Note: Toggle plots by clicking on the legend |
Peak |
T site |
Q-type |
Chemical Shift |
Relative |
Peak Width |
Peak Shape |
Assigment |
(topological) | (ppm) |
Peak Area |
(ppm) |
(x)L (1-x)G |
|
Si2 | T2 | Q4(0Al) | -111.57 | 1.000 | 0.69 | 0.847 |
Si1 | T1 | Q4(0Al) | -107.70 | 4.000 | 0.49 | 0.847 |
Authors: | Fyfe, C.A., Lewis, A.R., Chezeau, J.M., Grondey, H. | ||||
Title: | 19F/29Si Distance Determinations in Fluoride-Containing Octadecasil from Solid-State NMR Measurements | ||||
Reference: | J. Am. Chem. Soc., 119, 12210-12222 (1997) DOI: 10.1021/ja9701873 |
||||
Figure: | Figure 2b | ||||
Authors: | Fyfe, C.A., Lewis, A.R., Chezeau, J.M., Grondey, H. | ||||
Title: | 19F/29Si Distance Determinations in Fluoride-Containing Octadecasil from Solid-State NMR Measurements | ||||
Reference: | J. Am. Chem. Soc., 119, 12210-12222 (1997) DOI: 10.1021/ja9701873 | ||||
Method: | relative intensities | ||||
Figure: | Figure 2b |
Authors: | Caullet, P., Guth, J.L., Hazm, J., Lamblin, J.M. and Gies, H. | |
Title: | Synthesis, Characterization and Crystal Structure of the New Clathrasil Phase Octadecasil | |
Reference: | Eur. J. Solid State Inorg. Chem., 28, 345-361 (1991) |
To reference this collection of solid-state NMR spectra, we suggest: | ||
Authors: | Brouwer, D.H., Brouwer, C.C., Mesa, S., Semelhago, C.A., Steckley, E.E., Sun, M.P.Y., Mikolajewski, J.G., and Baerlocher, Ch. | |
Title: | Solid-state 29Si NMR spectra of pure silica zeolites for the International Zeolite Association Database of Zeolite Structures | |
Reference: | Microporous Mesoporous Mat., 297, 110000 (2020) DOI: 10.1016/j.micromeso.2020.110000 |
Obs. freq. | 79.495 MHz (Field = 9.4 Tesla) | |
Pulse sequence | single pulse | |
MAS frequency | 2.2 kHz | |
Spectrum | Digitized and processed by Brouwer Lab, Redeemer University | |
Data processing | Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook |
[Si - O]-AST |
Download digitized spectrum in JCAMP-DX format (This file includes also the data listed on this page) | Download all lines from the above plot in .csv format (This file contains only the plotted data) |