##TITLE=              29Si MAS NMR spectrum of pure silica Dodecasil-3C (cubic phase at 383 K)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Strobl et al. J. Am. Chem. Soc., 109, 4733-4734 (1987) Figure 1
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 15:35:56
##SOURCE REFERENCE=   MTN-29Si-Strobl-1987-383K
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              MTN
##NAMES=              Dodecasil-3C
##NAMES=              ZSM-39
##SAMPLE DESCRIPTION= Dodecasil-3C, cubic phase
##TEMPERATURE=        383 K

$$Bibliographic information 
##$AUTHORS=           Strobl, H., Fyfe, C.A., Kokotailo, G.T., Pasztor, C.T., Bibby, D.M.
##$TITLE=             High-Symmetry, High-Temperature Zeolite Lattice Structures
##$JOURNAL=           Journal of the American Chemical Society
##$VOLUME=            109
##$PAGES=             4733-4734
##$YEAR=              1987
##$DOI=               10.1021/ja00249a053
##$FIGURE=            Figure 1

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         3
##$PEAK LABELS=        Si1        Si2        Si3       
##$PEAK TSITES=        T1         T2         T3        
##$PEAK POSITIONS=    -119.556   -115.157   -109.254   
##$PEAK AREAS=         24.        8.         1.        
##$PEAK WIDTHS=        0.40135    0.35918    0.35918   
##$PEAK SHAPES=        1          1          1         
##$NUMBERING REF=     Gies, H. Z. Kristallogr. 167, 73-82 (1984)
##$ASSIGN REF=        Strobl et al. J. Am. Chem. Soc., 109, 4733-4734 (1987) Figure 1
##$ASSIGN METHOD=     relative intensities
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 79.5
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -100.08               
##LASTX=              -125.06               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            1250
##FIRSTY=             -0.17883              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -100.08             -0.17883              
 -100.1              -0.19108              
 -100.12             -0.1907               
 -100.14             -0.19056              
 -100.16             -0.19052              
 -100.18             -0.19052              
 -100.2              -0.19051              
 -100.22             -0.19051              
 -100.24             -0.19051              
 -100.26             -0.19051              
 -100.28             -0.19051              
 -100.3              -0.19045              
 -100.32             -0.19056              
 -100.34             -0.18954              
 -100.36             -0.19174              
 -100.38             -0.26152              
 -100.4              -0.33781              
 -100.42             -0.33579              
 -100.44             -0.33476              
 -100.46             -0.33453              
 -100.48             -0.33444              
 -100.5              -0.33442              
 -100.52             -0.33370              
 -100.54             -0.33411              
 -100.56             -0.39527              
 -100.58             -0.46247              
 -100.6              -0.45060              
 -100.62             -0.38033              
 -100.64             -0.32081              
 -100.66             -0.24985              
 -100.68             -0.20169              
 -100.7              -0.21862              
 -100.72             -0.29518              
 -100.74             -0.33454              
 -100.76             -0.33371              
 -100.78             -0.32793              
 -100.8              -0.24318              
 -100.82             -0.18909              
 -100.84             -0.19040              
 -100.86             -0.19040              
 -100.88             -0.19051              
 -100.9              -0.19050              
 -100.92             -0.19051              
 -100.94             -0.19051              
 -100.96             -0.19051              
 -100.98             -0.19051              
 -101.               -0.19051              
 -101.02             -0.19051              
 -101.04             -0.19051              
 -101.06             -0.19051              
 -101.08             -0.19051              
 -101.1              -0.19051              
 -101.12             -0.19051              
 -101.14             -0.19051              
 -101.16             -0.19051              
 -101.18             -0.19051              
 -101.2              -0.19051              
 -101.22             -0.19051              
 -101.24             -0.19051              
 -101.26             -0.19051              
 -101.28             -0.19051              
 -101.3              -0.19051              
 -101.32             -0.19051              
 -101.34             -0.19051              
 -101.36             -0.19051              
 -101.38             -0.19051              
 -101.4              -0.19051              
 -101.42             -0.19046              
 -101.44             -0.19045              
 -101.46             -0.1897               
 -101.48             -0.17522              
 -101.5              -0.11534              
 -101.52             -0.04680              
 -101.54              0.04054              
 -101.56              0.09792              
 -101.58              0.02858              
 -101.6              -0.04836              
 -101.62             -0.04816              
 -101.64             -0.04616              
 -101.66             -0.04397              
 -101.68             -0.12596              
 -101.7              -0.18770              
 -101.72             -0.18973              
 -101.74             -0.19034              
 -101.76             -0.19010              
 -101.78             -0.19023              
 -101.8              -0.18452              
 -101.82             -0.11958              
 -101.84             -0.04249              
 -101.86             -0.04669              
 -101.88             -0.04612              
 -101.9              -0.04669              
 -101.92             -0.04440              
 -101.94             -0.02765              
 -101.96             -0.02645              
 -101.98             -0.03498              
 -102.               -0.04349              
 -102.02             -0.04622              
 -102.04             -0.04648              
 -102.06             -0.04653              
 -102.08             -0.04655              
 -102.1              -0.04656              
 -102.12             -0.04656              
 -102.14             -0.04656              
 -102.16             -0.04656              
 -102.18             -0.04659              
 -102.2              -0.04654              
 -102.22             -0.04713              
 -102.24             -0.04593              
 -102.26             -0.05627              
 -102.28             -0.12470              
 -102.3              -0.18808              
 -102.32             -0.13369              
 -102.34             -0.05051              
 -102.36             -0.04776              
 -102.38             -0.04677              
 -102.4              -0.04692              
 -102.42             -0.04674              
 -102.44             -0.05109              
 -102.46             -0.09417              
 -102.48             -0.15181              
 -102.5              -0.19101              
 -102.52             -0.18964              
 -102.54             -0.1906               
 -102.56             -0.19044              
 -102.58             -0.19052              
 -102.6              -0.19051              
 -102.62             -0.19051              
 -102.64             -0.19051              
 -102.66             -0.19051              
 -102.68             -0.19051              
 -102.7              -0.19051              
 -102.72             -0.19051              
 -102.74             -0.19051              
 -102.76             -0.19051              
 -102.78             -0.19051              
 -102.8              -0.19051              
 -102.82             -0.19051              
 -102.84             -0.19051              
 -102.86             -0.19051              
 -102.88             -0.19051              
 -102.9              -0.19051              
 -102.92             -0.19051              
 -102.94             -0.19051              
 -102.96             -0.19051              
 -102.98             -0.19051              
 -103.               -0.19051              
 -103.02             -0.19051              
 -103.04             -0.19051              
 -103.06             -0.19051              
 -103.08             -0.19051              
 -103.1              -0.19051              
 -103.12             -0.19051              
 -103.14             -0.19051              
 -103.16             -0.19051              
 -103.18             -0.19051              
 -103.2              -0.19051              
 -103.22             -0.19051              
 -103.24             -0.19051              
 -103.26             -0.19051              
 -103.28             -0.19051              
 -103.3              -0.19053              
 -103.32             -0.19054              
 -103.34             -0.19086              
 -103.36             -0.19078              
 -103.38             -0.1965               
 -103.4              -0.26149              
 -103.42             -0.33805              
 -103.44             -0.33447              
 -103.46             -0.32660              
 -103.48             -0.25817              
 -103.5              -0.18571              
 -103.52             -0.19132              
 -103.54             -0.18773              
 -103.56             -0.19316              
 -103.58             -0.24829              
 -103.6              -0.30259              
 -103.62             -0.26707              
 -103.64             -0.18700              
 -103.66             -0.19008              
 -103.68             -0.19018              
 -103.7              -0.19048              
 -103.72             -0.18977              
 -103.74             -0.19055              
 -103.76             -0.25623              
 -103.78             -0.33620              
 -103.8              -0.33196              
 -103.82             -0.33532              
 -103.84             -0.32457              
 -103.86             -0.25628              
 -103.88             -0.19292              
 -103.9              -0.24739              
 -103.92             -0.33051              
 -103.94             -0.33297              
 -103.96             -0.33387              
 -103.98             -0.32910              
 -104.               -0.26495              
 -104.02             -0.18402              
 -104.04             -0.14117              
 -104.06             -0.15217              
 -104.08             -0.16504              
 -104.1              -0.18034              
 -104.12             -0.19730              
 -104.14             -0.21518              
 -104.16             -0.23321              
 -104.18             -0.25063              
 -104.2              -0.26671              
 -104.22             -0.28067              
 -104.24             -0.31145              
 -104.26             -0.33347              
 -104.28             -0.33526              
 -104.3              -0.33554              
 -104.32             -0.24964              
 -104.34             -0.19103              
 -104.36             -0.19233              
 -104.38             -0.19035              
 -104.4              -0.20305              
 -104.42             -0.29016              
 -104.44             -0.33681              
 -104.46             -0.33420              
 -104.48             -0.33385              
 -104.5              -0.33376              
 -104.52             -0.33385              
 -104.54             -0.33407              
 -104.56             -0.33434              
 -104.58             -0.33421              
 -104.6              -0.33419              
 -104.62             -0.33050              
 -104.64             -0.28770              
 -104.66             -0.23011              
 -104.68             -0.19056              
 -104.7              -0.19148              
 -104.72             -0.19039              
 -104.74             -0.19277              
 -104.76             -0.18905              
 -104.78             -0.13446              
 -104.8              -0.07617              
 -104.82             -0.04853              
 -104.84             -0.04826              
 -104.86             -0.07570              
 -104.88             -0.13361              
 -104.9              -0.18858              
 -104.92             -0.18956              
 -104.94             -0.19039              
 -104.96             -0.16565              
 -104.98             -0.09534              
 -105.               -0.04441              
 -105.02             -0.04663              
 -105.04             -0.04650              
 -105.06             -0.04648              
 -105.08             -0.04916              
 -105.1              -0.04762              
 -105.12             -0.06919              
 -105.14             -0.09713              
 -105.16             -0.1277               
 -105.18             -0.15714              
 -105.2              -0.18174              
 -105.22             -0.18821              
 -105.24             -0.19023              
 -105.26             -0.19032              
 -105.28             -0.19050              
 -105.3              -0.1905               
 -105.32             -0.19051              
 -105.34             -0.19050              
 -105.36             -0.19051              
 -105.38             -0.19043              
 -105.4              -0.19060              
 -105.42             -0.16035              
 -105.44             -0.08952              
 -105.46             -0.04844              
 -105.48             -0.04714              
 -105.5              -0.04720              
 -105.52             -0.00960              
 -105.54             -0.01013              
 -105.56             -0.03424              
 -105.58             -0.04737              
 -105.6              -0.04683              
 -105.62             -0.04656              
 -105.64             -0.04658              
 -105.66             -0.04656              
 -105.68             -0.04656              
 -105.7              -0.04656              
 -105.72             -0.04656              
 -105.74             -0.04656              
 -105.76             -0.04656              
 -105.78             -0.04656              
 -105.8              -0.04656              
 -105.82             -0.04656              
 -105.84             -0.04656              
 -105.86             -0.04656              
 -105.88             -0.04656              
 -105.9              -0.04656              
 -105.92             -0.04656              
 -105.94             -0.04656              
 -105.96             -0.04656              
 -105.98             -0.04656              
 -106.               -0.04656              
 -106.02             -0.04656              
 -106.04             -0.04656              
 -106.06             -0.04656              
 -106.08             -0.04656              
 -106.1              -0.04657              
 -106.12             -0.04656              
 -106.14             -0.04654              
 -106.16             -0.04647              
 -106.18             -0.04646              
 -106.2              -0.04414              
 -106.22              0.00239              
 -106.24             -0.01564              
 -106.26             -0.03955              
 -106.28             -0.04543              
 -106.3              -0.04663              
 -106.32             -0.04647              
 -106.34             -0.04656              
 -106.36             -0.04656              
 -106.38             -0.04656              
 -106.4              -0.04656              
 -106.42             -0.04656              
 -106.44             -0.04655              
 -106.46             -0.04653              
 -106.48             -0.04651              
 -106.5              -0.04600              
 -106.52             -0.04615              
 -106.54             -0.10887              
 -106.56             -0.18999              
 -106.58             -0.18829              
 -106.6              -0.19073              
 -106.62             -0.18214              
 -106.64             -0.11407              
 -106.66             -0.04187              
 -106.68             -0.04717              
 -106.7              -0.04639              
 -106.72             -0.04640              
 -106.74             -0.04595              
 -106.76             -0.04283              
 -106.78              0.01994              
 -106.8               0.10064              
 -106.82              0.09786              
 -106.84              0.09946              
 -106.86              0.14352              
 -106.88              0.31127              
 -106.9               0.38548              
 -106.92              0.38399              
 -106.94              0.38537              
 -106.96              0.38553              
 -106.98              0.3849               
 -107.                0.30479              
 -107.02              0.16017              
 -107.04              0.09940              
 -107.06              0.09781              
 -107.08              0.09758              
 -107.1               0.09811              
 -107.12              0.09828              
 -107.14             -0.00541              
 -107.16             -0.16332              
 -107.18             -0.18907              
 -107.2              -0.19049              
 -107.22             -0.19005              
 -107.24             -0.19067              
 -107.26             -0.18457              
 -107.28             -0.13940              
 -107.3              -0.08655              
 -107.32             -0.04190              
 -107.34              0.04075              
 -107.36              0.09848              
 -107.38              0.09775              
 -107.4               0.09748              
 -107.42              0.09740              
 -107.44              0.09739              
 -107.46              0.09738              
 -107.48              0.09734              
 -107.5               0.09737              
 -107.52              0.09661              
 -107.54              0.09756              
 -107.56              0.08443              
 -107.58             -0.00213              
 -107.6               0.00027              
 -107.62              0.07669              
 -107.64              0.09727              
 -107.66              0.09737              
 -107.68              0.09738              
 -107.7               0.09738              
 -107.72              0.09738              
 -107.74              0.09738              
 -107.76              0.09738              
 -107.78              0.09738              
 -107.8               0.09738              
 -107.82              0.09738              
 -107.84              0.09738              
 -107.86              0.09738              
 -107.88              0.09738              
 -107.9               0.09738              
 -107.92              0.09738              
 -107.94              0.09738              
 -107.96              0.09738              
 -107.98              0.09738              
 -108.                0.09738              
 -108.02              0.09738              
 -108.04              0.09738              
 -108.06              0.09738              
 -108.08              0.09738              
 -108.1               0.09738              
 -108.12              0.09738              
 -108.14              0.09738              
 -108.16              0.09734              
 -108.18              0.09740              
 -108.2               0.09666              
 -108.22              0.09801              
 -108.24              0.08530              
 -108.26              0.01128              
 -108.28             -0.03633              
 -108.3              -0.04678              
 -108.32             -0.04625              
 -108.34             -0.08601              
 -108.36             -0.16242              
 -108.38             -0.19063              
 -108.4              -0.19048              
 -108.42             -0.18961              
 -108.44             -0.16741              
 -108.46             -0.08354              
 -108.48             -0.04645              
 -108.5              -0.04722              
 -108.52             -0.04651              
 -108.54             -0.04661              
 -108.56             -0.04655              
 -108.58             -0.04656              
 -108.6              -0.04656              
 -108.62             -0.04656              
 -108.64             -0.04656              
 -108.66             -0.04655              
 -108.68             -0.04652              
 -108.7              -0.04651              
 -108.72             -0.04592              
 -108.74             -0.04618              
 -108.76             -0.03576              
 -108.78              0.04908              
 -108.8               0.11391              
 -108.82              0.24584              
 -108.84              0.39374              
 -108.86              0.38498              
 -108.88              0.37596              
 -108.9               0.39426              
 -108.92              0.61602              
 -108.94              0.83093              
 -108.96              0.97595              
 -108.98              1.06853              
 -109.                1.19409              
 -109.02              1.31412              
 -109.04              1.48132              
 -109.06              1.73197              
 -109.08              1.87088              
 -109.1               2.11433              
 -109.12              2.35462              
 -109.14              2.46167              
 -109.16              2.69789              
 -109.18              2.79424              
 -109.2               2.86227              
 -109.22              2.96669              
 -109.24              3.02847              
 -109.26              3.07251              
 -109.28              2.99291              
 -109.3               2.93367              
 -109.32              2.69166              
 -109.34              2.36052              
 -109.36              2.33146              
 -109.38              2.07033              
 -109.4               1.89599              
 -109.42              1.70482              
 -109.44              1.46474              
 -109.46              1.39046              
 -109.48              1.27442              
 -109.5               1.19907              
 -109.52              1.19849              
 -109.54              1.19836              
 -109.56              1.13688              
 -109.58              1.05227              
 -109.6               1.01221              
 -109.62              0.95521              
 -109.64              0.91445              
 -109.66              0.91413              
 -109.68              0.91343              
 -109.7               0.87156              
 -109.72              0.81745              
 -109.74              0.81908              
 -109.76              0.81682              
 -109.78              0.75032              
 -109.8               0.67073              
 -109.82              0.67514              
 -109.84              0.67299              
 -109.86              0.67225              
 -109.88              0.64417              
 -109.9               0.56828              
 -109.92              0.47139              
 -109.94              0.38858              
 -109.96              0.38659              
 -109.98              0.38544              
 -110.                0.38539              
 -110.02              0.38529              
 -110.04              0.38530              
 -110.06              0.38529              
 -110.08              0.38529              
 -110.1               0.38529              
 -110.12              0.38529              
 -110.14              0.38529              
 -110.16              0.38524              
 -110.18              0.38534              
 -110.2               0.38547              
 -110.22              0.38619              
 -110.24              0.38728              
 -110.26              0.30329              
 -110.28              0.24299              
 -110.3               0.24226              
 -110.32              0.24140              
 -110.34              0.24141              
 -110.36              0.24134              
 -110.38              0.24134              
 -110.4               0.24134              
 -110.42              0.24134              
 -110.44              0.24134              
 -110.46              0.24134              
 -110.48              0.24134              
 -110.5               0.24134              
 -110.52              0.24134              
 -110.54              0.24134              
 -110.56              0.24134              
 -110.58              0.24134              
 -110.6               0.24134              
 -110.62              0.24134              
 -110.64              0.24144              
 -110.66              0.24136              
 -110.68              0.24307              
 -110.7               0.24089              
 -110.72              0.15162              
 -110.74              0.09668              
 -110.76              0.16738              
 -110.78              0.24369              
 -110.8               0.24297              
 -110.82              0.24159              
 -110.84              0.24151              
 -110.86              0.24179              
 -110.88              0.24219              
 -110.9               0.18277              
 -110.92              0.10027              
 -110.94              0.10756              
 -110.96              0.19154              
 -110.98              0.24252              
 -111.                0.24135              
 -111.02              0.23161              
 -111.04              0.15883              
 -111.06              0.10846              
 -111.08              0.09717              
 -111.1               0.09725              
 -111.12              0.09753              
 -111.14              0.09808              
 -111.16              0.10067              
 -111.18              0.15657              
 -111.2               0.21345              
 -111.22              0.24034              
 -111.24              0.23860              
 -111.26              0.21045              
 -111.28              0.15101              
 -111.3               0.09763              
 -111.32              0.09717              
 -111.34              0.09834              
 -111.36              0.09476              
 -111.38              0.09004              
 -111.4               0.08478              
 -111.42              0.07902              
 -111.44              0.07283              
 -111.46              0.06626              
 -111.48              0.05936              
 -111.5               0.05220              
 -111.52              0.04483              
 -111.54              0.03731              
 -111.56              0.02969              
 -111.58              0.02203              
 -111.6               0.01439              
 -111.62              0.00682              
 -111.64             -0.00061              
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##END=
