SFO: NMR spectra

References

Spectrum

	Authors:	Afeworki, M., Cao, G., Dorset, D.L., Strohmaier, K.G., Kennedy, G.J.
	Title:	Multinuclear and multidimensional solid-state NMR characterization of EMM-8
	Reference:	Microporous Mesoporous Mater., 103, 216-224 (2007)
	Figure:	Figure 4a

Peak Assignment

	Authors:	Afeworki, M., Cao, G., Dorset, D.L., Strohmaier, K.G., Kennedy, G.J.
	Title:	Multinuclear and multidimensional solid-state NMR characterization of EMM-8
	Reference:	Microporous Mesoporous Mater., 103, 216-224 (2007)
	Method:	2D correlation NMR
	Figure:	Figure 8a

Crystal Structure

	Authors:	Morris, R.E., Burton, A., Bull, L.M. and Zones, S.I.
	Title:	SSZ-51 - A new aluminophosphate zeotype: synthesis, crystal structure, NMR, and dehydration properties
	Reference:	Chem. Mater., 16, 2844-2851 (2004)

Digitization and Modeling of Spectrum

	To reference this collection of solid-state NMR spectra, we suggest:
	Authors:	Brouwer, D.H. and White, A.L.
	Title:	A comprehensive collection of solid-state ³¹P NMR spectra of aluminophosphate zeolites.
	Reference:	Microporous Mesoporous Mat., 337, 111934 (2022)

Spectrum information

	Obs. freq.	202 MHz (Field = 11.7 Tesla)
	Pulse sequence	single pulse
	MAS frequency	10 kHz
	Spectrum	Digitized and processed by Brouwer Lab, Redeemer University
	Data processing	Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook
	Comment	Peak assignments based on a 2D 27Al/31P correlation spectrum

Chemical Formula

|(DMAP)₄ (H₂O)₂|₂ [Al₁₆P₁₆O₆₄]₂-SFO
DMAP = C₇H₁₀N₂ = 4-dimethylaminopyridine
= N,N-dimethylpyridin-4-amine (stick drawing)

Downloads

	Download digitized spectrum in JCAMP-DX format (This file includes also the data listed on this page)
	Download all lines from the above plot in .csv format (This file contains only the plotted data)