| Note: Toggle plots by clicking on the legend |
Peak |
T site |
Q-type |
Chemical Shift |
Relative |
Peak Width |
Peak Shape |
Assigment |
(topological) | (ppm) |
Peak Area |
(ppm) |
(x)L (1-x)G |
|
P2 | T2 | Q4(4Al) | -30.40 | 1.000 | 1.82 | 0.339 |
P1 | T3 | Q4(4Al) | -28.55 | 1.000 | 1.84 | 0.339 |
P3 | T1 | Q4(4Al) | -12.57 | 1.000 | 1.44 | 0.339 |
| Authors: | He, H., Klinowski, J. | ||||
| Title: | Solid state NMR studies of the aluminophosphate molecular sieve AlPO4-18 | ||||
| Reference: | J. Phys. Chem., 97, 10385-10388 (1993 DOI: 10.1021/j100142a020) |
||||
| Figure: | Figure 2a | ||||
| Authors: | He, H., Klinowski, J. | ||||
| Title: | Solid state NMR studies of the aluminophosphate molecular sieve AlPO4-18 | ||||
| Reference: | J. Phys. Chem., 97, 10385-10388 (1993) DOI: 10.1021/j100142a020 | ||||
| Method: | average bond angles | ||||
| Figure: | Figure 2a | ||||
| Authors: | Simmen, A., McCusker, L.B., Baerlocher, Ch. and Meier, W.M. | |
| Title: | The structure determination and Rietveld refinement of the aluminophosphate AlPO4-18 | |
| Reference: | Zeolites, 11, 654-661 (1991) DOI: 10.1016/S0144-2449(05)80167-8 |
| To reference this collection of solid-state NMR spectra, we suggest: | ||
| Authors: | Brouwer, D.H. and White, A.L. | |
| Title: | A comprehensive collection of solid-state 31P NMR spectra of aluminophosphate zeolites. | |
| Reference: | Microporous Mesoporous Mat., 337, 111934 (2022) DOI: 10.1016/j.micromeso.2022.111934 | |
| Obs. freq. | 162 MHz (Field = 9.4 Tesla) | |
| Pulse sequence | single pulse | |
| MAS frequency | 8-10 kHz | |
| Spectrum | Digitized and processed by Brouwer Lab, Redeemer University | |
| Data processing | Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook |
|
| Comment | Peak assignments are tentative since they are based on average bond angles determined from PXRD |
| [Al - P - O]-AEI |
| Download digitized spectrum in JCAMP-DX format (This file includes also the data listed on this page) | Download all lines from the above plot in .csv format (This file contains only the plotted data) |