               0.90359              
 -111.12              0.88799              
 -111.14              0.85982              
 -111.16              0.83672              
 -111.18              0.81258              
 -111.2               0.78499              
 -111.22              0.7693               
 -111.24              0.74460              
 -111.26              0.70885              
 -111.28              0.67610              
 -111.3               0.64387              
 -111.32              0.60968              
 -111.34              0.58613              
 -111.36              0.58383              
 -111.38              0.55425              
 -111.4               0.50577              
 -111.42              0.47459              
 -111.44              0.46152              
 -111.46              0.45129              
 -111.48              0.43121              
 -111.5               0.40266              
 -111.52              0.38401              
 -111.54              0.36566              
 -111.56              0.34359              
 -111.58              0.33724              
 -111.6               0.33001              
 -111.62              0.31837              
 -111.64              0.31300              
 -111.66              0.31320              
 -111.68              0.31083              
 -111.7               0.30493              
 -111.72              0.30401              
 -111.74              0.30899              
 -111.76              0.31336              
 -111.78              0.31285              
 -111.8               0.31268              
 -111.82              0.31263              
 -111.84              0.31290              
 -111.86              0.31345              
 -111.88              0.30831              
 -111.9               0.30503              
 -111.92              0.30525              
 -111.94              0.29561              
 -111.96              0.28221              
 -111.98              0.27362              
 -112.                0.26879              
 -112.02              0.25450              
 -112.04              0.23731              
 -112.06              0.22043              
 -112.08              0.19782              
 -112.1               0.18136              
 -112.12              0.17466              
 -112.14              0.16930              
 -112.16              0.15387              
 -112.18              0.13840              
 -112.2               0.12922              
 -112.22              0.12342              
 -112.24              0.12191              
 -112.26              0.12316              
 -112.28              0.12269              
 -112.3               0.11697              
 -112.32              0.11421              
 -112.34              0.11513              
 -112.36              0.11501              
 -112.38              0.11517              
 -112.4               0.11450              
 -112.42              0.1152               
 -112.44              0.12100              
 -112.46              0.12358              
 -112.48              0.12209              
 -112.5               0.12227              
 -112.52              0.12779              
 -112.54              0.13102              
 -112.56              0.13010              
 -112.58              0.13012              
 -112.6               0.13032              
 -112.62              0.13007              
 -112.64              0.13019              
 -112.66              0.13110              
 -112.68              0.12671              
 -112.7               0.12247              
 -112.72              0.12327              
 -112.74              0.11410              
 -112.76              0.10390              
 -112.78              0.09955              
 -112.8               0.09426              
 -112.82              0.08782              
 -112.84              0.08406              
 -112.86              0.08450              
 -112.88              0.08465              
 -112.9               0.08465              
 -112.92              0.08447              
 -112.94              0.08412              
 -112.96              0.08797              
 -112.98              0.09467              
 -113.                0.09973              
 -113.02              0.10027              
 -113.04              0.09918              
 -113.06              0.10041              
 -113.08              0.10605              
 -113.1               0.11376              
 -113.12              0.11283              
 -113.14              0.10739              
 -113.16              0.11308              
 -113.18              0.11579              
 -113.2               0.11514              
 -113.22              0.11529              
 -113.24              0.10950              
 -113.26              0.10762              
 -113.28              0.10653              
 -113.3               0.09505              
 -113.32              0.08650              
 -113.34              0.08420              
 -113.36              0.08456              
 -113.38              0.08484              
 -113.4               0.08384              
 -113.42              0.08553              
 -113.44              0.09151              
 -113.46              0.09261              
 -113.48              0.09249              
 -113.5               0.09196              
 -113.52              0.08610              
 -113.54              0.08378              
 -113.56              0.08476              
 -113.58              0.08460              
 -113.6               0.08453              
 -113.62              0.08459              
 -113.64              0.08457              
 -113.66              0.08458              
 -113.68              0.08453              
 -113.7               0.08466              
 -113.72              0.08458              
 -113.74              0.08397              
 -113.76              0.08719              
 -113.78              0.09357              
 -113.8               0.09904              
 -113.82              0.10347              
 -113.84              0.11223              
 -113.86              0.12312              
 -113.88              0.12835              
 -113.9               0.13655              
 -113.92              0.14941              
 -113.94              0.16012              
 -113.96              0.16146              
 -113.98              0.16034              
 -114.                0.16064              
 -114.02              0.16052              
 -114.04              0.16133              
 -114.06              0.15900              
 -114.08              0.15308              
 -114.1               0.14871              
 -114.12              0.13679              
 -114.14              0.11868              
 -114.16              0.10234              
 -114.18              0.08649              
 -114.2               0.06846              
 -114.22              0.05352              
 -114.24              0.04857              
 -114.26              0.03871              
 -114.28              0.03013              
 -114.3               0.03124              
 -114.32              0.03069              
 -114.34              0.03429              
 -114.36              0.03908              
 -114.38              0.03811              
 -114.4               0.04678              
 -114.42              0.05685              
 -114.44              0.06170              
 -114.46              0.07212              
 -114.48              0.08392              
 -114.5               0.09455              
 -114.52              0.10554              
 -114.54              0.11710              
 -114.56              0.12616              
 -114.58              0.13034              
 -114.6               0.13044              
 -114.62              0.13004              
 -114.64              0.13033              
 -114.66              0.13028              
 -114.68              0.12939              
 -114.7               0.13298              
 -114.72              0.13824              
 -114.74              0.13809              
 -114.76              0.13758              
 -114.78              0.13796              
 -114.8               0.13782              
 -114.82              0.13720              
 -114.84              0.14052              
 -114.86              0.14681              
 -114.88              0.15223              
 -114.9               0.15734              
 -114.92              0.16384              
 -114.94              0.16829              
 -114.96              0.16732              
 -114.98              0.17482              
 -115.                0.18638              
 -115.02              0.19099              
 -115.04              0.19043              
 -115.06              0.19393              
 -115.08              0.19893              
 -115.1               0.19830              
 -115.12              0.20298              
 -115.14              0.20661              
 -115.16              0.20626              
 -115.18              0.21208              
 -115.2               0.21402              
 -115.22              0.21473              
 -115.24              0.22084              
 -115.26              0.22185              
 -115.28              0.22230              
 -115.3               0.23001              
 -115.32              0.24264              
 -115.34              0.24134              
 -115.36              0.23659              
 -115.38              0.24354              
 -115.4               0.25384              
 -115.42              0.26734              
 -115.44              0.28537              
 -115.46              0.30290              
 -115.48              0.30752              
 -115.5               0.32141              
 -115.52              0.35079              
 -115.54              0.3677               
 -115.56              0.38704              
 -115.58              0.42072              
 -115.6               0.4601               
 -115.62              0.48177              
 -115.64              0.49264              
 -115.66              0.51291              
 -115.68              0.55550              
 -115.7               0.60896              
 -115.72              0.66464              
 -115.74              0.71945              
 -115.76              0.76877              
 -115.78              0.79573              
 -115.8               0.84242              
 -115.82              0.94474              
 -115.84              1.00364              
 -115.86              1.08691              
 -115.88              1.21052              
 -115.9               1.25527              
 -115.92              1.32355              
 -115.94              1.48426              
 -115.96              1.69658              
 -115.98              1.85826              
 -116.                2.00453              
 -116.02              2.12058              
 -116.04              2.17239              
 -116.06              2.39209              
 -116.08              2.63506              
 -116.1               2.74515              
 -116.12              2.9128               
 -116.14              3.06229              
 -116.16              3.18945              
 -116.18              3.36069              
 -116.2               3.46711              
 -116.22              3.53625              
 -116.24              3.62958              
 -116.26              3.72905              
 -116.28              3.75475              
 -116.3               3.74178              
 -116.32              3.74079              
 -116.34              3.66748              
 -116.36              3.57376              
 -116.38              3.5095               
 -116.4               3.45247              
 -116.42              3.36961              
 -116.44              3.26837              
 -116.46              3.17145              
 -116.48              3.08065              
 -116.5               2.97541              
 -116.52              2.86803              
 -116.54              2.7817               
 -116.56              2.68833              
 -116.58              2.61946              
 -116.6               2.56345              
 -116.62              2.44275              
 -116.64              2.3113               
 -116.66              2.23304              
 -116.68              2.19398              
 -116.7               2.0867               
 -116.72              1.96316              
 -116.74              1.88171              
 -116.76              1.82034              
 -116.78              1.7205               
 -116.8               1.63027              
 -116.82              1.58638              
 -116.84              1.52094              
 -116.86              1.46531              
 -116.88              1.41164              
 -116.9               1.33093              
 -116.92              1.28654              
 -116.94              1.23902              
 -116.96              1.17171              
 -116.98              1.1405               
 -117.                1.0864               
 -117.02              0.99790              
 -117.04              0.91537              
 -117.06              0.86449              
 -117.08              0.82745              
 -117.1               0.78849              
 -117.12              0.75007              
 -117.14              0.71040              
 -117.16              0.65986              
 -117.18              0.61119              
 -117.2               0.60251              
 -117.22              0.59409              
 -117.24              0.57722              
 -117.26              0.57293              
 -117.28              0.55959              
 -117.3               0.54264              
 -117.32              0.53325              
 -117.34              0.52806              
 -117.36              0.51996              
 -117.38              0.50702              
 -117.4               0.49038              
 -117.42              0.46937              
 -117.44              0.44621              
 -117.46              0.42514              
 -117.48              0.40867              
 -117.5               0.39123              
 -117.52              0.36240              
 -117.54              0.32272              
 -117.56              0.29108              
 -117.58              0.27619              
 -117.6               0.26395              
 -117.62              0.24066              
 -117.64              0.22863              
 -117.66              0.21270              
 -117.68              0.19087              
 -117.7               0.1904               
 -117.72              0.18772              
 -117.74              0.18378              
 -117.76              0.19033              
 -117.78              0.19176              
 -117.8               0.19107              
 -117.82              0.19089              
 -117.84              0.18974              
 -117.86              0.19887              
 -117.88              0.20771              
 -117.9               0.20639              
 -117.92              0.20599              
 -117.94              0.20639              
 -117.96              0.20625              
 -117.98              0.20626              
 -118.                0.20627              
 -118.02              0.20629              
 -118.04              0.20627              
 -118.06              0.20612              
 -118.08              0.20680              
 -118.1               0.20545              
 -118.12              0.19960              
 -118.14              0.19313              
 -118.16              0.19046              
 -118.18              0.19111              
 -118.2               0.19111              
 -118.22              0.19106              
 -118.24              0.19098              
 -118.26              0.19102              
 -118.28              0.19170              
 -118.3               0.18858              
 -118.32              0.18244              
 -118.34              0.17710              
 -118.36              0.17071              
 -118.38              0.16804              
 -118.4               0.16819              
 -118.42              0.16276              
 -118.44              0.15874              
 -118.46              0.16243              
 -118.48              0.16841              
 -118.5               0.16354              
 -118.52              0.18405              
 -118.54              0.22448              
 -118.56              0.24451              
 -118.58              0.28435              
 -118.6               0.36361              
 -118.62              0.45349              
 -118.64              0.50170              
 -118.66              0.54558              
 -118.68              0.61641              
 -118.7               0.71299              
 -118.72              0.82154              
 -118.74              0.90265              
 -118.76              0.95293              
 -118.78              1.01615              
 -118.8               1.09205              
 -118.82              1.19912              
 -118.84              1.33249              
 -118.86              1.42676              
 -118.88              1.54911              
 -118.9               1.69376              
 -118.92              1.78041              
 -118.94              1.88499              
 -118.96              2.05051              
 -118.98              2.27878              
 -119.                2.55709              
 -119.02              2.84214              
 -119.04              3.05435              
 -119.06              3.21351              
 -119.08              3.57837              
 -119.1               4.06195              
 -119.12              4.46118              
 -119.14              4.70736              
 -119.16              4.94213              
 -119.18              5.21642              
 -119.2               5.47255              
 -119.22              5.65876              
 -119.24              5.88831              
 -119.26              6.09776              
 -119.28              6.10892              
 -119.3               6.099                
 -119.32              6.07767              
 -119.34              5.9646               
 -119.36              5.76695              
 -119.38              5.59004              
 -119.4               5.46785              
 -119.42              5.34219              
 -119.44              5.15325              
 -119.46              4.98889              
 -119.48              4.88918              
 -119.5               4.74126              
 -119.52              4.42628              
 -119.54              4.15697              
 -119.56              4.11298              
 -119.58              4.01743              
 -119.6               3.77347              
 -119.62              3.47977              
 -119.64              3.27743              
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##END=
